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Influence of heat treatment on microstructure and tensile behavior of a hot isostatically pressed nickel-based superalloy

TLDR
In this article, a nickel-based superalloy powder RR1000 has been hot isostatically pressed (HIPed) and heat treated to produce different microstructures using a scanning electron microscope (SEM).
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This article is published in Journal of Alloys and Compounds.The article was published on 2013-11-25 and is currently open access. It has received 65 citations till now. The article focuses on the topics: Scanning electron microscope & Microstructure.

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Effect of hot isostatic pressing procedure on performance of Ti6Al4V: Surface qualities, microstructure and mechanical properties

TL;DR: In this paper, the effects of two different procedures (SL: simultaneous loading, AL: asynchronous loading) on the surface qualities, microstructure and mechanical properties of Ti6Al4V alloy part during hot isostatic pressing (HIP) were investigated.
Journal ArticleDOI

Effect of heat treatment on microstructure and mechanical properties of the hot-isostatic-pressed Inconel 718 powder compact

TL;DR: In this article, several heat treatments, including the solution plus aging with different solution temperature and the direct aging scheme, have been designed based on the phase relations of Inconel 718 and been employed for the optimization.
Journal ArticleDOI

Effect of pre-treatment on hot deformation behavior and processing map of an aged nickel-based superalloy

TL;DR: In this article, the effects of pre-treatment on the hot deformation behavior and processing maps of two pre-treated nickel-based superalloys are investigated over wide ranges of strain rate and temperature.
Journal ArticleDOI

On the strengthening and embrittlement mechanisms of an additively manufactured Nickel-base superalloy

TL;DR: In this paper, a microstructural hierarchy composed of weak texture, sub-micron cellular structures and dislocation cellular walls was promoted in the as-built sample, which provided an addition of 372 MPa in yield strength.
Journal ArticleDOI

The role of composition on the extent of individual strengthening mechanisms in polycrystalline Ni-based superalloys

TL;DR: In this article, the role of composition on each of the individual strengthening mechanisms was investigated for the commercial alloy RR1000, and it was found that composition plays a complex role on the yield strength due to the multifaceted effect of elemental phase partitioning.
References
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Deformation and Fracture Mechanics of Engineering Materials

TL;DR: In this article, the authors present an overview of fracture mechanics of engineering materials and examine the role of the transition temperature approach to fracture control in the engineering failure process, as well as various aspects of fracture toughness.
Journal ArticleDOI

Fundamental aspects of hot isostatic pressing: An overview

TL;DR: In this paper, the basic science of sintering and hipping is summarized and contrasted, and the current state of understanding and modeling of hipping can be classified either as microscopic or macroscopic in their approach.
Journal ArticleDOI

Strengthening Mechanisms in Polycrystalline Multimodal Nickel-Base Superalloys

TL;DR: In this paper, a model that considers solid-solution strengthening, Hall-Petch effects, precipitate shearing in the strong and weak pair-coupled modes, and dislocation bowing between precipitates has been developed and assessed.
Journal ArticleDOI

Practical applications of hotisostatic Pressing diagrams: Four case studies

TL;DR: In this paper, the construction of mechanism maps for hot-isostatic pressing is described, and a number of materials of commercial and scientific interest: tool steel, a superalloy, Al2O3, and ice.
Journal ArticleDOI

Microtwinning and other shearing mechanisms at intermediate temperatures in Ni-based superalloys

TL;DR: In this article, the nature of microtwins and the microtwinning dislocations at the atomic level have been determined using High Angle Annular Dark Field Scanning Transmission Electron Microscopy imaging.
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Q1. What are the contributions in "University of birmingham influence of heat treatment on microstructure and tensile behavior of a hot isostatically pressed nickel-based superalloy" ?

Tensile testing was performed at room temperature and 700oC and the deformed samples were examined using SEM and transmission electron microscope ( TEM ). Solution treatment below the γ′ solvus followed by air cooling resulted in the formation of finer cuboidal secondary γ′ ( 350nm-750nm ) and medium-sized spherical tertiary γ′ ( 100nm-200nm ). Ageing of the solution-treated or of the as-HIPed samples at 760°C resulted in the precipitation of a high population of fine γ′ ( around 50nm ) which further increased the strength. It is suggested that the optimum treatment of the powder superalloy is to solution-treat and age after HIPing ; this results in properties which are comparable with those of thermomechanically processed samples. 

Tensile deformation at 700℃ was mainly due to the formation of extended stacking faults across both γ and γ′. 

The need for jet engines to operate at higher temperatures to increase efficiency requires the development of nickel-based superalloys containing increased amount of the main strengthening elements such as Ti, Al, Mo, W, Ta and Hf. 

The flat fracture area could be due to plane strain conditions while the slant fracture part is because of plane stress conditions [24]. 

HIPing was carried out on stainless steel cans with a length of 180mm and an inner diameter of 45mm which after filling with powder, to a tap-density of between 60 and 65%, was outgassed and sealed by closing the evacuation tube by welding. 

directly HIPed nickel-based superalloy powder usually suffers from PPBs decorated with carbides, oxides or oxycarbides which are harmful to mechanical properties, especially the hot ductility, low cycle fatigue and stress rupture properties [10-14]. 

The dominant coarse and irregular-shaped primary and secondary γ′ precipitates in as-HIPed samples were replaced with a large volume fraction of finer cuboidal secondary γ′ and spherical tertiary γ′. 

Solution treatment at (S-40)°C (STA) plus ageing considerably decreased the volume fraction of secondary γ′ and changed the irregular-shaped γ′ in the as-HIPed samples into cuboidal or near-triangular morphology. 

increased alloying usually leads to extensive segregation in the cast ingots which results in significant reduction in their hot workability. 

Given that the thermally induced pores are mainly located at grain boundaries, they are believed to be formed due to boron-induced incipient melting at grain boundaries [18-19]. 

Solution treatment at 40°C below γ´ solvus together with ageing at 760°C completelytransformed the coarse and irregular-shaped γ′ in as-HIPed RR1000 samples into finer cuboidal secondary γ′ and medium-sized tertiary γ′. 

Some HIPed samples were solution-treated for 2h at (S-40)°C and S, respectively, after which the samples were air cooled (the cooling rate was measured to be around 105ºC/min). 

The powder used in this study is an argon-atomised nickel-based superalloy powder RR1000 which has a size range below 53µm in diameter. 

As compared with the room temperature fracture, fracture at 700℃ is more faceted and crystallographic which suggests that the deformation at elevated temperature is more planar, consistent with the above observation on deformation. 

The samples were polished and chemically etched in activated colloidal silica solution and cleaned in acetone and then examined using a JEOL 7000 FEG-SEM microscope to study the structural integrity. 

Some of the coarse precipitates present in the as-HIPed samples in fact remain after solution treatment because this temperature is below the γ′ solvus. 

Many of the stacking faults even extended across the γ channel into the adjacent tertiary γ′precipitates and formed complex arrays of faults. 

Net-shape HIPing [1-5] offers a possible solution to this high cost of producing components from powder since this would lead to the reduction in forging and machining operations and thus to considerable cost reduction. 

The TEM study of the deformed samples generally showed behavior very similar to that reported in many papers of deformed Ni superalloys, with shearing through and looping of dislocations around γ′ precipitates. 

The current study demonstrates that with proper processing conditions, desirable microstructure and mechanical properties for net-shape HIPed Ni-based superalloys could be achieved.• 

This is possible since the superalloy investigated in the present study was designed to produce a minimum value of stacking fault energy through maximum addition of Co to promote planar slip and to inhibit cross slip, which are beneficial for both crack growth rates and creep behaviour [22]. 

Ageing treatment generally shows no influence on primary and secondary γ′ in both as-HIPed and solution treated samples but seems to increase the population of fine tertiary γ′ (Fig.1 (d)).