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Stir casting process for manufacture of Al–SiC composites

TLDR
In this paper, microstructural characterizations of aluminum matrix composites at two casting temperatures (680 and 850°C) and stirring periods (2 and 6min) were evaluated by scanning electron microscopy (SEM) and high-resolution transition electron microscope (HRTEM) studies.
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This article is published in Rare Metals.The article was published on 2017-07-01 and is currently open access. It has received 176 citations till now. The article focuses on the topics: Chemical vapor infiltration & Ceramic.

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Composites Part A: Applied Science and Manufacturing

TL;DR: In this article, the authors present a Web of Science Record created on 2013-02-27, modified on 2017-05-10 and used for EPFL-ARTICLE-184271.

Materials by Design

TL;DR: Suib is a Board of Trustees Distinguished Professor of Chemistry and received the CT Medal of Science for his work in catalysis, semiconductors and ceramic composites as discussed by the authors.
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Recent progress in aluminum metal matrix composites: A review on processing, mechanical and wear properties

TL;DR: In this paper, a review of recent advances in processing, microstructure, wear, and mechanical characterization of aluminum composites reinforced with different particles are addressed, and future scope of these composites is also briefly discussed at the end of the manuscript.
References
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Hall-Petch relation and boundary strengthening

Niels Hansen
- 01 Oct 2004 - 
TL;DR: In this article, the Hall-Petch relation is discussed separately for the yield stress of polycrystalline metals and for the flow stress of deformed metals for a grain size range from about 20 nm to hundreds of micrometers.
Journal ArticleDOI

Particulate reinforced metal matrix composites — a review

TL;DR: The physical and mechanical properties that can be obtained with metal matrix composites (MMCs) have made them attractive candidate materials for aerospace, automotive and numerous other applications as discussed by the authors.
Journal ArticleDOI

Metal matrix composites: production by the stir casting method

TL;DR: In this paper, the relatively low cost stir casting technique is evaluated for use in the production of silicon carbide/aluminium alloy MMCs, and the technical difficulties associated with attaining a uniform distribution of reinforcement, good wettability between substances, and a low porosity material are presented and discussed.
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Wettability and spreading kinetics of molten aluminum on copper-coated ceramics

TL;DR: In this paper, the influence of Cu-coating on the spreading kinetics and equilibrium contact angles of aluminum on ceramics using a sessile drop technique was investigated.
Related Papers (5)
Frequently Asked Questions (18)
Q1. What was used as a protective shroud on the melt surface?

A preheated graphite stirrer was placed below the surface of melt and rotated at a speed of 500 r min -1 , and simultaneously argon gas of high purity was used as a protective shroud on the melt surface. 

In this study, micron-sized SiC particles were used as reinforcement to fabricate Al-3 wt % SiC composites at two casting temperatures ( 680 and 850 C ) and stirring periods ( 2 and 6 min ). Factors of reaction at matrix/ceramic interface, porosity, ceramic incorporation, and agglomeration of the particles were evaluated by scanning electron microscope ( SEM ) and high-resolution transition electron microscope ( HRTEM ) studies. 

It was reported that the porosity in cast MMCs was originated from gas entrapment during stirring, water vapor (H2O) on the surface of ceramic particles, hydrogen evolution, air bubbles entering the slurry as an air envelope to the reinforcement particles, and shrinkage during solidification process [9]. 

A high-resolution transmission electron microscope (HRTEM, Philips CM200) at an accelerating voltage of 200 kV was also used to study the reaction at the interface of the aluminum matrix and SiC particles. 

Gas pores, solidification shrinkage, and air gap between the agglomerated ceramic particles were observed in the samples after stir casting, while by changing the stirring time and temperature, the type and the amount of porosities could be altered. 

The main aim of this study is to lessen the number of defect locations within AMMCs produced from the stir casting method and hence to improve the quality of the fabricated composites. 

the following considerations for achieving AMMC via stir casting must be considered: no adverse chemical reaction between the reinforcement material and matrix alloy, no or very low porosity content in the cast AMMCs, wettability between the two main phases, and a uniform distribution of the reinforcement material. 

Line energy dispersive X-ray spectroscopy (EDX) microanalysis (Fig. 6) was used to evaluate thechemical characterization around a ceramic particle in Sample 3. 

After characterization, needlelike Al4C3 phase is detected with a different orientation growth from the crystalline plane orientations of silicon carbide. 

A higher stirring temperature would lead to a further incorporation of ceramic particles into the molten pure aluminum with an improved distribution. 

As can be seen, the on-set of aluminum melting is evident from about 650 C (endothermic peak) and just after this, an exothermic trend could be observed, which corresponds to the occurrence of a reaction between Al and SiC, leading to a large release of heat. 

No suitable bonding was obtained at the metal/ceramic interface for the stirring time of 2 min, indicating that a minimum stirring time is necessary for ceramic particles to be in contact with the melt to form a strong bond with the matrix. 

The considerable formation of shrinkage porosity at the interface significantly reduces the strength of the composite, even though it has a larger amount of ceramic particle incorporations. 

Stirring for 2 min at 680 C is not along-enough period or high-enough temperature combination process for the migration of carbon atoms and the formation of suitable bond between Al and SiC particles. 

The amount of ceramic particles incorporated into the molten aluminum was determined by leaching the composite using 2 mol L -1 hydrochloric acid, resulting in the removal of aluminum phase. 

it could be concluded that the presence of ceramic particles and the formation of shrinkage porosities around the particles are the two most important factors in determining the AMMC ductility as well as the mechanical properties in general. 

Agglomeration of the micron-sized SiC particles could be observed in all the samples, indicating that the stirring time, temperature, and viscosity of the melt could not affect this phenomenon. 

In order to determine the onset reaction temperature between pure aluminum and SiC powders, differential scanning calorimetry (DSC, Netzsch STA 409, Germany) was performed. 

Trending Questions (1)
What is stir castinbg?

Stir casting is an economical process used to fabricate aluminum matrix composites. It involves the incorporation of reinforcement particles, such as SiC, into the aluminum matrix through stirring at specific temperatures and periods.