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Journal ArticleDOI

Ambient-temperature supercritical drying of transparent silica aerogels☆

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TLDR
In this article, a technique to supercritically dry alcogels to transparent silica aerogels at near ambient temperature was described, and the time required for drying was reduced from 2-3 days to 8-10 hours.
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This article is published in Materials Letters.The article was published on 1985-07-01. It has received 248 citations till now. The article focuses on the topics: Supercritical fluid & Supercritical drying.

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Citations
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Silica aerogel; synthesis, properties and characterization

TL;DR: In this article, a review of research work and developments in synthesis, properties and characterization of silica aerogels is presented, with particular attention paid to drying, which is a critical step in aerogel synthesis and makes the production of this material more economical and commercial.
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Theory of Drying

TL;DR: In this paper, the authors examined the forces that produce shrinkage and the mechanisms responsible for transport of liquid, and a variety of strategies for avoiding fracture during drying were discussed, with the emphasis on the constant rate period (CRP) when the pores are full of liquid.
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Aerogel insulation for building applications: A state-of-the-art review

TL;DR: In this article, a review of the knowledge of aerogel insulation in general and for building applications in particular is given, where the possibility of high transmittances in the solar spectrum is of high interest for the construction sector.
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Silica aerogel: synthesis and applications

TL;DR: In this paper, a review of the synthesis of silica aerogels by the sol-gel method, as well as drying techniques and applications in current industrial development and scientific research is presented.
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Toward aerogel based thermal superinsulation in buildings: A comprehensive review

TL;DR: Aerogel is a kind of synthetic porous material, in which the liquid component of the gel is replaced with a gas as mentioned in this paper, and it is considered as one of the most promising thermal insulating materials for building applications.
References
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Journal ArticleDOI

Techniques for the preservaation of three-dimensional structure in preparing specimens for the electron microscope†

TL;DR: In this paper, a method of sample preparation that reduces distortion and maintains 3D structure is described, where a droplet is placed on a formvar-coated screen and fix with osmic acid vapor.
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Coherent Expanded-Aerogels

TL;DR: The two-phase structure of gels has been investigated extensively in colloid chemistry as discussed by the authors, and the results of diffusion experiments through gels, the fact that the electrical conductivity, refractive index, and vapor pressure before and after setting are identical, at least in certain cases, and the known facts of syneresis would seem to leave little room for doubt of the two phase nature of Gels in general.
Journal ArticleDOI

Coherent Expanded-Aerogels

TL;DR: The two-phase structure of gels has been investigated extensively in colloid chemistry as discussed by the authors, and the results of diffusion experiments through gels, the fact that the electrical conductivity, refractive index, and vapor pressure before and after setting are identical, at least in certain cases, and the known facts of syneresis would seem to leave little room for doubt of the two phase nature of Gels in general.
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Transparent silica aerogels for window insulation

TL;DR: In this article, the microstructure and optical properties of transparent silica aerogels were investigated and the energy transfer through hypothetical aerogel windows were calculated through theoretical analysis.
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