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Open AccessJournal ArticleDOI

Mass and heat transfer in ternary distillation of methanol-ethanol-water systems by a wetted-wall column

TLDR
In this article, an experimental study of vapor-phase sensible heat and mass fluxes in ternary distillation of the methanol-ethanol-water system was made with a wetted-wall column at total reflux conditions.
Abstract
Experimental study of vapor-phase sensible heat and mass fluxes in ternary distillation of the methanol-ethanol-water system was made with a wetted-wall column at total reflux conditions. From heat and mass balances for the liquid film, a theoretical expression was derived for the interfacial velocity caused by mass fluxes. The interfacial velocity was shown to be a function of the sensible heat and diffusion fluxes. Observed vapor-phase sensible heat fluxes showed good agreement with the theoretical values obtained by laminar flow theories. Observed vapor-phase diffusion fluxes obtained from mass flux measurements also showed good agreement with the theoretical values, but a poor correlation was obtained for vapor-phase mass fluxes. Observed interfacial velocities were compared with the calculated values.

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Journal ArticleDOI

A background review on falling film distillation in wetted-wall columns: From fundamentals towards intensified technologies

TL;DR: In this article, a review brings a historical perspective of theoretical and experimental works as well as deposited patents on falling film distillation from the beginning of 20th Century to present, aiming to guideline future perspectives in chemical separations.
Journal ArticleDOI

Simulation and optimization of heterogeneous azeotropic distillation process with a rate-based model

TL;DR: In this article, a rate-based simulation method for sieve tray columns is developed with the correlations of clear liquid height and mass transfer rate that were obtained in previous experiments of the homogeneous and heterogeneous ternary distillation with a Sieve tray column.
Journal ArticleDOI

Hydrodynamics and mass transfer in heterogeneous distillation with sieve tray column

TL;DR: In this article, the effect of liquid-phase resistance on separation performance of a sieve tray column in heterogeneous distillation is studied experimentally under total reflux conditions, and a correlation for clear liquid height in the heterogeneous liquid region is obtained by modifying the correlation of the homogeneous systems.
Journal ArticleDOI

Mass Transfer in Binary and Ternary Distillation by a Packed Column with Structured Packing

TL;DR: In this paper, a mass transfer correlation for distillation using a laboratory size wire-gauze structured packing was developed in terms of dimensionless diffusion flux based on experimental data for an acetone-ethanol system under total reflux conditions.
Journal ArticleDOI

Mass transfer in binary distillation of nitrogen-oxygen and argon-oxygen systems in a wetted-wall column

TL;DR: In this paper, mass fluxes in binary distillation of the nitrogen-oxygen and argonoxygen systems in a wetted-wall column were made under total reflux conditions for a wide range of turbulent flows.
References
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Book

Convective Heat and Mass Transfer

TL;DR: In this article, the echangeurs de : chaleur, couche de : limite, modeles de : turbulence, transfert de masse reference record created on 2005-11-18, modified on 2016-08-08
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