Journal ArticleDOI
The new Material Science Powder Diffraction beamline at ALBA Synchrotron
TLDR
In this article, the authors describe the installation and preliminary commissioning of the material science powder diffraction (MSPD) beamline at the Spanish synchrotron ALBA-CELLS.Abstract:
The current report describes the installation and the preliminary commissioning of the Material Science Powder Diffraction (MSPD) beamline at the Spanish synchrotron ALBA-CELLS. The beamline is fully dedicated to powder diffraction techniques and consists of two experimental stations positioned in series: a High Pressure/Microdiffraction station and a High Resolution/High Throughput powder diffraction station.read more
Citations
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Towards a calcium-based rechargeable battery
TL;DR: The results presented here constitute the first step towards the development of a new rechargeable battery technology using calcium anodes, and the reversibility of the process on cycling has been ascertained.
Journal ArticleDOI
Comprehensive Investigation of the Na3V2(PO4)2F3–NaV2(PO4)2F3 System by Operando High Resolution Synchrotron X-ray Diffraction
Matteo Bianchini,François Fauth,Nicolas Brisset,François Weill,Emmanuelle Suard,Christian Masquelier,Christian Masquelier,Laurence Croguennec +7 more
TL;DR: In this paper, high angular resolution synchrotron radiation diffraction measurements, realized operando on sodium batteries upon charge, reveal an extremely interesting phase diagram, created by the successive crystallization of four intermediate phases before the end composition NaV2(PO4)2F3 is reached.
Journal ArticleDOI
Na3V2(PO4)2F3 Revisited: A High-Resolution Diffraction Study
Matteo Bianchini,Nicolas Brisset,François Fauth,François Weill,Erik Elkaim,Emmanuelle Suard,Christian Masquelier,Christian Masquelier,Laurence Croguennec +8 more
TL;DR: In this paper, the crystal structure of the high-temperature form of Na3V2(PO4)2F3 (at 400 K) was determined for the first time using very high angular resolution synchrotron radiation diffraction.
Journal ArticleDOI
Beamline P02.1 at PETRA III for High-Resolution and High-Energy Powder Diffraction
Ann-Christin Dippel,Hanns-Peter Liermann,Jan Torben Delitz,Peter Walter,Horst Schulte-Schrepping,Oliver H. Seeck,H. Franz +6 more
TL;DR: By providing the capabilities for high-resolution, high-energy and time-resolved powder X-ray diffraction, beamline P02.1 is a versatile tool to tackle various problems in materials science, crystallography and chemistry.
Journal ArticleDOI
A NASICON-Type Positive Electrode for Na Batteries with High Energy Density: Na4MnV(PO4)3
Fan Chen,Fan Chen,Vadim M. Kovrugin,Vadim M. Kovrugin,Rénald David,Rénald David,Olivier Mentré,François Fauth,Jean-Noël Chotard,Jean-Noël Chotard,Christian Masquelier,Christian Masquelier +11 more
References
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Journal ArticleDOI
Two-dimensional detector software: From real detector to idealised image or two-theta scan
TL;DR: Calibration methods and software have been developed for single crystal diffraction experiments, using both approaches for calibrate, and apply corrections, to obtain accurate angle and intensity information.
Journal ArticleDOI
Calibration of the ruby pressure gauge to 800 kbar under quasi-hydrostatic conditions
TL;DR: An improved calibration curve of the pressure shift of the ruby R1 emission line was obtained under quasi-hydrostatic conditions in the diamond-window, high-pressure cell to 800 kbar.
Journal ArticleDOI
Hydrostatic limits of 11 pressure transmitting media
TL;DR: In this paper, the authors present a systematic and comparative study of the pressure-induced solidification of 11 frequently used pressure transmitting fluids using the ruby fluorescence technique in a diamond anvil cell.
Journal ArticleDOI
The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source
Anna Bergamaschi,Antonio Cervellino,Roberto Dinapoli,Fabia Gozzo,B. Henrich,Ian Johnson,P. Kraft,Aldo Mozzanica,Bernd Schmitt,Xintian Shi +9 more
TL;DR: A report on the characterization, calibration and performances of the MYTHEN photon-counting silicon microstrip detector at the powder diffraction station at the Swiss Light Source is given.
Journal ArticleDOI
New diamond cell for single-crystal x-ray diffraction
TL;DR: In this paper, a diamond cell conical diamond anvils with an x-ray aperture of 85° were successfully tested to over 50GPa using helium as a pressure medium.