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Analysis and optimization of temperature distribution in carbon fiber reinforced composite materials during microwave curing process

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TLDR
In this paper, the influence of ply orientation and thickness on through-thickness temperature distribution of carbon fiber reinforced composite laminates was investigated in two different types of epoxy systems.
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This article is published in Journal of Materials Processing Technology.The article was published on 2014-03-01 and is currently open access. It has received 65 citations till now. The article focuses on the topics: Epoxy & Microwave.

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Citations
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Journal ArticleDOI

Rapid energy-efficient manufacturing of polymers and composites via frontal polymerization

TL;DR: Frontal polymerization of dicyclopentadiene is used to generate thermoset polymers and composite materials with much lower energy requirements and cure times than are needed in conventional oven or autoclave curing approaches.
Journal ArticleDOI

Accelerated microwave curing of fibre-reinforced thermoset polymer composites for structural applications: A review of scientific challenges

TL;DR: In this paper, the fundamental principles behind efficient accelerated curing of composites using microwave radiation heating are reviewed and presented, especially focusing on the relation between penetration depth, microwave frequency, dielectric properties and cure degree.
Journal ArticleDOI

In-situ curing of glass fiber reinforced polymer composites via resistive heating of carbon nanotube films

TL;DR: In this paper, a time and energy-saving out-of-oven curing process based on the resistive heating of a macroscale carbon nanotube (CNT) film made using the floating catalyst chemical vapor deposition method was reported.
Journal ArticleDOI

Aligned Carbon Nanotube Film Enables Thermally Induced State Transformations in Layered Polymeric Materials

TL;DR: Experimental results indicate that the use of an "out-of-oven" A-CNT integrated heater leads to orders of magnitude reductions in the energy required to process polymeric layered structures such as composites.
Journal ArticleDOI

Interfacial shear strength of microwave processed carbon fiber/epoxy composites characterized by an improved fiber-bundle pull-out test

TL;DR: In this paper, an improved fiber-bundle pull-out test was developed to solve the problem of severe arcing caused by exposed carbon fibers, which brought an increase of about 52.8% in interfacial shear strength.
References
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Journal ArticleDOI

Tooling design and microwave curing technologies for the manufacturing of fiber-reinforced polymer composites in aerospace applications

TL;DR: In this article, the authors report the problems in the fabrication of advanced composite materials identified through literature survey, and an investigation carried out by the authors about the composite manufacturing status in China's aerospace industry.
Journal ArticleDOI

Applications of fixed and variable frequency microwave (VFM) facilities in polymeric materials processing and joining

TL;DR: In this paper, the authors present a state-of-the-art review of microwave technologies, processing methods and industrial applications, using variable frequency microwave (VFM) facilities, geared towards advanced materials processing and chemical synthesis.
Journal ArticleDOI

Experimental studies on comparison of microwave curing and thermal curing of epoxy resins used for alternative mould materials

TL;DR: In this paper, three epoxy resins, namely R2512, R2515 and R2516, were used in combination with two hardeners H2403 and H2409 to study the glass transition temperature of alternative mold materials by using both microwave heating and conventional oven heating.
Journal ArticleDOI

Cure studies on bifunctional epoxy matrices using a domestic microwave oven

TL;DR: In this article, three types of bifunctional epoxyamine matrix systems (two room temperature (RT) cure types and one elevated temperature (ET) cure type), used for aerospace composite applications, were cured in a domestic microwave oven.
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Frequently Asked Questions (15)
Q1. What contributions have the authors mentioned in the paper "Analysis and optimization of temperature distribution in carbon fiber reinforced composite materials during microwave curing process" ?

Two different types of epoxy systems have been studied. The maximum temperature difference of the samples formed using themodified microwave curing technologies in this research could be reduced by 79 % to 2. 1 °C. 

Future studies will be carried out to identify the relationship between several physical mechanisms in microwave curing to get a better temperature distribution and establish the standard process specifications. 

The physical mechanism of microwave curing includes the natural heat convection of air inthe microwave oven, heat conduction inside the composite material and the directly heating action of microwave. 

Using the vacuum pressure technology and ceramic tooling, the composite samples achieved lower cost in manufacturing and better performance. 

Bogetti and Gillespie (1992) reported that the complex gradients of temperature in thickness direction of composite laminates may cause serious process-induced residual stress and deformation. 

Under the action of an electromagnetic field, the temperature at the surface of carbon fiberreinforced composites is lower than the target temperature, no matter for what kinds of composite laminates. 

Boey and Yap (2001) reported that microwave curing was more effective than conventional heating in enhancing the reaction rates during cross-linking by testing different curing agents in curing. 

The condition to be satisfied to get such a Bragg reflected wavelength is known as Bragg condition and is given by Grattan and Meggitt (1997) as: 2B nD (1) 

The thickness values of composite laminates are 4.5, 7.5 and 22.5mm, corresponding to sample #1, sample #2 and sample #3 respectively. 

The most important dwell stages were studied to analysis the temperature distribution influenced by ply orientation and thickness. 

A periodic perturbation of the refractive index can be formed along the fiber length through the change of reflection wavelength influenced by the physical or mechanical characteristics of the grating area. 

Based on the analysis, in order to uniform the temperature distribution of compositelaminates, different solutions need to be applied. 

For the above reason, alternative processing technologies, such as microwave curingtechnologies have been developed to form composite structures and provide a uniform temperature distribution. 

Considering the previous work, the 0.09Mpa vacuum pressure was provided when heating from 100 °C or 90 °C to the end of heat preservation. 

The composite laminates were laid up on a ceramic tooling coated with release agent and the edge areas were covered by sealant tapes.