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In situ raman spectroscopy of solid catalyzed reactions in supercritical co2 within a si/glass microreactor
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TLDR
In this article, the in situ monitoring of a solid catalyzed reaction by Raman spectroscopy in a packed bed Si/glass microreactor up to pressures of 10 MPa is reported.References
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Fabrication, mechanical testing and application of high-pressure glass microreactor chips
Roald M. Tiggelaar,Fernando Benito-Lopez,D.C. Hermes,Helmut Rathgen,Richard J.M. Egberink,Frieder Mugele,David N. Reinhoudt,Albert van den Berg,Willem Verboom,Han J.G.E. Gardeniers +9 more
TL;DR: In this paper, the design, fabrication and high pressure performance of several inplane fiber-based interface geometries to microreactor chips for high pressure chemistry are discussed, and an application is presented.
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Operating characteristics of a transpiring-wall SCWO reactor with a hydrothermal flame as internal heat source
TL;DR: In this paper, a transpiring-wall reactor with a hydrothermal flame as internal heat source has been investigated, where the wall contact of supercritical reaction media is prevented by fluid dynamical means.
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Transparent silicon/glass microreactor for high-pressure and high-temperature reactions
TL;DR: In this paper, a Si/glass microreactor with soldered microfluidic connections for high-pressure and high-temperature applications is presented, which is applied for a well-described solid catalyzed exothermic hydrogenation at operating conditions up to 51 bar and 71°C.
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Hydrogenation reactions using scCO2 as a solvent in microchannel reactors
TL;DR: The reactions proceeded very rapidly (within 1 second), by making the best use of scCO(2) and utilizing the large specific interfacial area of the microchannel reactor, and high reaction productivity was attained in each channel.