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Two-Dimensional Time-Resolved X-ray Diffraction Study of Directional Solidification in Steels

TLDR
In this article, in situ characterization of directional solidification process during welding was carried out using the time resolved X-ray diffraction technique utilizing intense synchrotron radiation, and the behavior of dendrites in steels under welding conditions of a practical manufacturing process were investigated using the TRXRD method for in-situ weld observation with the uniquely-sensitive two-dimensional pixel detector.
Abstract
In situ characterization of directional solidification process during welding was carried out using the time resolved X-ray diffraction technique utilizing intense synchrotron radiation. Then, behaviour of dendrites in steels under welding conditions of a practical manufacturing process were investigated using the TRXRD method for in-situ weld observation with the uniquely-sensitive two-dimensional pixel detector. Consequently, the crystal growth during the rapid cooling was caught in detail and employed a systematic peak profile analysis in order to acquire the essential information for controlling the weld microstructure. Our results would suggest the microstructure formation process of low alloy in directional solidification during rapid cooling. Simultaneously, we discuss the possibility of detecting the nucleation.

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Revisiting the Structure of Martensite in Iron-Carbon Steels

TL;DR: In this paper, the formation and crystal structure of martensite in quenched Fe-C steels based on the extensive published literature on the subject is described. But the authors focus on the H-point, which is defined as the point at which martensites will form at the highest C contents.
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A new nanoscale metastable iron phase in carbon steels

TL;DR: An intensive TEM investigation revealed that extra diffraction spots observed by transmission electron microscopy are in fact attributed to the metastable ω phase in particle-like morphology with an overall size of several or dozens of nanometres.
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Real time observation of martensite transformation for a 0.4C low alloyed steel by neutron diffraction

TL;DR: In this article, a high-intensity and high-resolution neutron diffractometer with a thermomechanically controlled processing simulator was employed in-situ to investigate martensite transformation behavior with and without ausforming for a medium-carbon low-alloy steel.
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In situ observation of phase transformation in Fe–0.15C binary alloy

TL;DR: In this paper, high temperature laser scanning confocal microscopy with an infrared imaging furnace has been used to directly observe the morphological development of γ-→-α transformations, which makes possible that phase transformation can be identified in real time during heating and continuously cooling process.
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Single photon counting pixel detectors for synchrotron radiation experiments

TL;DR: PILATUS as mentioned in this paper is an X-ray single photon counting pixel detector based on the hybrid-pixel detector technology, which was developed in collaboration with SPring-8.
References
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Book

Elements of X-ray diffraction

TL;DR: In this article, the authors present a chemical analysis of X-ray diffraction by Xray Spectrometry and phase-diagram Determination of single crystal structures and phase diagrams.
Journal Article

The Rietveld method

TL;DR: In this paper, the early days of the Rietveld method are described, along with a retrospective view of its application in various areas of physics, such as X-ray and neutron analysis.
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Über den Mechanismus der Stahlhärtung

TL;DR: Herstellung von teilweise in Martensit zerfallenen Austenitkristallen durch lang-same Erstarrung and nachfolgendes Abschrecken.
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