Journal ArticleDOI
Synthesis,TG, DSC and infrared spectral study of NiMn2(C4H4O4)3·6N2H4
TLDR
Nickel manganese succinato-hydrazinate (NiMn2(C4H4O4)3·6N2H4) has been synthesized for the first time by a novel precursor technique and characterized by IR, AAS and XRD as discussed by the authors.Abstract:
Nickel manganese succinato-hydrazinate (NiMn2(C4H4O4)3·6N2H4), has been synthesized for the first time by a novel precursor technique and characterized by IR, AAS and XRD. Thermal decomposition of the compound was studied from room temperature (rT) to 800°C by differential scanning calorimetry (DSC) and thermogravimetric (TG) analysis besides isothermal mass loss studies. The compound was found to decompose autocatalytically, once ignited. TG-DSC shows two steps decomposition i.e. dehydrazination followed by decarboxylation. The infrared spectral studies show the N–N stretching frequency at 972 cm–1 suggesting a bidentate bridging structure of hydrazine molecule in (NiMn2(C4H4O4)3·6N2H4).read more
Citations
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Influence of B-site Gd+3 substitution on various properties of Co-ferrite nanoparticles
Manoj Salgaonkar,Rajendra S. Gad +1 more
TL;DR: In this paper, the effect of rare earth substitution on various properties of nanocrystalline cobalt ferrite material with composition CoFe2-xGdxO (x = 0, 0.02, 0., 0.04, 0,08, and 0.1) prepared using combustion method was investigated.
Conceptual Review of Iron in Ayurveda
TL;DR: The use of iron in Ayurvedic preparations dates back to the time of Charaka as mentioned in this paper, where iron is treated in cow's urine and extensively used therapeutically as Ayaskruti or as Lauha rasayana before the evolution of Rasashastra as Ayaska.
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Effect of dopant on the characterization of KAP crystal
TL;DR: In this paper, the effect of ammonium sulphate as dopant on the characteristic properties of KAP crystal was studied by thermal and spectral analysis, and a semi organic crystal was grown by Slow Evaporation Solution Growth Technique.
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Thermal, spectral and diffraction properties of Hg(II)-exchanged montmorillonite with alkylamines
M. Loduhová,E. Jóna,V. Bizovská,V. Pavlík,R. Durný,Z. Harmatová,R. Janík,Z. Jankurová,S. C. Mojumdar +8 more
TL;DR: In this article, the effect of steric properties of studied alkylamines is evident, showing that methyl, dimethyl and trimethylamines are intercalated into the interlayer space of Hg-MMT.
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A new amorphous phase of stannic phosphor–silicate
TL;DR: In this article, a new phase of stannic phosphor-silicate inorganic ion exchanger has been synthesized under different conditions of preparation and its chemical composition was determined.
References
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An assessment of high voltage electron microscopy (HVEM). An invited review
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TL;DR: High voltage electron microscopy (HVEM) has been extensively applied in the field of materials science as discussed by the authors, covering the study of heavy metals, ceramics and minerals, large-scale structures, dynamic processes and radiation damage.