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Journal ArticleDOI

Determination of organic compounds in water using dispersive liquid-liquid microextraction

TLDR
The ability of DLLME technique in the extraction of other organic compounds such as organochlorine pesticides, organophosphorus pesticides and substituted benzene compounds were studied.
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This article is published in Journal of Chromatography A.The article was published on 2006-05-26. It has received 2959 citations till now. The article focuses on the topics: Extraction (chemistry) & Aqueous two-phase system.

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Citations
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Journal ArticleDOI

Dispersive liquid–liquid microextraction based on hydrophobic deep eutectic solvents: Application for tetracyclines monitoring in milk

TL;DR: In this article, eleven hydrophobic deep eutectic solvents (hDESs) based on some naturally occurring fatty acids, alcohols, and choline chloride were synthesized and evaluated as green extractants in the dispersive liquid-liquid microextraction (DLLME) of oxytetracycline, tetracyCLine, and doxycycline.
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Magnetic solid phase extraction using gold immobilized magnetic mesoporous silica nanoparticles coupled with dispersive liquid-liquid microextraction for determination of polycyclic aromatic hydrocarbons.

TL;DR: An efficient magnetic sorbent was introduced for solid phase extraction by incorporation of the gold nanoparticles into the hexagonal lattice of magnetic MCM-41 to achieve high pre-concentration factors (PFs) and was coupled with dispersive liquid-liquid microextraction (DLLME) procedure.
Journal ArticleDOI

Low cost methodology for estrogens monitoring in water samples using dispersive liquid-liquid microextraction and HPLC with fluorescence detection.

TL;DR: A new low cost methodology for estrogens' analysis in water samples was developed, based on dispersive liquid-liquid microextraction followed by high-performance liquid chromatography with fluorescence detection, which is fast, cheap, easy-to-use, uses low volumes of organic solvents and has the possibility of a large number of samples to be extracted in parallel.
Journal ArticleDOI

Emulsification liquid phase microextraction followed by on-line phase separation coupled to high performance liquid chromatography.

TL;DR: An emulsification liquid phase microextraction followed by on-line phase separation coupled to high performance liquid chromatography (HPLC) is introduced based on a novel idea for the separation of dispersed organic phase from aqueous phase and was successfully applied to determine selected parabens in some water and cosmetic samples.
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Microwave-Based Technique for Fast and Reliable Extraction of Organic Contaminants from Food, with a Special Focus on Hydrocarbon Contaminants.

TL;DR: In the first part of this review, an updated overview of the microwave-based extraction technique used for rapid and efficient extraction of organic contaminants from food is given, and the latest applications concerning the use of microwave energy for the determination of hydrocarbon contaminants are reported and critically overviewed.
References
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Journal ArticleDOI

Solvent microextraction into a single drop.

TL;DR: An analytical technique is described which combines solvent extraction with gas chromatographic (GC) analysis in a simple and inexpensive apparatus involving very little solvent consumption and is in good agreement with a convective-diffusive kinetic model.
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Analytical chemistry in a drop. Solvent extraction in a microdrop.

TL;DR: This unique microextraction system is simple and flexible, permits automated backwashing, consumes only microquantities of organic solvents, and is capable of being coupled with other analytical systems.
Journal ArticleDOI

Liquid-Phase Microextraction in a Single Drop of Organic Solvent by Using a Conventional Microsyringe

TL;DR: In this article, two modes of liquid-phase microextraction (LPME) were developed for capillary gas chromatography, i.e., static and dynamic LPME, which involve the use of very small amounts of organic solvent in a conventional microsyringe.
Journal ArticleDOI

Mass Transfer Characteristics of Solvent Extraction into a Single Drop at the Tip of a Syringe Needle

TL;DR: In this article, the authors measured the amount of a sample compound extracted into a 1-μL drop of n-octane suspended in a stirred aqueous solution from the tip of a microsyringe needle.
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