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Journal ArticleDOI

The stylus or scratch method for thin film adhesion measurement: some observations and comments

D W Butler, +2 more
- 01 Jun 1970 - 
- Vol. 3, Iss: 6, pp 877-883
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TLDR
In this paper, the effect of applying a rounded stylus to thin metallic films on glass substrates has been investigated using diamond and steel styli with tip radii of approximately 25 μm and loadings of up to 230 g.
Abstract
The effect of applying a rounded stylus to thin metallic films on glass substrates has been investigated using diamond and steel styli with tip radii of approximately 25 μm and loadings of up to 230 g. The films were vacuum-deposited indium, tin, lead, gold, copper, aluminium, nickel, chromium and molybdenum of various thicknesses up to 32 μm. Scanning electron microscope and optical interference microscope observations showed that the process of scratch formation was generally very complex and varied with the film material, indicating that it is not possible to deduce absolute values of adhesion forces using a simple general theoretical model. The method can, however, be used with caution for qualitative comparisons under certain restricted conditions.

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Citations
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Journal ArticleDOI

Adhesion testing by the scratch test method: The influence of intrinsic and extrinsic parameters on the critical load

TL;DR: In this paper, the critical load determined by the scratch test is widely regarded as representative of coating adhesion; however, it remains difficult to express quantitatively the adherence because the critical loads depend on several parameters related to the testing conditions and to the coating-substrate system.
Journal ArticleDOI

Scratch adhesion testing of hard coatings

A.J. Perry
- 16 Sep 1983 - 
TL;DR: In this article, the scratch test for adhesion is reviewed as the only method currently available for testing thin, hard and well-adhering coatings such as TiC on steel or cemented carbide substrates.
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The use of scratch adhesion testing for the determination of interfacial adhesion: The importance of frictional drag

TL;DR: The scratch adhesion test can be considered as a combination of (i) an indentation stress field, (ii) an internal stress field and (iii) a frictional stress field.
Journal ArticleDOI

The science of adhesion

TL;DR: In this paper, the authors reviewed the mechanics and mechanisms of failure of adhesive joints and the effects of various operating environments on joint performance, including surface and interfacial phenomena, including mechanisms of adhesion.
References
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Journal ArticleDOI

Measurement of Adhesion of Thin Films

TL;DR: In this article, a rounded steel point of smooth contour is drawn across the film surface and the load on the point is gradually increased until the film is removed, leaving a clear channel.
Journal ArticleDOI

The Determination of Static and Dynamic Yield Stresses Using a Steel Ball

TL;DR: In this paper, the static and dynamical yield stress of the material of a thick steel plate may be estimated by pressing and by dropping a hard steel ball on a plane surface of the plate which has been ground and then polished.
Journal ArticleDOI

Some factors influencing the adhesion of films produced by vacuum evaporation

TL;DR: HAL as discussed by the authors is a multi-disciplinary open access archive for the deposit and dissemination of scientific research documents, whether they are published or not, which may come from teaching and research institutions in France or abroad, or from public or private research centers.
Journal ArticleDOI

Plastic Flow and Fracture of Glass

TL;DR: In this paper, a completely new approach is attempted in which glass is treated as an elastic-plastic solid and a complete theory of glass flow and strength is developed, based on brittle fracture theory.