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Showing papers in "Materials Research Bulletin in 1996"


Journal ArticleDOI
TL;DR: In this paper, a straightforward combustion synthesis technique to prepare submicron calcium aluminates using the corresponding metal nitrates-urea mixtures, at low temperature and short reaction times, was discussed.

221 citations


Journal ArticleDOI
TL;DR: In this paper, the dielectric properties of the hexagonal perovskite oxides, La4BaTi4O15, La 4Ba2Ti5O18 and Ba5Nb4O5O15 have been characterized at microwave frequencies.

189 citations


Journal ArticleDOI
TL;DR: The electrical anisotropy of layer-structured bismuth titanate (Bi 4 Ti 3 O 12 ) has been investigated by measurements of Seebeck coefficient, dielectric permittivity, DC conductivity, and complex impedance on single and polycrystalline samples as mentioned in this paper.

182 citations


Journal ArticleDOI
TL;DR: In this article, the effects of grinding and sintering processes on the Seebeck coefficient, electrical conductivity, and thermoelectric figure of merit were investigated for different particle sizes.

134 citations


Journal ArticleDOI
TL;DR: In this paper, the deintercalation of calcium from the interlayer of CaSi 2 was performed by using concentrated HCl solutions at low temperatures, 0 and −30 °C.

131 citations


Journal ArticleDOI
TL;DR: The phase diagram of the nonstoichiometric oxide SrCo 0.8 Fe 0.2 O 3 − δ has been determined as a function of temperature (550 °C ≤ T ≤ 900 °C) and oxygen partial pressure (0.015 atm ≤ pO 2 ≤ 1 atm) by thermogravimetric analysis as discussed by the authors.

127 citations


Journal ArticleDOI
TL;DR: In this article, the thermal stability of stoichiometric spinel phases in the system Li{sub 1+{delta}}Mn{sub 2{minus}delta]O{sub 4} (0 {le} {delta}{le} 0.33) has been investigated by high-temperature powder X-ray diffraction, differential thermal analysis, and thermogravimetric analysis.

120 citations


Journal ArticleDOI
TL;DR: In this article, the effect of temperature on the plane-wave SE of a lightly doped (0.006 M p-TS) polypyrrole (PPy) film was also investigated.

112 citations


Journal ArticleDOI
TL;DR: In this article, the ion exchange properties of the sodium birnessite Na0.32MnO2,yH2O were investigated and compared with previous data obtained for some compounds and in relation with mechanism invoked for Li electrochemical insertion into solgel and chemical birnessites.

101 citations


Journal ArticleDOI
TL;DR: In this article, the photoluminescence spectra of Eu3+-doped lanthanide oxysulfide [Y2O2S, La2O 2S, and Gd 2O2 S] powder phosphors have been analyzed and the richness of the red color has been verified by determining their color coordinates from the CIE standard charts.

97 citations


Journal ArticleDOI
TL;DR: In this article, the structures and luminescent properties of a series of Eu2+ doped Ba and Sr borates have been investigated and a simple structural relationship is established that distinguishes violet and blue emitting compounds from those that emit at longer wavelengths (> 500 nm.

Journal ArticleDOI
TL;DR: In this article, the insertion loss, return loss and electromagnetic shielding effectiveness of carbon-black and carbon-fiber-filled polypropylene composites were studied in the 8 to 12 GHz frequency range.

Journal ArticleDOI
TL;DR: In this article, the luminescence properties of Y2SiO5 and energy transfer from Ce3+ to Tb3+ were studied in two modifications of the crystal structure, low temperature X (1) type and high temperature X(2) type.

Journal ArticleDOI
TL;DR: Yttrium oxide doped with trivalent europium has been prepared by self-propagating high temperature (SPHT) synthesis, also known as combustion synthesis, with nitrogen-based fuels as mentioned in this paper.

Journal ArticleDOI
TL;DR: Pyrrole was polymerized in the presence of ultrafine zirconium (IV) oxide (ZrO2) particles which act as a dispersant for pyrrole as mentioned in this paper.

Journal ArticleDOI
TL;DR: In this paper, an inorganic sol-gel method was developed to produce vanadium dioxide (VO{sub 2}) thin films which exhibit an apparently reversible electrical resistance switching at about 60 C.

Journal ArticleDOI
Shigehito Deki1, Y. Aoi1, Y. Miyake1, A. Gotoh1, Akihiko Kajinami1 
TL;DR: In this article, a vanadium oxide thin film has been prepared from an aqueous solution system of (V2O5-HF) with addition of aluminum metal by a novel wet preparation method called Liquid Phase Deposition (LPD).

Journal ArticleDOI
TL;DR: In this paper, photo-induced second harmonic generation (SHG) and piezooptics were used as the main tools in the investigations of low-temperature optical properties of PbO-Bi 2O3-Ga2O3 glasses.

Journal ArticleDOI
TL;DR: The crystal structure of the ion-exchangeable layered perovskite compounds K2La2Ti3O10 and Li2La 2Ti 3O10 was determined by Rietveld analysis for the powder X-ray diffraction pattern as discussed by the authors.

Journal ArticleDOI
TL;DR: In this paper, a new process for submicronic MgO powder synthesis starting with Mg(OCH 3 ) 2 was studied and the influence of various experimental parameters (water to alkoxide ratio, temperature, reaction time) was investigated.

Journal ArticleDOI
TL;DR: In this paper, triple phosphates of calcium, sodium and trivalent elements (Eu, Nd, Fe) in Ca3(PO4)2-RPO4-Na3PO4 systems were predicted on the basis of crystal chemistry data and synthesized.

Journal ArticleDOI
TL;DR: In this paper, single crystals of the PbO-B{sub 2}OI{sub 3} pseudo binary system were successfully obtained by a flux method using Pb O-B[sub 2]OI[sub 3] flux.

Journal ArticleDOI
TL;DR: In this paper, the longitudinal and transversal frequencies of a series of cobaltite spinels were determined from the infrared reflectance spectra of thin layers on a cobalt substrate.

Journal ArticleDOI
TL;DR: The linear thermal expansion curves did not show any hystersis indicating the absence of microcracking in the sintered bodies of Synroc-B powder as discussed by the authors, which achieved a thermal expansion coefficient of $8.72\times 10^{-6} K^{-1}

Journal ArticleDOI
TL;DR: In this article, a vacuum infiltration process has been developed to process aluminum-base composites reinforced with particulate SiC{sub p}. Electroless nickel coating of SiC {sub p} was used to improve wetting by molten aluminum.

Journal ArticleDOI
TL;DR: In this article, the metal cobaltites, MCo2O4 where M = Mg, Mn, Ni, Zn or Cd were obtained from the above complexes as decomposition residues by heating these complexes in a pre-heated silica crucible at 500 °C for about fifteen minutes.

Journal ArticleDOI
TL;DR: In this article, the layered hosts Na-montmorillonite, MoS2, MoSe2, TiS2 and TaS2 were combined with linear poly(ethylenimine) (LPEI) in aqueous solution.

Journal ArticleDOI
TL;DR: The compound Sr5TiNb4O17 was prepared and its crystal structure determined by single-crystal X-ray diffraction as mentioned in this paper, which consists of alternating perovskite-like slabs offset with respect to each other by a 2 and c 2.

Journal ArticleDOI
TL;DR: In this article, nano-sized amorphous molybdenum dioxide powders have been prepared for the first time using γ-ray radiation in ambient pressure and room temperature.

Journal ArticleDOI
TL;DR: In this paper, the photocatalytic activity in photodehydrogenation of H2S of zinc ferrites synthesized by shock wave loading is investigated and compared with that of zinc preconditioned by calcination.