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An experimental and numerical study on the volume change of particle-filled elastomers in various loading modes

TLDR
In this paper, the volumetric response between uniaxial tension and confined axial compression loading for commercial particle-filled hydrogenated nitrile butadiene rubber (HNBR) and fluoroelastomer (FKM) compounds was investigated.
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This article is published in Mechanics of Materials.The article was published on 2017-03-01 and is currently open access. It has received 17 citations till now. The article focuses on the topics: Hydrostatic stress & Tension (physics).

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Citations
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Journal ArticleDOI

Rate-dependent phase-field damage modeling of rubber and its experimental parameter identification

TL;DR: In this article, a rate-independent phase-field model for finite strains was proposed and three degradation functions were assessed for their accuracy to model the rubber's rate-dependent fracture, and an adaptive time-stepping approach with a corrector scheme was employed to increase the computational efficiency.
Journal ArticleDOI

Effect of microstructural damage on the mechanical properties of silica nanoparticle-reinforced silicone rubber composites

TL;DR: In this paper, the authors investigated the microscopic damage mechanism and its effect on the mechanical properties of silicone rubber-based composites reinforced by surface unmodified and modified nanoparticles, which is helpful not only for the understanding of mechanical performance of nanoparticle-reinforced flexible elastomer composites, but also for the design of novel flexible composites with matching strength and toughness.
Journal ArticleDOI

Stress-strain response and volume change of a highly filled rubbery composite: Experimental measurements and numerical simulations

TL;DR: In this paper, the authors measured the stress-strain response of a rubbery polymer network highly filled with micrometric glass beads, which was measured at low strain rate in uniaxial tension.
Journal ArticleDOI

Parameters estimation of generalized Maxwell model for SBR and carbon-filled SBR using a direct high-frequency DMA measurement system

TL;DR: In this article, a new high-frequency DMA (HFDMA) was proposed to fit Generalized Maxwell Model (GMM) equations through numerical optimization techniques, which is shown to be 5%−7% more accurate than the indirect measurement method at least for the SBR and SBR-CB.
Journal ArticleDOI

Resolving cavitation in silica-filled styrene-butadiene rubber composites upon cyclic tensile testing

TL;DR: In this article, 3D digital image correlation (3D-DIC) and micro-computed x-ray tomography (μCT) were employed with in-situ approaches.
References
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Proceedings ArticleDOI

A Combined Corner and Edge Detector

TL;DR: The problem the authors are addressing in Alvey Project MMI149 is that of using computer vision to understand the unconstrained 3D world, in which the viewed scenes will in general contain too wide a diversity of objects for topdown recognition techniques to work.
Journal ArticleDOI

scikit-image: Image processing in Python

TL;DR: The advantages of open source to achieve the goals of the scikit-image library are highlighted, and several real-world image processing applications that use scik it-image are showcased.
Journal ArticleDOI

A Theory of Large Elastic Deformation

TL;DR: In this paper, it was deduced that the general strain energy function, W, has the form W=G4 ∑ i=13(λi−1λi)2+H 4 ∑ t=13 (λi2−1 ε)2 + H 4, where the λi's are the principal stretches, G is the modulus of rigidity, and H is a new elastic constant not found in previous theories.
Journal ArticleDOI

Influence of voids on shear band instabilities under plane strain conditions

TL;DR: In this paper, the effect of microscopic voids on the failure mechanism of a ductile material is investigated by considering an elastic-plastic medium containing a boubly periodic array of circular cylindrical voids.
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Frequently Asked Questions (16)
Q1. What have the authors contributed in "An experimental and numerical study on the volume change of particle- lled elastomers in various loading modes" ?

Laboratory tests show that there is a pronounced di erence in the volumetric response between uniaxial tension and con ned axial compression loading for commercial particlelled hydrogenated nitrile butadiene rubber ( HNBR ) and uoroelastomer ( FKM ) compounds. To gain an increased understanding of the macroscopically obtained results, a tension in situ scanning electron microscopy study was performed. 

However, further studies on the e ect of particle geometry, size distribution, and interaction e ects should be carried out before de nitive conclusions can be drawn. 

The model was exposed to UT loading by applying the stress - time data obtained in the experimental tests to the upper boundary as a negative pressure force, while the vertical external boundary was free to move horizontally. 

For the in situ tension images, it was found that deforming the specimens changed the conductive properties of the compounds, reducing the image quality at large deformations. 

For the early research on the volumetric behaviour of elastomers, the most accessible method for measuring global volume changes accompanying deformation was through dilatometry tests [16, 17, 18, 19]. 

Prior to any deformation, images at 60, 100 and 300 times magni cation were obtained of the surface at both the centre and the edge of the specimen, resulting in six images for each compound. 

The largest particle found in the inspected regions had a projected area of 1125 m2, found at the edge of the FKM material, while the smallest particle possible to identify with this method at 60 magni cation had a projectedarea of 0.09 m2. 

For this purpose, a grey scale speckle pattern was applied to the specimens prior to testing, and two Prosilica GC2450 CCD cameras were used to capture frames of the wide and narrow surface of the specimen throughout the tests. 

These llers improve mechanical properties like sti ness and strength, but may also alter the volumetric behaviour of the compounds. 

Unit cell simulations are often used to explain globally observed results by studying mechanisms occurring at the scale of the material constituents. 

the fraction of internal voids is expected to be limited, due to the sti and elastic volume response observed in the CAC experiments. 

The stress needed to separate the two surfaces increases linearly with a sti ness k until an initiation stress Tini is reached (coinciding with the initiation deformation ini). 

Using DIC, Le Cam and Toussaint [20] looked at the competition between volume increase due to void growth and volume decrease due to crystallization in natural rubber loaded in tension. 

Due to the absolute lack of experimental data on the matrix-particle interface behaviour of the materials, the parameters of the base model were set to be Tini = 6 MPa, k = 6 GPa/ m, and Gc = 15 J/m 2, as this gave a reasonable representation of the experimental results. 

as already mentioned, the model is too simple to provide quantitatively precise results due to the lack of matrix cavitation, neglecting the particle size distribution, inaccurate modelling of the complex particle geometries, and the lack of particle interaction e ects. 

Some implications of this loading mode dependent volume behaviour for the constitutive modelling of particle- lled elastomers are discussed in the following section.