Structure of the Precipitated Particles at the Third Stage of Tempering of Martensitic Iron-Carbon Steel Studied by High Resolution Electron Microscopy
TLDR
In this article, it was shown that the forbidden spots observed in electron diffraction patterns from the precipitates can reasonably be interpreted on the basis of the characteristic growth nature of the carbide phases.Abstract:
Application of the lattice and structure imaging techniques in electron microscopy has shown that θ-Fe3C and χ-Fe5C2 intergrow microsyntactically in the precipitated particles at the early third stage of martensite tempering (520~670K). Also is found the microsyntactic intergrowth of higher Carbides, θn-Fe2n+1Cn, having structures closely related With those of θ-Fe3C and χ-Fe5C2. All the forbidden spots observed in electron diffraction patterns from the precipitates can reasonably be interpreted on the basis of the characteristic growth nature of the carbide phases. At the later stage of tempering (720-870K), the precipitates are θ-Fe3C containing various kinds of planar defect. Amechanism is presented for the transformation from χ-Fe5C2 to θ-Fe3C.read more
Citations
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Crystallographic Study of the Tempering of Martensitic Carbon Steel by Electron Microscopy and Diffraction
TL;DR: In this article, the structural changes taking place during the tempering proceed in four stages, starting at 370 K, where interstitial carbon atom clusters are formed below 270 K, rearrange to make a modulated structure between 270 and 360 K, and disappear at about 370 K.
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Precipitation of paraequilibrium cementite: Experiments, and thermodynamic and kinetic modeling
Gautam Ghosh,Gregory B. Olson +1 more
TL;DR: In this article, the precipitation of paraequilibrum cementite prior to the strengthening M2C phase is investigated using two model ultra-high strength (UHS) steels.
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Atomic and nanoscale chemical and structural changes in quenched and tempered 4340 steel
Amy J. Clarke,Michael K Miller,Robert D. Field,Robert D. Field,D.R. Coughlin,Paul J. Gibbs,Kester D. Clarke,David Alexander,K.A. Powers,Pallas A. Papin,G. Krauss +10 more
TL;DR: In this article, atom probe tomography and transmission electron microscopy (TEM) have been used to determine the location and distribution of carbon and alloying elements associated with the complex structural changes that occur at the atomic and nanoscale in 4340 steel after quenching to martensite and tempering at 325, 450 or 575°C.
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Annealing behaviour of nanostructured carbon steel produced by severe plastic deformation
TL;DR: In this article, the influence of annealing on the structure, phase composition and microhardness of carbon steel produced by high pressure torsion (HPT) was examined, showing that the material which is far from thermodynamic equilibrium exhibits enhanced thermal stability and a more sluggish mechanical softening than conventional martensite obtained by quenching from elevated temperatures.
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Epsilon carbide precipitation during tempering of plain carbon martensite
Yasuya Ohmori,I. Tamura +1 more
TL;DR: In this paper, the first stage of tempering initiates with the nucleation of very fine e-carbide particles on the closely spaced parallel line defects, the morphology being so-called cross-hatched e-carbide needles.
References
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Crystal structure and morphology of the carbide precipitated from martensitic high carbon steel during the first stage of tempering
Y Hirotsu,S. Nagakura +1 more
TL;DR: A martensitic steel containing 1.13 wt. %C was tempered at 120°C for 1-100 days and the structure and morphology of precipitated carbide were studied by electron microscopy and selected area diffraction as discussed by the authors.
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Nature of χ-Carbide and Its Possible Occurrence in Steels
K. H. Jack,S. Wild +1 more
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A new iron carbide in hydrocarbon synthesis catalysts
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