Journal ArticleDOI
A simple, fast and cheap non-SPE screening method for antibacterial residue analysis in milk and liver using liquid chromatography–tandem mass spectrometry
Magda Targa Martins,Magda Targa Martins,Jéssica Melo,Fabiano Barreto,Fabiano Barreto,Rodrigo Barcellos Hoff,Louise Jank,Louise Jank,Michele Soares Bittencourt,Juliana Bazzan Arsand,Juliana Bazzan Arsand,Elfrides Eva Scherman Schapoval +11 more
TLDR
An efficient technique for the analysis of multiclass antibacterial residues (fluoroquinolones, tetracyclines, sulfonamides and trimethoprim) was developed based on simple, environment-friendly extraction for bovine milk, cattle and poultry liver and proved that it can be an important tool in routine analysis, since it is very fast and reliable.About:
This article is published in Talanta.The article was published on 2014-11-01. It has received 39 citations till now. The article focuses on the topics: Maximum Residue Limit & European union.read more
Citations
More filters
Journal ArticleDOI
Antibiotic residues in milk: Past, present, and future.
TL;DR: It is observed that antibiotics residues are more common in milk samples that are being manifested in increasing researches on antibiotic detection and measures should be adopted to cease this residue.
Journal ArticleDOI
Sulphonate functionalized covalent organic framework-based magnetic sorbent for effective solid phase extraction and determination of fluoroquinolones.
Aying Wen,Guoliang Li,Guoliang Li,Di Wu,Yanxin Yu,Yan Yang,Na Hu,Honglun Wang,Jian Chen,Yongning Wu +9 more
TL;DR: Results indicated that the Fe3O4@COF(TpBD)@Au-MPS is a promising magnetic adsorbent for trace fluoroquinolones determination in meat samples and a facile strategy for COF functionalization, but also developed an efficient method for detecting fluoroquolones in foodstuffs.
Journal ArticleDOI
Multiclass methods for the analysis of antibiotic residues in milk by liquid chromatography coupled to mass spectrometry: A review
Rosanna Rossi,Giorgio Saluti,Simone Moretti,Irene Diamanti,Danilo Giusepponi,Roberta Galarini +5 more
TL;DR: This article reviews the major multiclass methods published for the determination of antibiotic residues in milk by liquid chromatography coupled to mass spectrometry, with a special focus on sample preparation approaches.
Journal ArticleDOI
A fast and simple LC-ESI-MS/MS method for detecting pyrrolizidine alkaloids in honey with full validation and measurement uncertainty
Andressa Camargo Valese,Luciano Molognoni,Leandro Antunes de Sá Ploêncio,Flávia Gontijo de Lima,Luciano Valdemiro Gonzaga,Silvana Lima Górniak,Heitor Daguer,Fabiano Barreto,Ana Carolina Oliveira Costa +8 more
Journal ArticleDOI
Screening and confirmatory method for multiclass determination of 62 antibiotics in meat.
Simone Moretti,Guglielmo Dusi,Danilo Giusepponi,Simona Pellicciotti,Rosanna Rossi,Giorgio Saluti,Gabriele Cruciani,Roberta Galarini +7 more
TL;DR: The studied performance characteristics were selectivity, linearity, precision, trueness, decision limits, detection capabilities, detection and quantification limits, and Ruggedness tests demonstrated the applicability to swine and poultry muscle.
References
More filters
Journal ArticleDOI
Antibiotics and antibiotic resistance in water environments
TL;DR: Methods to reduce resistant bacterial load in wastewaters, and the amount of antimicrobial agents, in most cases originated in hospitals and farms, include optimization of disinfection procedures and management of wastewater and manure.
Journal ArticleDOI
Signal suppression/enhancement in high-performance liquid chromatography tandem mass spectrometry
TL;DR: The review discusses the pitfalls of the matrix effect in mass spectrometry detection hyphenated to liquid chromatography separation and proposes hypotheses to explain the observed behaviours and proposes methods and strategies to overcome the matrix effects.
Journal ArticleDOI
Fast screening methods to detect antibiotic residues in food samples
TL;DR: The lowest limits of detection were achieved using microbiological inhibition tests and immunoassays with time-resolved fluorometry detection, so antibiotic residues at levels lower than the maximum residue limits established by legislation were detected.
Journal ArticleDOI
Complexities in tetracycline analysis-chemistry, matrix extraction, cleanup, and liquid chromatography.
TL;DR: This review compiles, compares, and discusses the results and observations found in published methods, while focusing on chemical principles in order to increase the practicing chemist's understanding of TCs to aid him/her in developing useful analyses.