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Journal ArticleDOI

Preparation and structure analysis of titanium oxide nanotubes

Gaohui Du, +4 more
- 16 Nov 2001 - 
- Vol. 79, Iss: 22, pp 3702-3704
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TLDR
In this paper, the atomic structure of the synthesized tubular material is imaged by high-resolution transmission electron microscopy (HRTEM), and the composition of individual tubular structures is determined using selected area energy dispersive X-ray spectroscopy (EDX).
Abstract
Well crystallized nanoscale tubular materials have been synthesized via the reaction of TiO2 crystals of either anatase or rutile phase and NaOH aqueous solution. The atomic structure of the synthesized tubular material is imaged by high-resolution transmission electron microscopy (HRTEM), and the composition of individual tubular structures is determined using selected area energy dispersive X-ray spectroscopy (EDX). Our results show that the tubular materials are well crystallized tubes with an average diameter of about 9 nm and little dispersion, and are composed of mainly titanium and oxygen. The atomic ratio of O/Ti is found, however, to vary from tube to tube. Detailed electron and x-ray diffraction studies show that the structure of our titanium oxide nanotubes do not agree with those made of TiO2 crystals with either anatase or rutile phase. HRTEM observations revealed that the titanium oxide nanotubes usually have multiple shells, in analogy with multiwalled carbon nanotubes, but the shell spacin...

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Citations
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Journal ArticleDOI

Strong Visible Absorption and Photoluminescence of Titanic Acid Nanotubes by Hydrothermal Method

TL;DR: Titanic acid nanotubes (with a chemical formula H2Ti2O4(OH)(2) abbreviated as TANTs) were synthesized by the hydrothermal method using commercial TiO2 nanoparticle powder (P25, Degussa, Germany) including anatase and rutile phase as starting material.
Journal ArticleDOI

TiO2 Nanotube-Supported Cu as the Catalyst for Selective NO Reduction with NH3

TL;DR: Analysis with temperature programmed reduction, X–ray photoelectron spectroscopy, and NO adsorption reflected that the layeredtitanate feature of the tube wall was advantageous for even distribution of the Cu species, thus leading to the high–catalytic activity of the tubular Cu/TiO2 catalyst.
Journal ArticleDOI

The multi-staged formation process of titanium oxide nanotubes and its thermal stability

TL;DR: In this article, the multi-staged formation process of titanium oxide nanotubes was investigated in detail under a hydrothermal treatment, and the thermal stability of the tube products was investigated by X-ray diffraction (XRD) and scanning electron microscope (SEM).
Journal ArticleDOI

Thermal Properties and Combustion Behaviors of Polystyrene/Surface-Modified TiO2 Nanotubes Nanocomposites

TL;DR: In this paper, a modified Titanium dioxide nanotubes, surface modified with phenl dichlorophosphate, were incorporated in polystyrene by in situ bulk radical polymerization.
Journal ArticleDOI

Chemical morphology freezing: chemical protection of the physical morphology of high photoactivity anatase TiO2 nanotubes

TL;DR: In this article, a simple chemical morphology freezing method was used to prevent the thermodynamic behavior of nanomaterials by using a simple LaMer-model carbon and then coating with a silica sheath.
References
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Journal ArticleDOI

Helical microtubules of graphitic carbon

Sumio Iijima
- 01 Nov 1991 - 
TL;DR: Iijima et al. as mentioned in this paper reported the preparation of a new type of finite carbon structure consisting of needle-like tubes, which were produced using an arc-discharge evaporation method similar to that used for fullerene synthesis.
Journal ArticleDOI

Room-temperature transistor based on a single carbon nanotube

TL;DR: In this paper, the fabrication of a three-terminal switching device at the level of a single molecule represents an important step towards molecular electronics and has attracted much interest, particularly because it could lead to new miniaturization strategies in the electronics and computer industry.
Book

Physical properties of carbon nanotubes

TL;DR: In this paper, an introductory textbook for graduate students and researchers from various fields of science who wish to learn about carbon nanotubes is presented, focusing on the basic principles behind the physical properties and giving the background necessary to understand the recent developments.
Book

Science of fullerenes and carbon nanotubes

TL;DR: In this paper, the authors present a detailed overview of the properties of Fullerenes and their properties in surface science applications, such as scanning tunnel microscopy, growth and fragmentation studies, and chemical synthesis.
Journal ArticleDOI

Boron Nitride Nanotubes

TL;DR: Electron energy-loss spectroscopy on individual tubes yielded B:N ratios of approximately 1, which is consistent with theoretical predictions of stable BN tube structures.
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