Crystal structure of diethyl 2-(2-chlorophenyl)-1,3-dioxane-5,5-dicarboxylate, C16H19Cl1O6
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TLDR
In this paper, the triclinic P1̅ (no. 2), a = 7.905(3), b = 9.194(4) Å, c = 13.094(5)Å, α = 99.928°, β = 105.341°, γ = 109.283°, V = 830.2Abstract:
Abstract C16H19ClO6, triclinic, P1̅ (no. 2), a = 7.905(3) Å, b = 9.194(4) Å, c = 13.094(5) Å, α = 99.928(4)°, β = 105.341(4)°, γ = 109.283(4)°, V = 830.2(6) Å3, Z = 2, Rgt(F) = 0.0343, wRref(F2) = 0.0898, T = 296(2)K.read more
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Journal Article
Tethering for Selective Synthesis of 2,2′-Biphenols : the Acetal Method
TL;DR: In this article, the 2,2'-biphenols were obtained by stepwise tethering of two monomeric phenols, and the resulting dibenzo[1,3]dioxepines were analyzed by quantum chemical calculations to obtain information about the activation barrier for ring flip between the enantiomers.
References
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A short history of SHELX
TL;DR: This paper could serve as a general literature citation when one or more of the open-source SH ELX programs (and the Bruker AXS version SHELXTL) are employed in the course of a crystal-structure determination.
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OLEX2: a complete structure solution, refinement and analysis program
TL;DR: OLEX2 seamlessly links all aspects of the structure solution, refinement and publication process and presents them in a single workflow-driven package, with the ultimate goal of producing an application which will be useful to both chemists and crystallographers.
Book
Protecting Groups in Organic Synthesis
TL;DR: The protection of alcohols, aldehydes, and carboxylic acids has been extensively studied in the literature, see as discussed by the authors for a detailed survey of the most common abbreviations for protecting groups and reagents.
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Protecting groups in organic synthesis. Part 8. Conversion of aldehydes into geminal diacetates
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Tethering for Selective Synthesis of 2,2′‐Biphenols: The Acetal Method
TL;DR: Hydlytic removal of the dioxepine acetal unit revealed the 2,2'-biphenol target and the resulting dibenzo[1,3]dioxepines have been analysed by quantum chemical calculations to obtain information about the activation barrier for ring flip between the enantiomers.
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