Journal ArticleDOI
Spectroscopic and microscopic investigations of the thermal decomposition of nickel oxysalts: Part 2. Nickel nitrate hexahydrate
TLDR
In this article, the thermal decomposition of nickel nitrate hexahydrate (NiNHH) under dynamic atmosphere of air has been thoroughly studied using infrared spectroscopy and X-ray diffractometry.About:
This article is published in Thermochimica Acta.The article was published on 1993-11-15. It has received 22 citations till now. The article focuses on the topics: Thermal decomposition & Differential thermal analysis.read more
Citations
More filters
Journal ArticleDOI
Oxygen Evolution Reaction Dynamics, Faradaic Charge Efficiency, and the Active Metal Redox States of Ni–Fe Oxide Water Splitting Electrocatalysts
Mikaela Görlin,Petko Chernev,Jorge Ferreira de Araújo,Tobias Reier,Sören Dresp,Benjamin Paul,Ralph Krähnert,Holger Dau,Peter Strasser +8 more
TL;DR: It is concluded that a discussion of the superior catalytic OER activity of Ni-FeOOH electrocatalysts in terms of surface catalysis and redox-inactive metal sites likely represents an oversimplification that fails to capture essential aspects of the synergisms at highly active Ni- Fe sites.
Journal ArticleDOI
Development of Ni-Pd bimetallic catalysts for the utilization of carbon dioxide and methane by dry reforming
TL;DR: In this article, Ni-Pd bimetallic supported catalysts were prepared by simple impregnation method using various carriers, and the catalytic performance of the catalysts was investigated at 500, 600 and 700°C under atmospheric pressure and a CH 4 to CO 2 feed ratio of 1.5 wt% revealed the best results.
Journal ArticleDOI
Monolithic nickel(II)-based aerogels using an organic epoxide: the importance of the counterion
TL;DR: In this paper, the epoxide addition method was used to obtain a monolithic pure nickel (II) oxide aerogel material using powder X-ray diffraction, electron microscopy and elemental analysis.
Journal ArticleDOI
The Leidenfrost effect during spray pyrolysis of nickel oxide-gadolinia doped ceria composite thin films
TL;DR: In this paper, thin films were prepared by air blast spray pyrolysis with precursors containing nickel nitrate, cerium nitrate and gadolinium chloride in ethanol and a high boiling point organic solvent.
Journal ArticleDOI
Densification and grain growth of 8YSZ containing NiO
TL;DR: In this paper, the effects of NiO addition on sintering yttria-stabilized zirconia were systematically studied to understand the role of the additive in the sinting process of the solid electrolyte.
References
More filters
Journal ArticleDOI
Kinetic Parameters from Thermogravimetric Data
A. W. Coats,J. P. Redfern +1 more
TL;DR: In this article, a thermocouple is used to measure the sample temperature in a Stanton HT-D thermobalance, the bead of which is positioned in or near the sample, depending on crucible design.
Journal ArticleDOI
Thermal decomposition of metal nitrates and their hydrates
Jacob Mu,Daniel D. Perlmutter +1 more
TL;DR: In this article, the controlled decomposition of various metal nitrates and their common hydrates was carried out in a thermogravimetric analyzer, a differential scanning calorimeter, and a differential thermal analyzer.
Journal ArticleDOI
The thermal properties of inorganic compounds: I. Some mercury(I) and (II) compounds
TL;DR: In this article, the TG and DTA curves of the yellow and red forms of HgO and other halides are reported, and a lower initial procedural dissociation temperature, 400°C, was observed for the yellow form of hgO versus 460°C for the red form.
Journal ArticleDOI
Degradation studies on nickel nitrate hexahydrate: Part 2. evolved gas analysis
TL;DR: In this paper, the coordination chemistry of nickel, the rate of removal of water from the sample, and the ability of water vapour to hydrolyse the intermediate nickel nitrate dihydrate were investigated.
Journal ArticleDOI
Degradation studies on nickel nitrate hexahydrate. Part 1. Effect of experimental conditions
TL;DR: In this article, the effect of heat on nickel nitrate hexahydrate has been investigated in terms of variations in experimental conditions, such as sample size, heating rate and atmosphere.