Journal ArticleDOI
Evolved Gas Analysis by Infrared Spectroscopy
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TLDR
The analytical applications of the evolved gas analysis (EGA) performed by infrared spectroscopy, for the period extending from 2005 to 2009, are collected in this paper, where the nature of volatile products released by a substance subjected to a controlled temperature program are determined, with the possibility to prove a supposed reaction, either under isothermal or under heating conditions.Abstract:
The analytical applications of the evolved gas analysis (EGA) performed by infrared spectroscopy, for the period extending from 2005 to 2009, are collected in this review. By this technique, the nature of volatile products released by a substance subjected to a controlled temperature program are on-line determined, with the possibility to prove a supposed reaction, either under isothermal or under heating conditions.read more
Citations
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Vibrational Spectroscopy of Ionic Liquids
TL;DR: The conceptual basis of theoretical frameworks which have been used to interpret vibrational spectra of ionic liquids are reviewed, helping the reader to distinguish the scope of application of different methods of calculation.
Journal ArticleDOI
Investigation on the effect of particle size and heating rate on pyrolysis characteristics of a bituminous coal by TG–FTIR
TL;DR: In this article, thermal behavior of five different coal particle fractions were investigated using thermogravimetric analyzer (TGA) under various heating rates with the maximum of 1000 K/min.
Journal ArticleDOI
Thermal decomposition of energetic materials using TG-FTIR and TG-MS: a state-of-the-art review
TL;DR: In this article, the thermal decomposition mechanisms of energy-rich materials have been investigated experimentally and theoretically for decades, but there are still many unanswered questions concerning their thermal decompositions.
Journal ArticleDOI
TG-FTIR and kinetics of devolatilization of Sulcis coal
TL;DR: In this article, the N2-pyrolysis of low-rank Sulcis coal was investigated by thermogravimetric techniques (TG/DTG) in the temperature range ambient to 1000°C under dynamic heating conditions (50, 75, and 100,°Cmin−1 heating rates).
Journal ArticleDOI
Evolved Gas Analysis by Mass Spectrometry
TL;DR: The analytical applications of the evolved gas analyses (EGAs) performed by mass spectrometry for the period extending from 2005 to 2010 are collected in this paper, with the possibility to prove a supposed reaction either under isothermal or under heating conditions.
References
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Journal ArticleDOI
Characteristics of hemicellulose, cellulose and lignin pyrolysis
TL;DR: In this article, the pyrolysis characteristics of three main components (hemicellulose, cellulose and lignin) of biomass were investigated using, respectively, a thermogravimetric analyzer (TGA) with differential scanning calorimetry (DSC) detector and a pack bed.
Journal ArticleDOI
Mechanism study of wood lignin pyrolysis by using TG–FTIR analysis
TL;DR: In this paper, Van Soest's method was performed to extract lignin from different species of biomass, including fir and birch lignins, and the microstructure was studied by a Fourier transform infrared spectrometry.
Journal ArticleDOI
The mechanism for thermal decomposition of cellulose and its main products
Dekui Shen,Sai Gu +1 more
TL;DR: It is found that the formation of CO is enhanced with elevated temperature and residence time, while slight change is observed for the yield of CO(2).
Journal ArticleDOI
Flame retardancy mechanisms of aluminium phosphinate in combination with melamine polyphosphate and zinc borate in glass-fibre reinforced polyamide 6,6
TL;DR: In this paper, the fire retardancy mechanisms of aluminium diethylphosphinate in combination with melamine polyphosphate and zinc borate were analyzed in glass-fibre reinforced polyamide 6,6.
Journal ArticleDOI
Influence of the oxidation state of phosphorus on the decomposition and fire behaviour of flame-retarded epoxy resin composites
Ulrike Braun,Aliaksandr I. Balabanovich,Bernhard Schartel,U. Knoll,Johannes Artner,Michael Ciesielski,Manfred Döring,R. M. Perez,Jan K.W. Sandler,Volker Altstädt,Thorsten Hoffmann,Doris Pospiech +11 more
TL;DR: In this paper, a systematic and comparative evaluation of the pyrolysis of halogen-free flame-retarded epoxy resins containing phosphine oxide, phosphinate, phosphonate, and phosphate (phosphorus contents around 2.6 wt%) and the fire behavior of their carbon fiber composites is presented.