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Acicular ferrite formation in a medium carbon steel with a two stage continuous cooling

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Madariaga, Gutie, and Capdevila as discussed by the authors proposed a method for analyzing the properties of Guipu-Zcoa metallurgical properties, and showed that the method can be applied in the field of forensic medicine.
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This article is published in Scripta Materialia.The article was published on 1999-07-09 and is currently open access. It has received 63 citations till now. The article focuses on the topics: Acicular ferrite & Acicular.

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Citations
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On the Role of Non-metallic Inclusions in the Nucleation of Acicular Ferrite in Steels

TL;DR: In this article, the effects of non-metallic inclusions in nucleating acicular ferrite in steels during cooling from a weld or cooling from an austenitic temperature are reviewed.
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Acicular Ferrite Formation and Its Influencing Factors - A Review

TL;DR: In this paper, an overview of the impact of published results and the state of knowledge regarding acicular ferrite formation is provided, focusing on the effect of carbon, manganese and titanium addition to steel, as well as the optimum size, number and composition of non-metallic inclusions.
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Structure–mechanical property relationship in low carbon microalloyed steel plate processed using controlled rolling and two-stage continuous cooling

TL;DR: In this paper, the microstructure and mechanical properties of a low carbon micro-alloyed steel plate of medium thickness gauge were studied in a controlled rolling followed by two-stage continuous cooling.
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Evaluation of Mechanical Properties of Medium Carbon Steel Quenched in Water and Oil

TL;DR: In this paper, the microstructure of the quenched carbon steel samples was studied using optical microscope and the tensile strength and hardness values were relatively higher than those of the ascast samples, suggesting improved mechanical properties.
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Investigation on the behaviour of medium carbon and vanadium microalloyed steels by hot forging test

TL;DR: In this paper, two medium carbon steel grades were used in a controlled closed die forging followed by cooling in sand, air or oil mediums, and the results indicated that the microstructures of all close die forging and cooling conditions are dominated by ferrite and pearlite phases with different morphologies and grain sizes.
References
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Journal ArticleDOI

The mechanism of bainite formation in steels

TL;DR: In this article, microstructural evidence, together with a thermodynamic analysis, of the bainite reaction in steels are presented in support of a growth mechanism involving the propagation of displacive sub-units.
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A rationalisation of shear transformations in steels

TL;DR: In this paper, the authors provided experimental evidence in support of the theory that Widmanstatten ferrite formation involves the co-operative growth of mutually-accommodating plates.
Journal ArticleDOI

Solid-state nucleation of acicular ferrite on minerals added to molten steel

TL;DR: A technique has been developed for making samples of steel with controlled additions of powdered mineral phases as discussed by the authors, which has been studied from the point of view of the acicular ferrite microstructure, which forms when ferrite plates nucleate heterogeneously on nonmetallic inclusions.
Journal ArticleDOI

Formation of acicular ferrite at oxide particles in steels

TL;DR: In this paper, the formation of acicular ferrite is found to be dependent on the presence of a suitable distribution of oxide inclusions > 0·4 μm in size.
Journal ArticleDOI

Stress and the acicular ferrite transformation

TL;DR: In this article, it was shown that large changes in the development of the microstructure are induced when acicular ferrite grows while the austenite is in uniaxial compression.
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Frequently Asked Questions (16)
Q1. What are the contributions in "Acicular ferrite formation in a medium carbon steel with a two stage continuous cooling" ?

Madariaga et al. this paper proposed a two-stage continuous cooling cycle to produce acicular ferrite with a low volume fraction of other phases such as allotriomorphic ferrite, pearlite, and/or martensite. 

3. Lower cooling rates cause the development of other phases such as allotriomorphic ferrite or pearlite but a high volume fraction of acicular ferrite can be achieved using two stage continuous cooling cycles. 

The microstructure is mainly composed of poligonal ferrite and pearlite, with acicular ferrite, which is obtained at lower temperatures. 

Its main interest lies in the good combination of mechanical properties that presents as compared with bainite and above all with ferritic-perlitic microstructures. 

2. The observed inhibition of grain boundary nucleation of bainite enables the formation of fully acicular microstructures, although the high cooling rates (30°C/s) needed to completely avoid the formation of allotriomorphic ferrite reduce its industrial applicability. 

It is accepted that nucleation of acicular ferrite takes place inside the austenite grains at non metallic inclusions, whose nature and number can determine the transition from an acicular ferrite microstructure to a bainitic one. 

3The analysis of the microstructures obtained with isothermal treatments has shown the need for using temperatures below 500°C to ensure a high volume fraction of acicular ferrite plates. 

The results have shown that if the cooling rates required to avoid the formation of a high volume fraction of allotriomorphic ferrite and pearlite are maintained until room temperature, the development of martensite is inevitable. 

The result is an acicular microstructure where the high disorientation and chaotic arrangement does not occur between individual ferrite plates but between these intragranular sheaves. 

Lowering the treatment temperature to 450°C results in a significant increase of the number of ferrite plates at the expense of poligonal ferrite and pearlite, and the resultant microstructure has a clearly acicular appearance, see Fig. 1.d. 

In the present case, this phase is not desired in the microstructure and, in order to elude its formation, the cooling rates have to be lowered after reaching the range of temperatures where acicular ferrite develops. 

The CCT diagram presented in Fig. 2 shows that the non-isothermal austenite-to-acicular ferrite transformation in this steel occurs at cooling rates ranging from 25°C/s to 1°C/s. 

As a result, a two stage continuous cooling cycle is proposed as the best heat treatment to produce acicular ferrite with a low volume fraction of other phases such as alotriomorphic ferrite, pearlite, and/or martensite. 

The former is avoided cooling down at about 7°C/s and the latter is suppressed if cooling is carried out at 30°C/s. Nevertheless, as can be seen in the micrograph of Fig. 3.a, when the samples are continuously cooled down at 30°C/s, the obtained microstructure is martensite, which is not a desired phase due to its detrimental effect in toughness. 

The decomposition of the austenite is not completed before reaching the martensite start temperature, which causes the appearance of this phase at the end of the cooling. 

Micrographs of the isothermal treatments presented in Fig. 1 indicate that the formation of a great number of acicular ferrite plates takes place under 500°C, which has motivated the choice of this temperature, below the acicular ferrite start temperature for all the cooling rates tested in the CCT, as the temperature where the cooling rate is lowered.