scispace - formally typeset
Search or ask a question

Showing papers in "Review of Scientific Instruments in 2022"


Journal ArticleDOI
TL;DR: In this paper , the authors investigated the correlation between the vertical profile of beam intensity and the vertical profiles of plasma properties at the extraction region of the source, focusing on the influence of increasing cesium injection.
Abstract: Giant negative ion sources for neutral beam injectors deliver huge negative ion currents, thanks to their multi-beamlet configuration. As the single-beamlet optics defines the transmission losses along the beamline, the extraction of a similar current for all beamlets is extremely desirable, in order to facilitate the beam source operation (i.e., around perveance match). This Review investigates the correlation between the vertical profile of beam intensity and the vertical profiles of plasma properties at the extraction region of the source, focusing on the influence of increasing cesium injection. Only by the combined use of all available source diagnostics, described in this Review, can beam features on the scale of the non-uniformities be investigated with a sufficient space resolution. At RF power of 50 kW/driver, with intermediate bias currents and a filter field of 2.4 mT, it is found that the central part of the four vertical beam segments exhibits comparable plasma density and beamlet currents; at the edges of the central segments, both the beam and electron density appear to decrease (probably maintaining fixed electron-to-ion ratio); at the bottom of the source, an increase of cesium injection can compensate for the vertical drifts that cause a much higher presence of electrons and a lower amount of negative ions.

25 citations


Journal ArticleDOI
TL;DR: In this article , a low-noise low-voltage neural recording amplifier suitable for amplifying local field potentials and extracellular action potentials has been proposed to meet the end requirement of implantable neuro-medical system.
Abstract: Design of amplifier circuits with low-noise operable at low-power to be used, especially for implantable neural interfaces, remains a huge challenge. This research paper presents the design of a low-noise low-voltage neural recording amplifier suitable for amplifying local field potentials and extracellular action potentials so as to meet the end requirement of an implantable neuro-medical system. Critical performance parameters of the smaller circuit blocks of the complete neural amplifier architecture have been found with the help of detailed mathematical analysis and then verified by the simulations conducted using 0.18 µm 4M1P foundry Semi-conductor Laboratory N-well process. The neural amplifier design proposed in this paper passes neural signal of interest with a mid-band gain of 49.9 dB over a bandwidth of 5.3 Hz-8.6 kHz, draws only 11.5 µW of power from ±0.9 V supply voltage, and exhibits an input-referred noise of 2.6 µVrms with a noise efficiency factor of 2.27. The area consumed by the proposed neural amplifier architecture is 0.192 mm2. The complete circuit design carried out in this paper should prove to be useful in equipment for the diagnosis of neurological disorders.

17 citations


Journal ArticleDOI
TL;DR: In this paper , a micro-angle-resolved photoemission spectroscopy (ARPES) system was developed based on the synchrotron radiation beam focused with a Kirkpatrick-Baez mirror optics.
Abstract: Angle-resolved photoemission spectroscopy using a micro-focused beam spot [micro-angle-resolved photoemission spectroscopy (ARPES)] is becoming a powerful tool to elucidate key electronic states of exotic quantum materials. We have developed a versatile micro-ARPES system based on the synchrotron radiation beam focused with a Kirkpatrick-Baez mirror optics. The mirrors are monolithically installed on a stage, which is driven with five-axis motion, and are vibrationally separated from the ARPES measurement system. Spatial mapping of the Au photolithography pattern on Si signifies the beam spot size of 10 µm (horizontal) × 12 µm (vertical) at the sample position, which is well suited to resolve the fine structure in local electronic states. Utilization of the micro-beam and the high precision sample motion system enables the accurate spatially resolved band-structure mapping, as demonstrated by the observation of a small band anomaly associated with tiny sample bending near the edge of a cleaved topological insulator single crystal.

16 citations


Journal ArticleDOI
TL;DR: In this paper , the structural performance and research status of PWEHs based on different mechanisms, such as a rotating turbine, vortex-induced vibration, flutter, and galloping, are analyzed and summarized.
Abstract: Wireless sensor networks play a very important role in environmental monitoring, structural health monitoring, smart city construction, smart grid, and ecological agriculture. The wireless sensor nodes powered by a battery have a limited service life and need periodic maintenance due to the limitation of battery capacity. Fortunately, the development of environmental energy harvesting technology provides an effective way to eliminate the needs and the replacement of the batteries. Among the environmental stray energy, wind energy is rich, almost endless, widely distributed, and clean. Due to the advantages of simple structure, miniaturization, and high power density, wind energy harvesters using piezoelectric materials (PWEHs) have attracted much attention. By the ways of principal exploration, structure design, and performance optimization, great and steady progress has been made in the research of PWEH. This Review is focused on the review of PWEHs. After introducing the basic principle of PWEHs, the structural performance and research status of PWEHs based on different mechanisms, such as a rotating turbine, vortex-induced vibration, flutter, and galloping, are analyzed and summarized. Finally, the development trend of PWEHs has been prospected.

14 citations


Journal ArticleDOI
TL;DR: In this paper , the main microwave diagnostic techniques and tools adopted in electron cyclotron resonance (ECR) (and others) ion source laboratories, with a special focus on techniques and instruments developed at INFN-LNS, are reviewed.
Abstract: This paper reviews the main microwave diagnostic techniques and tools adopted in electron cyclotron resonance (ECR) (and others) ion source laboratories, with a special focus on techniques and instruments developed at INFN-LNS. Along with the tools used for optimization of microwave launching (power monitors, spectral analysis, and network analyzers), this paper deals, in particular, with more recent devices on-purpose developed to perform in-plasma analysis, such as absolute density measurements and density profiles retrieval. Among these, the first example of microwave interferometry for ECR compact machines (the VESPRI interferometer at INFN-LNS) will be briefly discussed, in combination with microwave polarimetric techniques based on Faraday rotation detection. More sophisticated microwave techniques are going to be designed and are now at a numerical study stage, e.g., profilometry and imaging via inverse scattering methods (this paper will offer short theoretical bases and first numerical results on 1D profilometry). In the end, the relevance about the implications and interplays of microwave techniques in multidiagnostic systems (microwave, optical, and x-ray domains) will be commented, with a special focus on time resolved microwave measurements and advanced signal processing via wavelet transform, useful for characterization of plasma instabilities.

12 citations


Journal ArticleDOI
TL;DR: In this paper , the authors present recent developments in cold-atom sensor miniaturization, focusing on key components that enable laser cooling on the chip-scale, and discuss the design, fabrication, and impact of the components on sensor scalability and performance.
Abstract: Laser cooled atoms have proven transformative for precision metrology, playing a pivotal role in state-of-the-art clocks and interferometers and having the potential to provide a step-change in our modern technological capabilities. To successfully explore their full potential, laser cooling platforms must be translated from the laboratory environment and into portable, compact quantum sensors for deployment in practical applications. This transition requires the amalgamation of a wide range of components and expertise if an unambiguously chip-scale cold atom sensor is to be realized. We present recent developments in cold-atom sensor miniaturization, focusing on key components that enable laser cooling on the chip-scale. The design, fabrication, and impact of the components on sensor scalability and performance will be discussed with an outlook to the next generation of chip-scale cold atom devices.

11 citations


Journal ArticleDOI
TL;DR: In this article , the authors present a measurement setup utilizing a single Josephson junction on a cantilever for high-resolution spatial measurements of spectroscopically resolved THz and microwave field distributions.
Abstract: Superconducting Josephson junctions have a wide range of applications ranging from quantum computing to voltage standards, and they may also be employed as versatile sensors for high-frequency radiation and magnetic fields. In this work, we present a unique measurement setup utilizing a single Josephson junction on a cantilever for high-resolution spatial measurements of spectroscopically resolved THz and microwave field distributions. This THz microscope can be utilized to measure power and frequency of electromagnetic radiation from ∼1 GHz to 5 THz. It may also be used to measure static magnetic fields and provide topological scans of samples. The samples can be both actively radiating or passively irradiated at either room temperature or cryogenic temperatures. We review the measurement setup of the THz microscope and describe the evaluation of its measurement data to achieve three-dimensional visualizations of the field distributions. The diverse capabilities of this unique tool are demonstrated by its different measurement modes with measurements of field distributions at 20 GHz and 1.4 THz, spectroscopically resolved THz measurements, and magnetic field measurements.

10 citations


Journal ArticleDOI
TL;DR: In this paper , the authors presented an ultrafast piezoelectric Z-scanner with a resonance frequency above 1.1 MHz, achieving a record response time of ∼0.14 µs, approximately twice as fast as conventional Z-scanners.
Abstract: The Z-scanner is the major component limiting the speed performance of all current high-speed atomic force microscopy systems. Here, we present an ultrafast piezoelectric Z-scanner with a resonance frequency above 1.1 MHz, achieving a record response time of ∼0.14 µs, approximately twice as fast as conventional piezoelectric-based Z-scanners. In the mechanical design, a small piezo-stack is supported at its bottom four vertices on a cone-like hollow, allowing the resonance frequency of the Z-scanner to remain as high as that of the piezo in free vibration. Its maximum displacement, ∼190 nm at 50 V, is large enough for imaging bio-molecules. For imaging bio-molecules in a buffer solution, the upper half of the Z-scanner is wrapped in a thin film resistant to water and chemicals, providing an excellent waterproof and mechanical durability without lowering the resonance frequency. We demonstrate that this Z-scanner can observe actin filaments, fragile biological polymers, for more than five times longer than the conventional Z-scanner at a tip velocity of 800 µm/s.

10 citations


Journal ArticleDOI
TL;DR: In this article , the effect of hydration on photoelectron circular dichroism (PECD) was explored using a micro-jet and the EASI (Electronic structure from Aqueous Solutions and Interfaces) setup.
Abstract: We present a unique experimental design that enables the measurement of photoelectron circular dichroism (PECD) from chiral molecules in aqueous solution. The effect is revealed from the intensity difference of photoelectron emission into a backward-scattering angle relative to the photon propagation direction when ionizing with circularly polarized light of different helicity. This leads to asymmetries (normalized intensity differences) that depend on the handedness of the chiral sample and exceed the ones in conventional dichroic mechanisms by orders of magnitude. The asymmetry is largest for photon energies within several electron volts above the ionization threshold. A primary aim is to explore the effect of hydration on PECD. The modular and flexible design of our experimental setup EASI (Electronic structure from Aqueous Solutions and Interfaces) also allows for detection of more common photoelectron angular distributions (PADs), requiring distinctively different detection geometries, and typically using linearly polarized light. A microjet is used for liquid-sample delivery. We describe EASI's technical features and present two selected experimental results, one based on synchrotron-light measurements and the other performed in the laboratory, using monochromatized He-II $\alpha$ radiation. The former demonstrates the principal effectiveness of PECD detection, illustrated for prototypic gas-phase fenchone. We also discuss the first data from liquid fenchone. In the second example we present valence photoelectron spectra from liquid water and NaI aqueous solution, here obtained from a planar-surface microjet (flatjet). This new development features a more favorable symmetry for angle-dependent photoelectron measurements.

10 citations


Journal ArticleDOI
TL;DR: The Quantum Instrumentation Control Kit (QICK) as mentioned in this paper is an Xilinx RF System-on-Chip (RFSoC)-based qubit controller that supports the direct synthesis of control pulses with carrier frequencies of up to 6 GHz.
Abstract: We introduce a Xilinx RF System-on-Chip (RFSoC)-based qubit controller (called the Quantum Instrumentation Control Kit, or QICK for short), which supports the direct synthesis of control pulses with carrier frequencies of up to 6 GHz. The QICK can control multiple qubits or other quantum devices. The QICK consists of a digital board hosting an RFSoC field-programmable gate array, custom firmware, and software and an optional companion custom-designed analog front-end board. We characterize the analog performance of the system as well as its digital latency, important for quantum error correction and feedback protocols. We benchmark the controller by performing standard characterizations of a transmon qubit. We achieve an average gate fidelity of Favg=99.93%. All of the schematics, firmware, and software are open-source.

10 citations


Journal ArticleDOI
TL;DR: In this article , a TPX3CAM was used for three-dimensional velocity map imaging of low energy electrons using a constant fraction discriminator and fast time to digital converter for the time information.
Abstract: We demonstrate three-dimensional velocity map imaging of low energy electrons using a TPX3CAM, where the three-dimensional momentum information [px, py, pz] is encoded in position and timing [x, y, t] of hits on the camera sensor. We make use of the camera sensor for the [x, y] information and a constant fraction discriminator and fast time to digital converter in the camera for the time information. We illustrate the capabilities of our apparatus by presenting above threshold ionization measurements of xenon, which produces well defined structures in the momentum resolved photoelectron yield.

Journal ArticleDOI
TL;DR: In this article , a flipped source follower (EFSF) LPF was proposed for the detection of electroencephalography (EEG) signals, which can achieve high power efficiency in future low-voltage and low-power biological systems.
Abstract: Owing to the impact of process voltage and temperature variations, the design of low-power low-pass filters (LPFs) with improved linearity is still one of the most challenging tasks for effective biological signal processing. This paper presents the design of a fourth-order Class-AB enhanced flipped source follower (EFSF) LPF circuit aimed at the detection of electroencephalography signals. The simulated results attained using complementary metal-oxide-semiconductor 180 nm technology node in Cadence Analog Design Environment demonstrate that the EFSF LPF emulates a DC-gain of -88 mdB with a bandwidth of 100 Hz and consumes 0.342 nW power from a supply voltage of 0.5 V. The calculated figure of merit for the proposed filter is 5.983 × 10-15 J with a dynamic range (DR) of 43.54 dB and input-referred noise of 91 µVrms. It consumes an area of 0.0458 mm2. To check the robustness of the proposed filter circuit, we performed Monte Carlo simulations with 200 runs. The statistical results achieved for the DC-gain, DR, and total harmonic distortion of the proposed filter show mean values of -188.09 mdB, 43.10 dB, and -41.85 dB along with standard deviation values of 285.21 mdB, 718.72 mdB, and 4.52 dB, respectively. The proposed Class-AB EFSF LPF can be used to achieve high power efficiency in future low-voltage and low-power biological systems.

Journal ArticleDOI
TL;DR: In this paper , the authors describe a conceptual design of a broadband inverted-geometry neutron spectrometer for the Second Target Station at the Spallation Neutron Source operated by Oak Ridge National Laboratory.
Abstract: BWAVES is an acronym for Broadband Wide-Angle VElocity Selector spectrometer, indicating that a novel WAVES (Wide-Angle VElocity Selector) device will be used to select the velocity/wavelength of the detected neutrons after they are scattered by the sample. We describe a conceptual design of BWAVES, a time-of-flight broadband inverted-geometry neutron spectrometer for the Second Target Station at the Spallation Neutron Source operated by Oak Ridge National Laboratory. Being the first inverted geometry spectrometer where the energy of the detected neutrons can be chosen by a WAVES device mechanically, irrespective of the limitations imposed by the crystal analyzers or filters, BWAVES will feature a uniquely broad, continuous dynamic range of measurable energy transfers, spanning 4.5 decades. This will enable measurements of both vibrational and relaxational excitations within the same, continuous scattering spectra. Novel approaches that are necessary for the implementation of a WAVES device at the BWAVES spectrometer will result in a spectrometer with the design and characteristics much different from those displayed by the neutron spectrometers in existence today.

Journal ArticleDOI
TL;DR: In this paper , the authors demonstrate the design and performance of a home-built ESR-STM capable of ESR at temperatures ranging from 1 to 10 K. The STM is incorporated with a homebuilt Joule-Thomson refrigerator and a two-axis vector magnet, which allows the deposition of atoms and molecules directly into the cold STM, eliminating the need to extract the sample for deposition.
Abstract: Recent advances in improving the spectroscopic energy resolution in scanning tunneling microscopy (STM) have been achieved by integrating electron spin resonance (ESR) with STM. Here, we demonstrate the design and performance of a homebuilt STM capable of ESR at temperatures ranging from 1 to 10 K. The STM is incorporated with a homebuilt Joule-Thomson refrigerator and a two-axis vector magnet. Our STM design allows for the deposition of atoms and molecules directly into the cold STM, eliminating the need to extract the sample for deposition. In addition, we adopt two methods to apply radio-frequency (RF) voltages to the tunnel junction: the early design of wiring to the STM tip directly and a more recent idea to use an RF antenna. Direct comparisons of ESR results measured using the two methods and simulations of electric field distribution around the tunnel junction show that, despite their different designs and capacitive coupling to the tunnel junction, there is no discernible difference in the driving and detection of ESR. Furthermore, at a magnetic field of ∼1.6 T, we observe ESR signals (near 40 GHz) sustained up to 10 K, which is the highest temperature for ESR-STM measurement reported to date, to the best of our knowledge. Although the ESR intensity exponentially decreases with increasing temperature, our ESR-STM system with low noise at the tunnel junction allows us to measure weak ESR signals with intensities of a few fA. Our new design of an ESR-STM system, which is operational in a large frequency and temperature range, can broaden the use of ESR spectroscopy in STM and enable the simple modification of existing STM systems, which will hopefully accelerate a generalized use of ESR-STM.

Journal ArticleDOI
TL;DR: In this article , a portable radio-frequency optically pumped magnetometer (RF OPM) working in unshielded conditions with sub-pT/Hz magnetic field sensitivity when used for the detection of small oscillating magnetic fields was developed.
Abstract: Electrically conductive objects can be detected using the principle of electromagnetic induction, where a primary oscillating magnetic field induces eddy currents in the object, which in turn produce a secondary magnetic field that can be measured with a magnetometer. We have developed a portable radio-frequency optically pumped magnetometer (RF OPM) working in unshielded conditions with sub-pT/Hz magnetic field sensitivity when used for the detection of small oscillating magnetic fields, setting a new benchmark for the sensitivity of a portable RF OPM in unshielded conditions. Using this OPM, we have detected the induced magnetic field from aluminum disks with diameters as small as 1.5 cm and with the disks being ∼25 cm from both the excitation coil and the magnetometer. When used for eddy current detection, our magnetometer achieves a sensitivity of a 2-6 pT/Hz. We have also detected a moving aluminum disk using our RF OPM and analyzed the magnetometer signals, which depend on the position of the disk, illustrating the potential of high sensitivity RF OPMs for remote sensing applications.

Journal ArticleDOI
TL;DR: In this paper , the authors describe an instrument for spectroscopically characterizing charged molecular clusters that have been selected according to both their isomeric form and their mass-to-charge ratio.
Abstract: Infrared and electronic spectra are indispensable for understanding the structural and energetic properties of charged molecules and clusters in the gas phase. However, the presence of isomers can potentially complicate the interpretation of spectra, even if the target molecules or clusters are mass-selected beforehand. Here, we describe an instrument for spectroscopically characterizing charged molecular clusters that have been selected according to both their isomeric form and their mass-to-charge ratio. Cluster ions generated by laser ablation of a solid sample are selected according to their collision cross sections with helium buffer gas using a drift tube ion mobility spectrometer and their mass-to-charge ratio using a quadrupole mass filter. The mobility- and mass-selected target ions are introduced into a cryogenically cooled, three-dimensional quadrupole ion trap where they are thermalized through inelastic collisions with an inert buffer gas (He or He/N2 mixture). Spectra of the molecular ions are obtained by tagging them with inert atoms or molecules (Ne and N2), which are dislodged following resonant excitation of an electronic transition, or by photodissociating the cluster itself following absorption of one or more photons. An electronic spectrum is generated by monitoring the charged photofragment yield as a function of wavelength. The capacity of the instrument is illustrated with the resonance-enhanced photodissociation action spectra of carbon clusters (Cn +) and polyacetylene cations (HC2nH+) that have been selected according to the mass-to-charge ratio and collision cross section with He buffer gas and of mass-selected Au2 + and Au2Ag+ clusters.

Journal ArticleDOI
TL;DR: In this article , the authors evaluate the optimization potential in terms of RF power losses and the RF power transfer efficiency of H-Ion sources for fusion plasmas, and propose a best-practice approach to achieve with low-risk effort an optimized ion source design in order to reduce losses and hence increase reliability.
Abstract: Radio frequency (RF) driven H- ion sources are operated at very high power levels of up 100 kW in order to achieve the desired performance. For the experimental setup, these are demanding conditions possibly limiting the source reliability. Therefore, assessing the optimization potential in terms of RF power losses and the RF power transfer efficiency η to the plasma has moved to the focus of both experimental and numerical modeling investigations at particle accelerator and neutral beam heating sources for fusion plasmas. It has been demonstrated that, e.g., at typical neutral beam injection ion source setups, about half of the RF power provided by the generator is lost in the RF coil and the Faraday shield due to Joule heating or via eddy currents. In a best practice approach, it is exemplarily demonstrated at the ITER RF prototype ion source how experimental evaluation accompanied by numerical modeling of the ion source can be used to improve η. Individual optimization measures regarding the Faraday shield, the RF coil, the discharge geometry, the RF driving frequency, and the application of ferrites are discussed, which could reduce the losses by a factor of two. The provided examples are intended as exemplary guidelines, which can be applied at other setups in order to achieve with low-risk effort an optimized ion source design in terms of reduced losses and hence increased reliability.

Journal ArticleDOI
TL;DR: In this paper , a holoscope axion search with a frequency-tunable cavity detector with a volume V = 0.234liter in a magnetic field B0 = 8.T was reported.
Abstract: We report on a holoscope axion search experiment near 19.6 µeV from the Taiwan Axion Search Experiment with Haloscope collaboration. This experiment is carried out via a frequency-tunable cavity detector with a volume V = 0.234 liter in a magnetic field B0 = 8 T. With a signal receiver that has a system noise temperature Tsys ≅ 2.2 K and an experiment time of about one month, the search excludes values of the axion-photon coupling constant gaγγ ≳ 8.1 × 10-14 GeV-1, a factor of 11 above the Kim-Shifman-Vainshtein-Zakharov benchmark model, at the 95% confidence level in the mass range of 19.4687-19.8436 µeV. We present the experimental setup and procedures to accomplish this search.

Journal ArticleDOI
TL;DR: A tunable probe photon energy is generated by the fourth harmonic generation of a tunable wavelength femtosecond laser source by combining a β-BaB2O4 crystal and a KBe2BO3F2 crystal as mentioned in this paper .
Abstract: Time- and angle-resolved photoemission spectroscopy (TrARPES) is a powerful technique for capturing the ultrafast dynamics of charge carriers and revealing photo-induced phase transitions in quantum materials. However, the lack of widely tunable probe photon energy, which is critical for accessing the dispersions at different out-of-plane momentum kz in TrARPES measurements, has hindered the ultrafast dynamics investigation of 3D quantum materials, such as Dirac or Weyl semimetals. Here, we report the development of a TrARPES system with a highly tunable probe photon energy from 5.3 to 7.0 eV. The tunable probe photon energy is generated by the fourth harmonic generation of a tunable wavelength femtosecond laser source by combining a β-BaB2O4 crystal and a KBe2BO3F2 crystal. A high energy resolution of 29-48 meV and time resolution of 280-320 fs are demonstrated on 3D topological materials ZrTe5 and Sb2Te3. Our work opens up new opportunities for exploring ultrafast dynamics in 3D quantum materials.

Journal ArticleDOI
TL;DR: The CHESS as discussed by the authors is a planned direct geometry neutron chopper spectrometer designed to detect and analyze weak signals intrinsic to small cross sections (e.g., small mass, small magnetic moments, or neutron absorbing materials) in powders, liquids, and crystals.
Abstract: CHESS, chopper spectrometer examining small samples, is a planned direct geometry neutron chopper spectrometer designed to detect and analyze weak signals intrinsic to small cross sections (e.g., small mass, small magnetic moments, or neutron absorbing materials) in powders, liquids, and crystals. CHESS is optimized to enable transformative investigations of quantum materials, spin liquids, thermoelectrics, battery materials, and liquids. The broad dynamic range of the instrument is also well suited to study relaxation processes and excitations in soft and biological matter. The 15 Hz repetition rate of the Second Target Station at the Spallation Neutron Source enables the use of multiple incident energies within a single source pulse, greatly expanding the information gained in a single measurement. Furthermore, the high flux grants an enhanced capability for polarization analysis. This enables the separation of nuclear from magnetic scattering or coherent from incoherent scattering in hydrogenous materials over a large range of energy and momentum transfer. This paper presents optimizations and technical solutions to address the key requirements envisioned in the science case and the anticipated uses of this instrument.

Journal ArticleDOI
TL;DR: In this article , a novel structured low-rank (SLR) decomposition-based magnetic anomaly detection (MAD) method was proposed to improve the performance of MAD with a low SNR.
Abstract: The magnetic anomalies generated by the ferromagnetic targets are usually buried within uncontrollable interference sources, such as the power frequency and random noises. In particular, the variability of the geomagnetic field and the low signal-to-noise ratio (SNR) of the magnetic anomalies cannot be avoided. In this paper, to improve the performance of magnetic anomaly detection (MAD) with a low SNR, we propose a novel structured low-rank (SLR) decomposition-based MAD method. In addition, a new framework based on the SLR and singular value decomposition (SVD) is constructed, dubbed SLR-SVD, and the corresponding working principle and implemented strategy are elaborated. Through comparing the SLR-SVD with two state-of-the-art methods, including principal component analysis and SVD, the results demonstrate that the proposed SLR-SVD can not only suppress the noise sufficiently, i.e., improving 55.26% approximately of the SNR, but also retain more boundary information of magnetic anomalies, i.e., decreasing approximately 68.05% of the mean squared error and improving approximately 28.47% of the structural similarity index.

Journal ArticleDOI
TL;DR: In this article , an ambient pressure cell is described for conducting synchrotron-based x-ray photoelectron spectroscopy (XPS) measurements during atomic layer deposition (ALD) processes.
Abstract: An ambient pressure cell is described for conducting synchrotron-based x-ray photoelectron spectroscopy (XPS) measurements during atomic layer deposition (ALD) processes. The instrument is capable of true in situ and operando experiments in which it is possible to directly obtain elemental and chemical information from the sample surface using XPS as the deposition process is ongoing. The setup is based on the ambient pressure XPS technique, in which sample environments with high pressure (several mbar) can be created without compromising the ultrahigh vacuum requirements needed for the operation of the spectrometer and the synchrotron beamline. The setup is intended for chemical characterization of the surface intermediates during the initial stages of the deposition processes. The SPECIES beamline and the ALD cell provide a unique experimental platform for obtaining new information on the surface chemistry during ALD half-cycles at high temporal resolution. Such information is valuable for understanding the ALD reaction mechanisms and crucial in further developing and improving ALD processes. We demonstrate the capabilities of the setup by studying the deposition of TiO2 on a SiO2 surface by using titanium(IV) tetraisopropoxide and water as precursors. Multiple core levels and the valence band of the substrate surface were followed during the film deposition using ambient pressure XPS.

Journal ArticleDOI
TL;DR: In this article , the benefits and challenges associated with micro-resonator use for EPR spectroscopy are discussed and a conceptual foundation for analysis of resonator sensitivity is presented.
Abstract: Electron paramagnetic resonance (EPR) spectroscopy characterizes the magnetic properties of paramagnetic materials at the atomic and molecular levels. Resonators are an enabling technology of EPR spectroscopy. Microresonators, which are miniaturized versions of resonators, have advanced inductive-detection EPR spectroscopy of mass-limited samples. Here, we provide our perspective of the benefits and challenges associated with microresonator use for EPR spectroscopy. To begin, we classify the application space for microresonators and present the conceptual foundation for analysis of resonator sensitivity. We summarize previous work and provide insight into the design and fabrication of microresonators as well as detail the requirements and challenges that arise in incorporating microresonators into EPR spectrometer systems. Finally, we provide our perspective on current challenges and prospective fruitful directions.

Journal ArticleDOI
TL;DR: In this article , the authors provide a formal description of ultrafast disruptive probing, a method in which the probe pulse disrupts a transient species that may be a metastable ion or a transient state of matter.
Abstract: Ultrafast science depends on different implementations of the well-known pump-probe method. Here, we provide a formal description of ultrafast disruptive probing, a method in which the probe pulse disrupts a transient species that may be a metastable ion or a transient state of matter. Disruptive probing has the advantage of allowing for simultaneous tracking of the yield of tens of different processes. Our presentation includes a numerical model and experimental data on multiple products resulting from the strong-field ionization of two different molecules, partially deuterated methanol and norbornene. The correlated enhancement and depletion signals between all the different fragmentation channels offer comprehensive information on photochemical reaction pathways. In combination with ion imaging and/or coincidence momentum imaging or as complementary to atom-specific probing or ultrafast diffraction methods, disruptive probing is a particularly powerful tool for the study of strong-field laser-matter interactions.

Journal ArticleDOI
TL;DR: In this paper , the authors proposed a self-terminating charge neutralization using two neutralization electron guns to automatically measure the total electron emission yield (TEEY) of insulators.
Abstract: For insulators, the accumulated charge on the surface after electron bombardment will interfere with the total electron emission yield (TEEY) measurement. This work develops a novel method to automatically measure the TEEY of insulators based on self-terminating charge neutralization using two neutralization electron guns. We perform theoretical analysis and experimental design for the neutralization of positive and negative charges. Positive charges are neutralized by an electron gun whose cathode is equipotential to the sample. Negative charges are neutralized by another electron gun whose cathode is adjusted to a negative potential with respect to the grounded sample, which is set between EP1/e and EP2/e. We test the control and stability performance of the TEEY measurement system based on the timing design of the electron gun switching and believe that it meets the TEEY measurement requirements. The TEEY measurements of glass, Si, and SiO2 are in good agreement with the data reported in the references, which validates the accuracy of our method in this work. We anticipate that our method provides an essential reference for the rapid TEEY measurements of insulators.

Journal ArticleDOI
TL;DR: In this paper , a high heat flux ball-pen probe head installed on the midplane manipulator is used in ASDEX-Upgrade (AUG) to measure several plasma parameters simultaneously and with high temporal resolution.
Abstract: A new high heat flux ball-pen probe head installed on the midplane manipulator is currently being used in ASDEX-Upgrade (AUG). The probe was designed to withstand high heat fluxes making possible the investigation of the plasma edge under harsh conditions, such as low power H-mode. Composed of seven pins (four Langmuir probes, mounted in two Mach probe pairs, and three ball-pen probes), the new probe head allows us to measure several plasma parameters simultaneously and with high temporal resolution. A novel method to correct the sheath potential dynamically accounting for the total secondary electron emission is introduced together with applications to obtain the electron temperature and plasma potential profiles. The total secondary electron emission yield is obtained from particle in cell simulations in AUG condition and probe realistic impact angle with respect to the magnetic field. Finally, the probe capability to investigate turbulence around the separatrix of AUG is discussed.

Journal ArticleDOI
TL;DR: Linien is a user-friendly and versatile tool for laser frequency stabilization that is capable of autonomously optimizing spectroscopy parameters by means of machine learning and can measure the error signal's power spectral density.
Abstract: We present a user-friendly and versatile tool for laser frequency stabilization. Its main focus is spectroscopy locking, but the software is suitable for lock-in techniques in general as well as bare proportional-integral-derivative (PID) operation. Besides allowing for sinusoidal modulation (up to 50 MHz), triangular ramp scanning, in-phase and quadrature demodulation (1-5 f), infinite impulse response, and PID filtering, Linien features two different algorithms for automatic lock point selection; one of them performs time-critical tasks completely on field-programmable gate arrays. Linien is capable of autonomously optimizing spectroscopy parameters by means of machine learning and can measure the error signal's power spectral density. The software is built in a modular way, providing both a graphical user interface as well as a Python scripting interface. It is based on the RedPitaya STEMLab platform but may be ported to different systems.

Journal ArticleDOI
TL;DR: In this article , a new shock tube facility has been designed, constructed, and characterized at the University of Central Florida, which is capable of withstanding pressures of up to 1000 atm, allowing for combustion diagnostics of extreme conditions.
Abstract: A new shock tube facility has been designed, constructed, and characterized at the University of Central Florida. This facility is capable of withstanding pressures of up to 1000 atm, allowing for combustion diagnostics of extreme conditions, such as in rocket combustion chambers or in novel power conversion cycles. For studies with toxic gas impurities, the high initial pressures required the development of a gas delivery system to ensure the longevity of the facility and the safety of the personnel. Data acquisition and experimental propagation were implemented with remote access to ensure safety, paired with a LabVIEW- and Python-based user interface. Thus far, test pressures of 270 atm, blast pressures of 730 atm, and temperatures approaching 10 000 K have been achieved. The extreme limitations of this facility allow for emission spectroscopy to be performed during the oxidation of fuel mixtures, e.g., alkanes diluted in argon and carbon dioxide. Ignition delay times were determined and compared to simulations using chemical kinetic mechanisms. The design, experimental procedures, processes of analysis, and uncertainty determination are outlined, and typical pressure profiles are compared with a new gas dynamics solver and empirical correlations developed across multiple shock tube facilities. Preliminary reactive mixture analyses are included with further investigation of the mixtures outlined.

Journal ArticleDOI
TL;DR: In this paper , a 28 GHz TE01 mode 160° miter bend employing two plane mirrors is proposed based on the quasi-optical technique and the coupled wave theory to realize high-efficiency transmission for the electron cyclotron resonance ion source.
Abstract: In this paper, a 28 GHz TE01 mode 160° miter bend employing two plane mirrors is proposed based on the quasi-optical technique and the coupled wave theory to realize high-efficiency transmission for the electron cyclotron resonance ion source. First, the TE01 mode was converted to TE0n hybrid modes with Gaussian beam characteristics by means of the designed mode converter. Second, the phase shift section was implemented to eliminate the phase difference of the hybrid modes. Then, upon reflection of two plane mirrors, the propagation direction of a wave beam is deviated by 160°. Finally, the hybrid modes were converted to the TE01 mode using the same structures of the phase shift section and the mode converter. The simulation results reveal that the TE01 mode transmission efficiency reaches 95.22% at the central frequency of 28 GHz. Additionally, the designed 160° miter bend has been fabricated, installed, and measured. The experimental results show that the power transmission efficiency reaches 98.54% including diffraction losses and ohmic losses.

Journal ArticleDOI
TL;DR: In this paper , a 15-point Thomson scattering diagnostic system is developed for ENN's spherical torus experiment XuanLong-50 (EXL-50) to enable measurements at low density (∼0.5 × 1018m-3) plasma operations, the opto-mechanical subsystems carefully designed to maximize the collection and transmission of the scattered light and to minimize the stray light level.
Abstract: A 15-point Thomson scattering diagnostic system is developed for ENN's spherical torus experiment XuanLong-50 (EXL-50). A BeamTech laser with 3 J/pulse (1064 nm wavelength) at 50 Hz repetition rate is chosen for measurements during EXL-50 plasma operations. To enable measurements at low density (∼0.5 × 1018 m-3) plasma operations, the opto-mechanical subsystems are carefully designed to maximize the collection and transmission of the scattered light and to minimize the stray light level. In addition, the high bandwidth trans-impedance amplifiers and segmented high speed waveform digitizers allow for the application of muti-pulse averaging to further improve the signal-to-noise ratio. Details of the diagnostic system are described and initial experimental results are presented.