Journal ArticleDOI
Metallation of 2-sulfanilamidopyrimidine (sulfadiazine). X-ray diffraction structure and solution behaviour of bis(sulfadiazinato) mercury(II) bis(dimethylsulfoxide)
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TLDR
The X-ray crystal structure of Hg(Sulfa) 2 · 2DMSO (1 ) was determined in this paper, and the coordination geometry about the mercury atom is approximately linear.About:
This article is published in Polyhedron.The article was published on 1997-01-01. It has received 23 citations till now. The article focuses on the topics: Mercury (element) & Crystal structure.read more
Citations
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Journal ArticleDOI
Coordination behaviour of sulfanilamide derivatives.
Angel García-Raso,Juan J. Fiol,Santiago Rigo,Antonio López-López,Elies Molins,Enrique Espinosa,Elisa Borrás,Gloria Alzuet,Joaquín Borrás,Alfonso Castiñeiras +9 more
TL;DR: In this paper, the X-ray crystal structures of [Hg(sulfamethoxypyridazinato)2] (2a), [Cd(Sulfadimitriou)2(H2O)] (4b) and [Zn(methoxazolato) 2(py)2.2(h2O)2 (6d) have been determined.
Journal ArticleDOI
Synthesis, characterization and antibacterial activity of a tridentate Schiff base derived from cephalothin and sulfadiazine, and its transition metal complexes.
TL;DR: Metal(II) coordination compounds of a cephalothin Schiff base (H2L) derived from the condensation of cep Halothin antibiotic with sulfadiazine were synthesized and behaves as a dianionic tridentate NOO chelating agent.
Journal ArticleDOI
Crystal structure of zinc(II) 2-sulfanilamidopyrimidine: a widely used topical burn drug
Rong-Xin Yuan,Ren-Gen Xiong,Zhen-Feng Chen,Pei Zhang,Huangxian Ju,Zong Dai,Zi-Jian Guo,Hoong-Kun Fun,Xiao-Zeng You +8 more
TL;DR: The reaction of H-SD (sulfadiazine) with Zn(OAc)2·2H2O in water-ethanol under solvothermal reaction conditions yields crystals of Zn (SD)2 (1) suitable for X-ray analysis as mentioned in this paper.
Journal ArticleDOI
Syntheses and characterisation of mercury complexes of sulfadiazine, sulfamerazine and sulfamethazine
TL;DR: In this paper, the synthesis and characterization of the Hg(II) complexes of sulfadiazine 1, sulfamerazine 2 and sulfamethazine 3 in dimethylformamide solution in presence of ammonia was described.
Journal ArticleDOI
Synthesis, spectroscopic characterization, antimicrobial activity and crystal structure of silver and copper complexes of sulfamethazine
Sanjay M. Tailor,Urmila H. Patel +1 more
TL;DR: In this paper, the results of IR, UV-vis, and 1H NMR spectral data and thermal analysis for 1 and 2 suggest that the binding of silver and copper t...
References
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Book
Infrared and Raman Spectra of Inorganic and Coordination Compounds
TL;DR: In this article, the normal modes of vibration are illustrated and corresponding vibrational frequencies are listed for each type, including diatomic, triatomic, fouratomic, five-atomic, six-atomic and seven-atomic types.
Journal ArticleDOI
Proton and carbon-13 assignments from sensitivity-enhanced detection of heteronuclear multiple-bond connectivity by 2D multiple quantum NMR
Ad Bax,Michael F. Summers +1 more
Journal ArticleDOI
Practical aspects of two-dimensional transverse NOE spectroscopy
Ad Bax,Donald G. Davis +1 more
TL;DR: In this paper, the authors proposed a new method for measuring homonuclear NOE effects under spin-locked conditions, which they referred to as rotatingframe Overhauser enhancement spectroscopy (ROESY) since this name suggests a similarity with the closely related 2D NOESY experiment.
Journal ArticleDOI
Sensitivity-enhanced two-dimensional heteronuclear shift correlation NMR spectroscopy
Ad Bax,Sankaran Subramanian +1 more
TL;DR: In this paper, a simple method that alleviates the dynamic range problem and that facilitates the suppression of signals from protons that are not coupled to the lowy nucleus is described, where the low-y nucleus was assumed to be 13C.
Book ChapterDOI
Inorganic Chemistry and Drug Design
TL;DR: The use of inorganic compounds in medicine dates back to ancient times as discussed by the authors, and mercurial chloride was known to be a diuretic during the Renaissance period, while arsenobetaine (Me 3 As + CH 2 C 0 2 − ) is relatively nontoxic.