Valerio Giannellini

TL;DR: Comparison of ionspray mass spectra of untreated and methanolysed flax-seed extracts confirmed meethanolysis as the crucial step in setting up any further analytical or preparative procedure concerned with secoisolariciresinol diglucoside.

TL;DR: A novel stability-indicating high-performance liquid chromatographic (HPLC) method was developed and validated for the assay of diacerhein in bulk forms and was found to be specific, linear, precise (including intermediate precision), accurate and robust.

TL;DR: The proposed method, exploiting ID without resort to the costly MS instrumentation, could be recommended whenever opportune deuterated analogues of the target analytes and GC capillary columns able to separate all the peaks involved are ready available on the market.

TL;DR: The improvement in attention to metabolic feelings consisted of acquiring a predictive ability of glycemia by distinction between unsolicited hunger feelings (metabolic hunger) and those associated with external cues, which served to predict the subsequent emergence of the metabolic hunger.

TL;DR: In this paper, the collisionally activated decomposition (CAD) experiments have been used for mass spectrometric characterization of fatty acids, revealing useful correlations with the original structure of the neutrals, giving evidence of both chain branching and double bond positions.