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Journal ArticleDOI

Silicon Particle Formation by Pyrolysis of Silane in a Hot Wall Gasphase Reactor

Hartmut Wiggers, +2 more
- 01 Mar 2001 - 
- Vol. 24, Iss: 3, pp 261-264
TLDR
In this article, the formation of silicon powder by pyrolysis of silane diluted in argon at different concentrations has been studied, where a hot wall gas-phase reactor was used for the thermal decomposition of SiH 4 at 1000°C and atmospheric pressure.
Abstract
The formation of silicon powder by pyrolysis of silane diluted in argon at different concentrations has been studied. A hot wall gas-phase reactor was used for the thermal decomposition of SiH 4 at 1000°C and atmospheric pressure. The composition, morphology, size, and shape of the particles produced has been studied utilizing electron microscopy, X-ray diffraction, infrared spectroscopy, and BET gas adsorption. Depending on the experimental conditions, agglomerates of polycrystalline, sintered particles have been obtained, which are composed of nanocrystallites of about 25 nm in size.

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Performance and cost of materials for lithium-based rechargeable automotive batteries

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Plasma synthesis of nanostructures for improved thermoelectric properties

TL;DR: In this article, the synthesis and processing of doped silicon nanoparticles from gas phase plasma synthesis is studied with respect to the utilization of silicon-based materials for thermoelectrics, and the requirements for the formation of dense sintered bodies, while keeping the crystallite size small.
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Gas-phase synthesis of functional nanomaterials: Challenges to kinetics, diagnostics, and process development

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Silicon/Polyaniline Nanocomposites as Anode Material for Lithium Ion Batteries

TL;DR: In this paper, the authors combined nano-silicon (n-Si) active material with an inactive material that acts as a binder and buffering matrix to improve the cycling behavior of lithium ion batteries.
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