(E)-3-[4-(Dimethyl-amino)-phen-yl]-1-(2-methyl-4-phenyl-quinolin-3-yl)prop-2-en-1-one 0.7-hydrate.
TLDR
In the title compound, C27H24N2O·0.7H2O, the quinoline ring system is approximately planar, with a maximum deviation of 0.011 (1) Å, and forms dihedral angles with the phenyl and benzene rings, respectively.Abstract:
In the title compound, C27H24N2O·0.7H2O, the quinoline ring system is approximately planar, with a maximum deviation of 0.011 (1) A, and forms dihedral angles of 74.70 (4) and 80.14 (4)° with the phenyl and benzene rings, respectively. In the crystal, the molecules are linked to the water molecules via intermolecular O—H⋯N hydrogen bonds and further stabilized by C—H⋯π interactions involving the centroid of the benzene ring of the quinoline group. This benzene ring is observed to form a π–π interaction with an adjacent pyridine ring [centroid–centroid distance = 3.7120 (6) A].read more
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Journal ArticleDOI
A short history of SHELX
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TL;DR: This paper reports on the current status of structure validation in chemical crystallography and describes the current state of research in this area.
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Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compounds
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A nitrogen‐gas‐stream cryostat for general X‐ray diffraction studies
J. Cosier,A. M. Glazer +1 more
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