Journal ArticleDOI
Synthesis,TG, DSC and infrared spectral study of NiMn2(C4H4O4)3·6N2H4
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TLDR
Nickel manganese succinato-hydrazinate (NiMn2(C4H4O4)3·6N2H4) has been synthesized for the first time by a novel precursor technique and characterized by IR, AAS and XRD as discussed by the authors.Abstract:
Nickel manganese succinato-hydrazinate (NiMn2(C4H4O4)3·6N2H4), has been synthesized for the first time by a novel precursor technique and characterized by IR, AAS and XRD. Thermal decomposition of the compound was studied from room temperature (rT) to 800°C by differential scanning calorimetry (DSC) and thermogravimetric (TG) analysis besides isothermal mass loss studies. The compound was found to decompose autocatalytically, once ignited. TG-DSC shows two steps decomposition i.e. dehydrazination followed by decarboxylation. The infrared spectral studies show the N–N stretching frequency at 972 cm–1 suggesting a bidentate bridging structure of hydrazine molecule in (NiMn2(C4H4O4)3·6N2H4).read more
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Investigation of natural rubber composites with addition of montmorillonite fillers using thermal analysis
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