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Journal ArticleDOI

Preparation and structure analysis of titanium oxide nanotubes

Gaohui Du, +4 more
- 16 Nov 2001 - 
- Vol. 79, Iss: 22, pp 3702-3704
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TLDR
In this paper, the atomic structure of the synthesized tubular material is imaged by high-resolution transmission electron microscopy (HRTEM), and the composition of individual tubular structures is determined using selected area energy dispersive X-ray spectroscopy (EDX).
Abstract
Well crystallized nanoscale tubular materials have been synthesized via the reaction of TiO2 crystals of either anatase or rutile phase and NaOH aqueous solution. The atomic structure of the synthesized tubular material is imaged by high-resolution transmission electron microscopy (HRTEM), and the composition of individual tubular structures is determined using selected area energy dispersive X-ray spectroscopy (EDX). Our results show that the tubular materials are well crystallized tubes with an average diameter of about 9 nm and little dispersion, and are composed of mainly titanium and oxygen. The atomic ratio of O/Ti is found, however, to vary from tube to tube. Detailed electron and x-ray diffraction studies show that the structure of our titanium oxide nanotubes do not agree with those made of TiO2 crystals with either anatase or rutile phase. HRTEM observations revealed that the titanium oxide nanotubes usually have multiple shells, in analogy with multiwalled carbon nanotubes, but the shell spacin...

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Citations
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Journal ArticleDOI

Review of the progress in preparing nano TiO2: an important environmental engineering material.

TL;DR: This review summarizes fourteen TiO2 preparation methods, such as the sol-gel method, solvothermal method, and reverse micelle method, with an emphasis on the different morphologies ofTiO2 and the influence factors in the synthesis.
Journal ArticleDOI

The design, fabrication, and photocatalytic utility of nanostructured semiconductors: focus on TiO2-based nanostructures

TL;DR: Applications and future directions of nanostructured TiO2 are considered in the context of various photoinduced phenomena such as hydrogen production, electricity generation via dye-sensitized solar cells, photokilling and self-cleaning effect, photo-oxidation of organic pollutant, wastewater management, and organic synthesis.
Journal ArticleDOI

Elongated Titanate Nanostructures and Their Applications

TL;DR: A critical survey of the literature is provided together with the development of prospective energy applications of elongated titanates in catalysis, photocatalysis, electrocatalysis, solar cells, fuel cells, lithium batteries and hydrogen storage.
Journal ArticleDOI

Controlled Growth and Characterization of Tungsten Oxide Nanowires Using Thermal Evaporation of WO3 Powder

TL;DR: In this paper, Tungsten oxide (WO3) nanowires were prepared on a tungsten substrate by thermal evaporation of WO3 powder at elevated temperature in a tube furnace.
Journal ArticleDOI

Fabrication of PbS quantum dot doped TiO2 nanotubes.

TL;DR: PbS quantum dots were prepared on the inside and outside surfaces of TiO(2) nanotubes by using thiolactic acid as an organic linker and characterized by TEM, as well as Raman, FT-IR, and UV-vis spectroscopy.
References
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Journal ArticleDOI

Helical microtubules of graphitic carbon

Sumio Iijima
- 01 Nov 1991 - 
TL;DR: Iijima et al. as mentioned in this paper reported the preparation of a new type of finite carbon structure consisting of needle-like tubes, which were produced using an arc-discharge evaporation method similar to that used for fullerene synthesis.
Journal ArticleDOI

Room-temperature transistor based on a single carbon nanotube

TL;DR: In this paper, the fabrication of a three-terminal switching device at the level of a single molecule represents an important step towards molecular electronics and has attracted much interest, particularly because it could lead to new miniaturization strategies in the electronics and computer industry.
Book

Physical properties of carbon nanotubes

TL;DR: In this paper, an introductory textbook for graduate students and researchers from various fields of science who wish to learn about carbon nanotubes is presented, focusing on the basic principles behind the physical properties and giving the background necessary to understand the recent developments.
Book

Science of fullerenes and carbon nanotubes

TL;DR: In this paper, the authors present a detailed overview of the properties of Fullerenes and their properties in surface science applications, such as scanning tunnel microscopy, growth and fragmentation studies, and chemical synthesis.
Journal ArticleDOI

Boron Nitride Nanotubes

TL;DR: Electron energy-loss spectroscopy on individual tubes yielded B:N ratios of approximately 1, which is consistent with theoretical predictions of stable BN tube structures.
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