M
Masaki Takata
Researcher at Tohoku University
Publications - 598
Citations - 31366
Masaki Takata is an academic researcher from Tohoku University. The author has contributed to research in topics: Powder diffraction & Charge density. The author has an hindex of 90, co-authored 594 publications receiving 28478 citations. Previous affiliations of Masaki Takata include Shimane University & National Institute for Materials Science.
Papers
More filters
Journal ArticleDOI
Electron density distribution of α-gallium
Journal ArticleDOI
Crystallization behavior of polyethylene on silicon wafers in solution casting processes traced by time-resolved measurements of synchrotron grazing-incidence small-angle and wide-angle X-ray scattering
Sono Sasaki,Hiroyasu Masunaga,K. Itou,Kohji Tashiro,Hiroshi Okuda,Atsushi Takahara,Masaki Takata +6 more
Abstract: Crystallization behavior of polyethylene (PE) on silicon wafers in solution casting processes has been successfully traced by time-resolved grazing-incidence small-angle and wide-angle X-ray scattering (GISWAXS) measurements utilizing synchrotron radiation. A p-xylene solution of PE kept at ca. 343 K was dropped on a silicon wafer at ca. 298 K. While the p-xylene evaporated naturally from the dropped solution sample, PE chains crystallized to be a thin film. Raman spectral measurements were performed simultaneously with the GISWAXS measurements to evaluate quantitatively the p-xylene the dropped solution contained. Grazing-incidence wide-angle X-ray scattering (GIWAXS) patterns indicated nucleation and crystal growth in the dropped solution and the following as-cast film. GIWAXS and Raman spectral data revealed that crystallization of PE was enhanced after complete evaporation of the p-xylene from the dropped solution. The [110] and [200] directions of the orthorhombic PE crystal became relatively parallel to the wafer surface with time, which implied that the flat-on lamellae with respect to the wafer surface were mainly formed in the as-cast film. On the other hand, grazing-incidence small-angle X-ray scattering (GISAXS) patterns implied formation of isolated lamellae in the dropped solution. The lamellae and amorphous might alternatively be stacked in the preferred direction perpendicular to the wafer surface. The synchrotron GISWAXS experimental method could be applied for kinetic study on hierarchical structure of polymer thin films.
Journal ArticleDOI
Nuclear density distribution in KH2PO4 determined by the combined software system remedy
Shintaro Kumazawa,S. Yamamura,Eiji Nishibori,Masaki Takata,Makoto Sakata,Fujio Izumi,Yoshinobu Ishii +6 more
TL;DR: In this paper, the nuclear density distributions for both paraelectric and ferroelectric phases of KDP were obtained by the software system named remedy, which is a combined program system of Rietveld refinement, rietan -98, and the maximum entropy method, mend for neutron diffraction.
Journal ArticleDOI
Structural Evolution Process of isotactic Polypropylene in the Isothermal Crystallization from the Melt
Kummetha Raghunatha Reddy,Kohji Tashiro,Takashi Sakurai,Noburu Yamaguchi,Makoto Hanesaka,Sono Sasaki,Hiroyasu Masunaga,Masaki Takata +7 more
TL;DR: In this article, the authors investigated the melt-isothermal crystallization behavior for isotactic polypropylene (iPP) by means of time-resolved simultaneous measurements of small-angle X-ray scattering (SAXS) and wide-angle x-ray diffraction (WAXD) using synchrotron radiation source in SPring-8.
Journal ArticleDOI
Epitaxy-driven Nanostructure Formation in Polymer Blend Thin Films Containing Regioregular Poly(3-hexylthiophene)
Hirotaka Ejima,Kazuhiro Ogita,Midori Yamamoto,Sono Sasaki,Takaaki Hikima,Masaki Takata,Naoko Yoshie +6 more
TL;DR: In this paper, Epitaxial crystallization onto a directionally crystallizable organic solvent, 1,3,5 trichlorobenzene, was applied to polymer blends containing regioregular poly(3-hexylthiophene-2,5-diyl) (P3HT) a...