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Journal ArticleDOI

A simple setup to simultaneously measure the resonant frequency and the absolute dissipation factor of a quartz crystal microbalance

Michael Rodahl, +1 more
- 01 Sep 1996 - 
- Vol. 67, Iss: 9, pp 3238-3241
TLDR
In this article, an experimental setup that can simultaneously measure the absolute dissipation factor and the resonant frequency of a short-circuited quartz crystal microbalance is described, where the crystal leads are fed through the center of the ferrite toroid and the secondary winding of the transformer is connected to a digitizing oscilloscope which records the decay of the crystal oscillation.
Abstract
An experimental setup is described that can simultaneously measure the absolute dissipation factor and the resonant frequency of a short‐circuited quartz crystal microbalance The crystal is driven at approximately its resonant frequency by a signal generator which is intermittently disconnected by a relay, causing the crystal oscillation amplitude to decay exponentially The decay is measured using a ferrite toroid transformer One of the crystal leads is fed through the center of the ferrite toroid and thereby acts as the primary winding of the transformer The secondary winding of the transformer is connected to a digitizing oscilloscope which records the decay of the crystal oscillation From the recorded decay curve, the absolute dissipation factor (calculated from the decay time constant) and the series resonant frequency of the freely oscillating crystal are obtained Alternatively, the dissipation factor and resonant frequency can be measured for the crystal oscillating under open‐circuit conditions, ie, in the parallel mode The measurements are automated

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Citations
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Journal ArticleDOI

Variations in Coupled Water, Viscoelastic Properties, and Film Thickness of a Mefp-1 Protein Film during Adsorption and Cross-Linking: A Quartz Crystal Microbalance with Dissipation Monitoring, Ellipsometry, and Surface Plasmon Resonance Study

TL;DR: It is shown how quantitative data about the thickness, shear elastic modulus, and shear viscosity of the protein film can be obtained with the QCM-D technique, even beyond the Sauerbrey regime, if frequency (f) and energy dissipation (D) measurements measured at multiple harmonics are combined with theoretical simulations using a Voight-based viscoelastic model.
Journal ArticleDOI

Molecular basis for the explanation of the exponential growth of polyelectrolyte multilayers.

TL;DR: It is found that, as postulated, PLL diffuses throughout the film down into the substrate after each new PLL injection and out of the film after each PLL rinsing and further after each HA injection, which explains the exponential growth regime.
Journal ArticleDOI

Simultaneous frequency and dissipation factor QCM measurements of biomolecular adsorption and cell adhesion

TL;DR: It is shown theoretically that viscoelastic layers with thicknesses comparable to the biofilms studied in this work can induce energy dissipation of the same magnitude as the measured ones.
Journal ArticleDOI

A comparative study of protein adsorption on titanium oxide surfaces using in situ ellipsometry, optical waveguide lightmode spectroscopy, and quartz crystal microbalance/dissipation

TL;DR: In this article, the adsorption kinetics of three model proteins (human serum albumin, fibrinogen and hemoglobin) were measured and compared using three different experimental techniques: optical waveguide lightmode spectroscopy (OWLS), ellipsometry (ELM) and quartz crystal microbalance (QCM-D).
Journal ArticleDOI

Intact Vesicle Adsorption and Supported Biomembrane Formation from Vesicles in Solution: Influence of Surface Chemistry, Vesicle Size, Temperature, and Osmotic Pressure†

TL;DR: In this paper, the adsorption kinetics of small unilamellar egg-yolk phosphatidylcholine vesicles were investigated by the quartz crystal microbalance−dissipation (QCM−D) technique, as a function of surface chemistry (on SiO2, Si3N4, Au, TiO2 and Pt), temperature (273−303 K), vesicle size (25−200 nm), and osmotic pressure.
References
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Journal ArticleDOI

Measurement of interfacial processes at electrode surfaces with the electrochemical quartz crystal microbalance

TL;DR: The last 10-15 years have seen electrochemista applying more and more sophisticated instrumental techniques to studies of electrode surfaces, both because of the increased availability of powerful new tools for interfacial characterization and because of an increased emphasis in modern electrochemical research on detailed characterization of the structure and composition of the interface as mentioned in this paper.
Journal ArticleDOI

Quartz crystal microbalance setup for frequency and Q‐factor measurements in gaseous and liquid environments

TL;DR: In this paper, an experimental setup has been constructed for simultaneous measurements of the frequency, the absolute Q factor, and the amplitude of oscillation of a quartz crystal microbalance (QCM).

Quartz crystal microbalance setup for frequency and G!?-factor rneasurements in gaseous and liquid environments

TL;DR: In this paper, an experimental setup has been constructed for simultaneous measurements of the frequency, the absolute Q factor, and the amplitude of oscillation of a quartz crystal microbalance (QCM).
Journal ArticleDOI

On the measurement of thin liquid overlayers with the quartz-crystal microbalance

TL;DR: In this article, the authors present a simple model that predicts the changes in resonance frequency and dissipation factor for a quartz-crystal microbalance (QCM) when it is coated with a viscous film that may or may not slip on the crystal.
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