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Influence of silicon content on the precipitation of secondary carbides and fatigue properties of a 5%Cr tempered martensitic steel

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TLDR
In this paper, the effect of silicon on the stability of secondary carbides was studied using transmission electron microscopy and small-angle neutron scattering, and it was concluded that silicon has a detrimental effect as it shifts the secondary hardening peak towards lower tempering temperatures.
Abstract
In comparison with the conventional AISI H11 tool steel, which contains approximately 1 wt.% silicon, the modified steel AISI H11 (∼0.35 wt.% silicon) exhibits improved tensile and fatigue properties at 550 °C – the estimated tool surface temperature during the high-pressure injection of aluminium alloys. The effect of silicon on the stability of secondary carbides was studied using transmission electron microscopy and small-angle neutron scattering. Silicon has a considerable influence on the precipitation of secondary carbides. A higher volume fraction and density of small particles were observed in the low-silicon-grade steel, both after heat treatment and after fatigue testing. The final discussion focuses on the influence of silicon in the precipitation sequence. It is concluded that silicon has a detrimental effect as it shifts the secondary hardening peak towards lower tempering temperatures.

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Journal ArticleDOI

The effect of the addition of alloying elements on carbide precipitation and mechanical properties in 5% chromium martensitic steels

TL;DR: In this paper, small angle neutron scattering and X-ray diffraction experiments, as well as transmission electron microscopy, were performed to characterize the precipitation of nanometric carbides, and the mechanical properties showed that the volume fraction of small precipitates directly influences the mechanical resistance at high temperature but has a detrimental effect on Charpy impact energy.
Journal ArticleDOI

High-temperature properties and microstructural stability of hot-work tool steels

TL;DR: In this article, the softening properties of tool steels with respect to their microstructure and high-temperature mechanical properties were investigated by tempering and isothermal fatigue testing.
Journal ArticleDOI

In-situ strengthening of a high strength low alloy steel during Wire and Arc Additive Manufacturing (WAAM)

TL;DR: In this article, SiC particles were added to the molten pool during WAAM of a high strength low alloy steel, and the introduction of these high melting point particles promoted grain refinement and precipitation of Fe3C due to SiC dissociation.
Journal ArticleDOI

The effect of silicon on precipitation and decomposition behaviors of M6C carbide in a Ni–Mo–Cr superalloy

TL;DR: In this paper, the effect of silicon addition on the precipitation and decomposition behaviors of M 6 C carbide in a Ni-Mo-Cr based superalloy and the tensile properties of this alloy have been investigated.
Journal ArticleDOI

The effects of annealing temperature and cooling rate on carbide precipitation behavior in H13 hot-work tool steel

TL;DR: In this article, the precipitation behavior of H13 hot-work tool steel was investigated as a function of both annealing temperature and cooling rate through thermodynamic calculations and microstructural analyses using transmission and scanning electron microscope and a dilatometer.
References
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Journal ArticleDOI

Neutron scattering lengths and cross sections

TL;DR: The application of thermal neutron scattering to the study of the structure and dynamics of condensed matter requires a knowledge of the scattering lengths and the corresponding scattering and absorption cross sections of the elements as discussed by the authors.
Book

Steels, Microstructure and Properties

TL;DR: In this article, the authors studied the effects of alloying elements in iron-carbon alloys and the formation of martensite, bainite reaction and acicular ferrite reaction.
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Bainite in Steels

TL;DR: The mechanism of the bainite transformation in steels is reviewed in this paper, with a summary of the early research and concluding with an assessment of the transformation in the context of the other reactions which occur as austenite is cooled to temperatures where it is no longer the stable phase.
Journal ArticleDOI

Structure and Resistivity of Liquid Metals

TL;DR: In this article, the authors used the known solution of the Percus-Yevick equation for this model to give a simple closed form for $a(K)$ (the liquid structure factor) which depends only on the effective packing density of the fluid.
Journal ArticleDOI

The evolution of dislocation density during heat treatment and creep of tempered martensite ferritic steels

TL;DR: In this article, the evolution of dislocation density in two tempered martensite ferritic steels (a 12% and a 9% chromium steel, X20 and P91) during heat treatment and creep is analyzed using transmission electron microscopy (TEM) and X-ray diffraction (XRD); both methods yield results which are in good agreement when rationalizing the XRD-data based on densities of free dislocations.
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