Journal ArticleDOI
Multiple solid-phase microextraction: Theory and applications
TLDR
A review of the state of the art in MSPME, including theory and applications, can be found in this article, where the authors also discuss the limits of detection and quantification, and the use of this methodology to determine fiber-sample distribution constant.Abstract:
Multiple solid-phase microextraction (MSPME) is a stepped procedure suitable for avoiding matrix-effect errors in quantitative analyses of complex matrix samples by SPME. It is based on calculating the amount of analyte corresponding to complete extraction using the peak areas of a few consecutive extractions from the same sample. This article reviews the state of the art in MSPME, including theory and applications. It also includes a debate on calculating the limits of detection and quantification, and the use of this methodology to determine fiber-sample distribution constant.read more
Citations
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Journal ArticleDOI
A critical review in calibration methods for solid-phase microextraction
Gangfeng Ouyang,Janusz Pawliszyn +1 more
TL;DR: In this review, a summary of the proposed SPME calibration methods was summarized and the characteristics of these methods were discussed.
Journal ArticleDOI
Recent advances in SPME techniques in biomedical analysis
Hiroyuki Kataoka,Keita Saito +1 more
TL;DR: This review focuses on recent advances in novel SPME techniques, including fiber S PME and in-tube SPMe, in biomedical analysis and summarizes the applications of these techniques to pharmacotherapeutic, forensic, and diagnostic studies, and to determinations of environmental and occupational exposure.
Journal ArticleDOI
Recent developments in solid-phase microextraction for on-site sampling and sample preparation
TL;DR: Solid-phase microextraction (SPME) has been widely used in on-site sampling and sample preparation applications as mentioned in this paper, including fiber SPME, stir-bar SBSE, thin-film micro-extraction, and different types of in-needle SPMEs.
Journal ArticleDOI
Sorbent- and liquid-phase microextraction techniques and membrane-assisted extraction in combination with gas chromatographic analysis: A review.
TL;DR: Solid-phase microextraction (SPME), stir-bar sorptive extraction (SBSE), on-line solid-phase extraction (SPE), liquid-phaseMicroExtraction (LPME) and membrane-assisted methods are critically evaluated and the applicability of each technique is demonstrated with examples.
Journal ArticleDOI
Establishment of the contribution of volatile compounds to the aroma of fermented sausages at different stages of processing and storage.
TL;DR: In this paper, the most important aroma compounds were determined using their odour-activity values (OAVs), and the compound quantification in the headspace (HS) was carried out by solid phase microextraction (SPME) and the total concentration in the sausage by multiple headspace SPME (multiple HS-SPME).
References
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Journal ArticleDOI
Solid phase microextraction with thermal desorption using fused silica optical fibers
Book
Solid phase microextraction : theory and practice
TL;DR: The inventor of the technique, Janusz Pawliszyn, describes the theoretical and practical aspects of this new technology, which received an "RD" rating.
Book
Applications of Solid Phase Microextraction
TL;DR: The use of SPME to measure free concentrations and phospholipid/water and protein/water partition coefficients of organic compounds has been extensively used in the literature as discussed by the authors.
Journal ArticleDOI
Automation and optimization of solid-phase microextraction
TL;DR: The solid phase microextraction (SPME) technique as mentioned in this paper involves exposing a fused silica fiber that has been coated with a stationary phase to and aqueous solution containing organic contaminants.
Journal ArticleDOI
Solid-phase microextraction
TL;DR: Solid-phase microextraction (SPME) as mentioned in this paper is a sample preparation technique that minimizes the consumption of organic solvents and has been shown to be useful in analytical chemistry.