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Journal ArticleDOI

Application of procedures for low level radionuclide analysis in environmental monitoring for the purpose of clearance measurements of materials from decommissioning of nuclear facilities

U. Hoeppener-Kramar, +2 more
- 01 Dec 1997 - 
- Vol. 226, Iss: 1, pp 99-103
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TLDR
In this paper, the procedures for the analysis of radionuclides of prior interest for decommissioning measures are outlined, together with the respective sample decomposition methods, for which adequate procedures were not available, new methods were developed.
Abstract
Materials from decommissioning of nuclear facilities can be re-used without restrictions, if their mass specific activities are in accordance to the guidelines for allowable concentrations. To determine the nuclide specific activity level of representative samples, a “clearance laboratory” was installed at the Research Center Karlsruhe. For the purpose of low level radionuclide analysis, procedures, developed for environmental monitoring, were successfully adapted to decommissioning materials. For radionuclides, for which adequate procedures were not available, new methods were developed. The procedures for the analysis of radionuclides of prior interest for decommissioning measures are outlined, together with the respective sample decomposition methods.

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Citations
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Journal ArticleDOI

Effective desorption of tritium from diverse solid matrices and its application to routine analysis of decommissioning materials

TL;DR: The furnace system investigated is highly effective at extracting tritium and (14)C from all sample types studied (soil, sediment, biota, wood, metal, plastic, concrete, graphite, etc.) and overall it demonstrates high and reproducible recoveries.
Journal ArticleDOI

Determination of 63Ni in the low level solid radioactive waste

TL;DR: In this article, the radiochemical analytical method for deterministic detection of 63 Ni in concrete samples originated from Nuclear Power Plant Mochovce, Slovakia was presented, where the sample of concrete was ashed and leached with aqua regia thereafter hydroxides were precipitated with ammonia solution, leaving Ni in aqueous phase.
Journal ArticleDOI

Improvement of Am and Cm determination in soil samples

TL;DR: In this paper, the determination of Am and Cm in a radiochemical procedure for the sequential analysis of Pu, Am, and cm in soils was improved and optimized using solvent extraction and extraction chromatography.
Journal ArticleDOI

A comparative study using liquid scintillation counting to determine 63Ni in low and intermediate level radioactive waste

TL;DR: In this paper, a comparative study using liquid scintillation counting was performed to measure 63Ni in low and intermediate level radioactive waste, three DMG-based radiochemical procedures (solvent extraction, precipitation, extraction chromatography) were investigated, the solvent extraction method being considered as the reference method.
References
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Journal ArticleDOI

Optimization of a radioanalytical procedure for the determination of uranium isotopes in environmental samples

TL;DR: A radiochemical procedure for the fast and sensitive measurement of uranium isotopes in gaseous and liquid effluents of nuclear facilities is described in this paper, where the detection limit for 1000 minutes of counting time is 2 mBq per sample and nuclide, the chemical yield is in the range of 50 to 80%.
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89Sr/90Sr-Determination in soils and sediments using crown ethers for Ca/Sr-separation

TL;DR: In this article, a radiochemical procedure is described for the sensitive determination of 89Sr and 90Sr activity concentrations in soil and sediment samples, which can be applied to all kind of environmental samples with small modifications of the sample preparation steps prior to analysis.
Journal ArticleDOI

Methods of Radiochemical Analysis

TL;DR: In this article, the authors present Methods of Radiochemical Analysis (MSA), a method for the analysis of radiochemical analysis of radiochemical data. International Journal of Radiation Biology and Related Studies in Physics, Chemistry and Medicine: Vol. 12, No. 2, No 2, pp. 200-200.
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