Journal ArticleDOI
NMR experiments with a new double rotor
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TLDR
In this paper, a double-rotation NMR model was proposed for polycrystalline compounds with dipole-dipole and second-order quadrupole interactions.About:
This article is published in Journal of Magnetic Resonance.The article was published on 1990-09-01. It has received 110 citations till now. The article focuses on the topics: Rotor (electric).read more
Citations
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Journal ArticleDOI
Modelling one- and two-dimensional solid-state NMR spectra†
Dominique Massiot,Franck Fayon,Mickaël Capron,Ian King,Ian King,Stéphanie Le Calvé,Bruno Alonso,Jean-Olivier Durand,Bruno Bujoli,Zhehong Gan,Gina L. Hoatson +10 more
TL;DR: In this article, the authors present some examples of modeling one and two-dimensional solid-state NMR spectra of I = ½ spin and quadrupolar nuclei, using laboratory-developed software that is made available to the NMR community.
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First-principles calculation of NMR parameters using the gauge including projector augmented wave method:a chemist's point of view
Christian Bonhomme,Christel Gervais,Florence Babonneau,Cristina Coelho,Frédérique Pourpoint,Thierry Azaïs,Sharon E. Ashbrook,John M. Griffin,Jonathan R. Yates,Francesco Mauri,Chris J. Pickard +10 more
TL;DR: Including Projector Augmented Wave Method: A Chemist’s Point of View is presented.
Journal ArticleDOI
Solid-state NMR spectroscopic methods in chemistry.
TL;DR: This Review outlines some of the developments of solid-state NMR spectroscopy, including techniques such as cross-polarization, magic-angle spinning, multiple-pulse sequences, homo- and heteronuclear decoupling and recoupling techniques,multiple-quantum spectroscology, and dynamic angle spinning, as well as their applications to structure determination.
Journal ArticleDOI
Satellite transitions in MAS NMR spectra of quadrupolar nuclei
TL;DR: In this article, the authors used one-pulse magic-angle spinning (MAS) NMR experiments of crystalline powders for the determination of quadrupole coupling constants and asymmetry parameters for the electric field gradient tensors from 17O, 23Na, and 27Al MAS NMR spectra.
Journal ArticleDOI
Quantitative Multiple-Quantum Magic-Angle-Spinning NMR Spectroscopy of Quadrupolar Nuclei in Solids
TL;DR: In this article, a rotation-induced adiabatic coherence transfer (RIACT) was proposed to extract quantitative information about site populations from isotropic MQ NMR spectra.
References
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Journal ArticleDOI
High resolution solid-state N.M.R.
TL;DR: By means of rotations around two axes inclined at zeros (magic angles) of the l = 2 and l = 4 Legendre polynomials, first-order and second-order N.M.R. broadening can be averaged away.
Journal ArticleDOI
Towards high-resolution NMR of more nuclei in solids: Sample spinning with time-dependent spinner axis angle
TL;DR: In this article, the theoretical principles of a new class of NMR experiments (DAS, dynamic angle spinning) which can remove not only the first-order broadening but also the second-order (or higher-order) broadenings are given.
Journal ArticleDOI
Dynamic-Angle Spinning of Quadrupolar Nuclei
TL;DR: In this article, a sample spins around an axis inclined at an angle θ ( t ) with respect to the magnetic field such that the averages of P n ( cos θ ) are zero.
Journal ArticleDOI
Oxygen-17 NMR in solids by dynamic-angle spinning and double rotation
Bradley F. Chmelka,Bradley F. Chmelka,Karl T. Mueller,Karl T. Mueller,Alexander Pines,Alexander Pines,Jonathan F. Stebbins,Jonathan F. Stebbins,Yue Wu,Yue Wu,Josef W. Zwanziger,Josef W. Zwanziger +11 more
TL;DR: In this article, Samoson et al. presented the first experimental results using DAS and showed the application of DOR to the resolution of distinct oxygen sites in an important class of oxide materials, including cristobalite (SiO2) and diopside (CaMgSi2O6).
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