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Blazed high-efficiency x-ray diffraction via transmission through arrays of nanometer-scale mirrors

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TLDR
The performance of a critical-angle transmission (CAT) grating in the EUV and soft x-ray band is demonstrated that for the first time combines the advantages of transmission gratings with the superior broadband efficiency of blazed reflection gratings via reflection from nanofabricated periodic arrays of atomically smooth nanometer-thin silicon mirrors.
Abstract
Diffraction gratings are ubiquitous wavelength dispersive elements for photons as well as for subatomic particles, atoms, and large molecules. They serve as enabling devices for spectroscopy, microscopy, and interferometry in numerous applications across the physical sciences. Transmission gratings are required in applications that demand high alignment and figure error tolerances, low weight and size, or a straight-through zero-order beam. However, photons or particles are often strongly absorbed upon transmission, e.g., in the increasingly important extreme ultraviolet (EUV) and soft x-ray band, leading to low diffraction efficiency. We demonstrate the performance of a critical-angle transmission (CAT) grating in the EUV and soft x-ray band that for the first time combines the advantages of transmission gratings with the superior broadband efficiency of blazed reflection gratings via reflection from nanofabricated periodic arrays of atomically smooth nanometer-thin silicon mirrors at angles below the critical angle for total external reflection. The efficiency of the CAT grating design is not limited to photons, but also opens the door to new, sensitive, and compact experiments and applications in atom and neutron optics, as well as for the efficient diffraction of electrons, ions, or molecules.

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Citations
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Journal ArticleDOI

Diffraction efficiency of 200-nm-period critical-angle transmission gratings in the soft x-ray and extreme ultraviolet wavelength bands

TL;DR: Measurements of the diffraction efficiency of 200-nm-period freestanding blazed transmission gratings for wavelengths in the 0.96 to 19.4 nm range show efficiencies in the range of ∼50-100% of theoretical predictions when taking the effects of the support mesh into account.
Journal ArticleDOI

Fabrication of 200nm period blazed transmission gratings on silicon-on-insulator wafers

TL;DR: In this article, the authors reported on the fabrication of 200nm period blazed transmission gratings on silicon-on-insulator (SOI) wafers with high aspect ratio (>100) and smooth sidewalls.
Journal ArticleDOI

Fabrication of subwavelength periodic nanostructures using liquid immersion Lloyd’s mirror interference lithography

TL;DR: A liquid immersion Lloyd's mirror interference lithography system to fabricate subwavelength periodic nanostructures and successfully fabricated a grating structure with 112 nm period using a laser with 325 nm wavelength, attaining a numerical aperture of 1.45.
Proceedings ArticleDOI

Critical-angle transmission grating spectrometer for high-resolution soft x-ray spectroscopy on the International X-ray Observatory

TL;DR: In this article, the authors present the current status of a transmission grating spectrometer based on recently developed high-efficiency critical-angle transmission (CAT) gratings that combine the traditional advantages of blazed and transmission gratings.
Journal ArticleDOI

Plasma etch fabrication of 60:1 aspect ratio silicon nanogratings with 200 nm pitch

TL;DR: In this article, a multistage dry-etch process was used to create 100 nm half-pitch gratings in silicon with depths up to 6μm, which were then used to mask the subsequent deep reactive-ion etching of silicon.
References
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Journal ArticleDOI

X-Ray Interactions: Photoabsorption, Scattering, Transmission, and Reflection at E = 50-30,000 eV, Z = 1-92

TL;DR: In this article, the atomic scattering factors for all angles of coherent scattering and at the higher photon energies are obtained from these tabulated forward-scattering values by adding a simple angle-dependent form-factor correction.
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Fluorescence-guided surgery with 5-aminolevulinic acid for resection of malignant glioma: a randomised controlled multicentre phase III trial.

TL;DR: Tumour fluorescence derived from 5-aminolevulinic acid enables more complete resections of contrast-enhancing tumour, leading to improved progression-free survival in patients with malignant glioma.
Journal ArticleDOI

Looking and listening to light: the evolution of whole-body photonic imaging.

TL;DR: Emphasis is shifting to photonic methods that use tomographic principles to noninvasively image optical contrast at depths of several millimeters to centimeters with high sensitivity and sub-millimeter to millimeter resolution.
Journal ArticleDOI

A diffusion theory model of spatially resolved, steady-state diffuse reflectance for the noninvasive determination of tissue optical properties in vivo

TL;DR: A model based upon steady-state diffusion theory which describes the radial dependence of diffuse reflectance of light from tissues is developed and the optical properties derived for the phantoms are within 5%-10% of those determined by other established techniques.
Journal ArticleDOI

Stable implementation of the rigorous coupled-wave analysis for surface-relief gratings: enhanced transmittance matrix approach

TL;DR: In this paper, an enhanced, numerically stable transmittance matrix approach is developed and is applied to the implementation of the rigorous coupled-wave analysis for surface-relief and multilevel gratings.
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