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Journal ArticleDOI

Phthalates determination in physiological saline solutions by HPLC-ES-MS.

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TLDR
The proposed analytical method has been applied to the analysis of commercial physiological saline solutions in order to check the presence of phthalates and to determine their concentration.
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This article is published in Talanta.The article was published on 2008-06-15. It has received 41 citations till now. The article focuses on the topics: Detection limit & Population.

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Fast microextraction of phthalate acid esters from beverage, environmental water and perfume samples by magnetic multi-walled carbon nanotubes

TL;DR: The MSPE-GC/MS method developed in current study provides a new option for the detection of PAEs from real samples with complex matrices and was successfully applied to the determination ofPAEs from bottled beverages, tap water and perfume samples.
Journal Article

On-line clean-up by multidimensional liquid chromatography-electrospray ionization tandem mass spectrometry for high throughput quantification of primary and secondary phthalate metabolites in human urine

TL;DR: In this paper, a multidimensional on-line HPLC method was developed for the quantitative determination of the secondary, chain oxidized monoester metabolites of diethylhexylphthalate (DEHP), 5-hydroxy-mono-(2-ethylhexyl)-phthalate(5OH-MEHP) and 5-oxo-mmono-polymethylmethylmethane (5ox-mphosphate) in urine samples from the general population.
Journal ArticleDOI

A review of separation methods for the determination of estrogens and plastics-derived estrogen mimics from aqueous systems

TL;DR: Various types of separation techniques are presented, with the express goal of emphasizing time and cost-effective methods that isolate and quantify trace-levels of multiple endocrine disruptors from aqueous systems.
Journal ArticleDOI

Polythiophene-coated Fe3O4 superparamagnetic nanocomposite: synthesis and application as a new sorbent for solid-phase extraction.

TL;DR: A novel type of superparamagnetic nanosorbent, polythiophene-coated Fe3O4 nanoparticles, have been successfully synthesized and applied as an efficient sorbent for extraction and preconcentration of several typical plasticizers from environmental water samples.
Journal ArticleDOI

Application of new approaches to liquid-phase microextraction for the determination of emerging pollutants

TL;DR: In this article, the application of liquid-phase microextraction (LPME) techniques to the analysis of emerging pollutants has been discussed, including single-drop micro-extraction, hollow-fiber LPME, dispersive liquid-liquid micro extractions (DLLME), and solidified floating organic drop micro extraction (SFODME).
References
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Journal ArticleDOI

Multi-walled carbon nanotubes packed cartridge for the solid-phase extraction of several phthalate esters from water samples and their determination by high performance liquid chromatography

TL;DR: In this article, a new solid-phase extraction system for HPLC determination of di-ethyl-phthalate, di-n-propylphthalate and di-cyclohexyl-phthalates was developed.
Journal ArticleDOI

Social and economic interest in the control of phthalic acid esters

TL;DR: An overview of the economic and social interest in the control of phthalate esters and in the availability of analytical methodologies for areas such as environmental and food analyses can be found in this paper.
Journal ArticleDOI

Hollow-fibre liquid-phase microextraction of phthalate esters from water.

TL;DR: The ability of both microextraction methods to concentrate many organic analytes was demonstrated as both methods allowed the confirmation of the presence of an extra contaminant in bottled mineral water samples.
Journal ArticleDOI

Determination of phthalate esters in water samples by solid-phase microextraction and gas chromatography with mass spectrometric detection.

TL;DR: Solid-phase microextraction with an 85 microm polyacrylate fiber, coupled to gas chromatography-mass spectrometry was used to determine six phthalate esters and bis(2-ethylhexyl) adipate in water samples to analyze both tap and commercial mineral water samples.

Determination of phthalate esters in water samples by solid-phase microextraction and gas chromatography with mass spectrometric

TL;DR: In this article, solid phase microextraction (SPME) with an 85 mm polyacrylate fiber coupled with gas chromatography-mass spec- trometry was used to determine six phthalate esters and bis(2-ethylhexyl) adipate in water samples.
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