Journal ArticleDOI
Microwave extraction. A novel sample preparation method for chromatography
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TLDR
The microwave extraction method was more effective than the traditional Soxhlet or shake-flask extraction methods and suitable for fast extractions of large sample series.About:
This article is published in Journal of Chromatography A.The article was published on 1986-12-26. It has received 484 citations till now. The article focuses on the topics: Sample preparation & Extraction (chemistry).read more
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Recent advances in extraction of nutraceuticals from plants
Lijun Wang,Curtis L. Weller +1 more
TL;DR: In this article, a critical review was conducted to introduce and compare the conventional Soxhlet extraction and the new alternative methods used for the extraction of nutraceuticals from plants, and the practical issues of each extraction method were discussed.
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Accelerated Solvent Extraction: A Technique for Sample Preparation
Bruce E. Richter,Brian A. Jones,and John L. Ezzell,Nathan L. Porter,Nebojsa Avdalovic and,Christopher A. Pohl +5 more
TL;DR: In this paper, the authors describe a new technique for sample preparation, accelerated solvent extraction (ASE), that combines elevated temperatures and pressures with liquid solvents, and investigate the effects of various operational parameters (i.e., temperature, pressure, and volume of solvent used) on the performance of ASE.
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Analytical-scale microwave-assisted extraction
TL;DR: This review gives a brief theoretical background of microwave heating and the basic principles of using microwave energy for extraction, and attempts to summarize all studies performed on closed-vessel MAE until now.
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Recent extraction techniques for natural products: microwave-assisted extraction and pressurised solvent extraction.
TL;DR: Through numerous examples, it is demonstrated that both techniques allow reduced solvent consumption and shorter extraction times, while the extraction yields of the analytes are equivalent to or even higher than those obtained with conventional methods.
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Soxhlet extraction of solid materials: an outdated technique with a promising innovative future
TL;DR: An overview of the evolution of Soxhlet extraction of solid materials and its comparison with the performance of other conventional and new extraction techniques is presented in this article, where a discussion on both conventional SoxHlet as compared with other conventional extraction techniques and some minor improvements of the former for specific applications is done.
References
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Journal ArticleDOI
A method for determination of vicine in plant material and in blood.
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Favism‐inducing toxins in broad beans (Vicia faba). Determination of vicine content and investigation of other non‐protein nitrogenous compounds in different broad bean cultivars
TL;DR: Vicine contents of seed coats and cotyledons of 58 cultivars of broad beans are reported and five compounds other than vicine were isolated from broad bean extracts.