Showing papers on "Flexural strength published in 2007"

Mechanical Properties of Steel Fiber-Reinforced Concrete

Abstract: This paper presents the results from an experimental program and an analytical assessment of the influence of addition of fibers on mechanical properties of concrete. Models derived based on the regression analysis of 60 test data for various mechanical properties of steel fiber-reinforced concrete have been presented. The various strength properties studied are cube and cylinder compres- sive strength, split tensile strength, modulus of rupture and postcracking performance, modulus of elasticity, Poisson's ratio, and strain corresponding to peak compressive stress. The variables considered are grade of concrete, namely, normal strength 35 MPa, moderately high strength 65 MPa, and high-strength concrete 85 MPa, and the volume fraction of the fiber Vf=0.0, 0.5, 1.0, and 1.5%. The strength of steel fiber-reinforced concrete predicted using the proposed models have been compared with the test data from the present study and with various other test data reported in the literature. The proposed model predicted the test data quite accurately. The study indicates that the fiber matrix interaction contributes significantly to enhancement of mechanical properties caused by the introduction of fibers, which is at variance with both existing models and formulations based on the law of mixtures. 85 MPa with various fiber dosages Vf=0, 0.5, 1.0, and 1.5%. An empirical relationship for various mechanical properties of SFRC has been proposed. The proposed model attempts to bring out the significance of fiber matrix interaction in all the strength properties. This study reports the experimental results of the strength properties of SFRC, namely, cube and cylinder compressive strength, split tensile strength, modulus of rupture, modulus of elasticity, Poisson's ratio, and strain corresponding to peak com- pressive stress. Empirical relationships were developed for vari- ous strength properties based on the regression analysis of the 60 test data. It is expected that these proposed models would be helpful in assessing the strength properties of fiber-reinforced concrete based on the matrix strength and fiber-RI.

Mechanical properties of wood–fiber reinforced polypropylene composites: Effect of a novel compatibilizer with isocyanate functional group

Abstract: Natural fibers are increasingly being used as reinforcement in commercial thermoplastics due to their low cost, high specific properties and renewable nature. While the maleic anhydride modified polypropylene (MAPP) is most commonly used as compatibilizer to improve interfacial adhesion between hydrophilic wood–fibers and hydrophobic polypropylene, in this study, a novel compatibilizer (m-TMI-g- PP) with isocyanate functional group was synthesized by grafting m-isopropenyl-\alpha,\alpha-dimethylbenzyl-isocyanate (m-TMI) onto isotactic polypropylene (PP) in a twin screw extruder. The effect of filler concentration on the mechanical properties of wood–fiber filled composites, prepared by using m-TMI-g-PP as the compatibilizer, was investigated. The addition of the compatibilizer resulted in greater reinforcement of composites, as indicated by the improvement in mechanical properties. Tensile strength of composites so prepared increased by almost 45%, whereas 85% increase in flexural properties was observed. However the addition of wood–fibers resulted in a decrease in elongation at break and impact strength of the composites.

Bioinspired self-healing of advanced composite structures using hollow glass fibres.

Abstract: Self-healing is receiving an increasing amount of worldwide interest as a method to autonomously address damage in materials. The incorporation of a self-healing capability within fibre-reinforced polymers has been investigated by a number of workers previously. The use of functional repair components stored inside hollow glass fibres (HGF) is one such bioinspired approach being considered. This paper considers the placement of self-healing HGF plies within both glass fibre/epoxy and carbon fibre/epoxy laminates to mitigate damage occurrence and restore mechanical strength. The study investigates the effect of embedded HGF on the host laminates mechanical properties and also the healing efficiency of the laminates after they were subjected to quasi-static impact damage. The results of flexural testing have shown that a significant fraction of flexural strength can be restored by the self-repairing effect of a healing resin stored within hollow fibres.

Mechanical properties and durability of mortar and concrete containing natural pozzolana and limestone blended cements

Abstract: The benefits of limestone filler (LF) and natural pozzolana (NP) as partial replacement of Portland cement are well established. Economic and environmental advantages by reducing CO2 emission are well known. However, both supplementary materials have certain shortfalls. LF addition to Portland cement causes an increase of hydration at early ages inducing a high early strength, but it can reduce the later strength due to the dilution effect. On the other hand, NP contributes to hydration after 28 days improving the strength at medium and later ages. Hence, ternary blended cement (OPC–LF–NP) with better performance could be produced. In this paper, mortar prisms in which Portland cement was replaced by up to 20%LF and 30%NP were tested in flexure and compressive strength at 2, 7, 28 and 90 days. Some samples were tested under sulfate and acid solutions and for chloride ions permeability. Results show that the use of ternary blended cement improves the early age and the long-term compressive and flexural strengths. Durability was also enhanced as better sulfate, acid and chloride ions penetration resistances were proved. (A) “Reprinted with permission from Elsevier”.

Mechanical properties and morphological characterization of exfoliated graphite–polypropylene nanocomposites

Abstract: This research explores the potential of using exfoliated graphite nanoplatelets, xGnP, (graphene sheets ∼10 nm thickness, ∼1 μm diameter), as reinforcement in polypropylene, PP. xGnP–PP nanocomposites were fabricated by melt mixing and injection molding. The feasibility of using xGnP–PP nanocomposites was investigated by evaluating the flexural strength, modulus and impact strength and studying the morphology of this system as a function of xGnP loading and aspect ratio and by comparing the xGnP–PP with composites made with commercial available reinforcements such as carbon fibers, carbon black and clays. It is concluded that the smaller aspect ratio xGnP has the strongest impact on the mechanical properties of PP, at loadings up to 5 vol.%, compared to the other reinforcements used, which reflects the compatibility between the exfoliated graphite nanoplatelets and the PP matrix and the exceptional mechanical properties of xGnP, similar to crystalline graphite.

Injection-molded short hemp fiber/glass fiber-reinforced polypropylene hybrid composites—Mechanical, water absorption and thermal properties

Abstract: Natural fiber-based thermoplastic composites are generally lower in strength performance compared to thermoset composites. However, they have the advantage of design flexibility and recycling possibilities. Hybridization with small amounts of synthetic fibers makes these natural fiber composites more suitable for technical applications such as automotive interior parts. Hemp fiber is one of the important lignocellulosic bast fiber and has been used as reinforcement for industrial applications. This study focused on the performance of injection-molded short hemp fiber and hemp/glass fiber hybrid polypropylene composites. Results showed that hybridization with glass fiber enhanced the performance properties. A value of 101 MPa for flexural strength and 5.5 GPa for the flexural modulus is achieved from a hybrid composite containing 25 wt % of hemp and 15 wt % of glass. Notched Izod impact strength of the hybrid composites exhibited great enhancement (34%). Analysis of fiber length distribution in the composite and fracture surface was performed to study the fiber breakage and fracture mechanism. Thermal properties and resistance to water absorption properties of the hemp fiber composites were improved by hybridization with glass fibers. Overall studies indicated that the short hemp/glass fiber hybrid polypropylene composites are promising candidates for structural applications where high stiffness and thermal resistance is required. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 2432–2441, 2007

Mechanical properties of high strength concrete reinforced with metallic and non-metallic fibres

Abstract: This paper focuses on the experimental investigation carried out on high strength concrete reinforced with hybrid fibres (combination of hooked steel and a non-metallic fibre) up to a volume fraction of 0.5%. The mechanical properties, namely, compressive strength, split tensile strength, flexural strength and flexural toughness were studied for concrete prepared using different hybrid fibre combinations – steel–polypropylene, steel–polyester and steel–glass. The flexural properties were studied using four point bending tests on beam specimens as per Japanese Concrete Institute (JCI) recommendations. Fibre addition was seen to enhance the pre-peak as well as post-peak region of the load–deflection curve, causing an increase in flexural strength and toughness, respectively. Addition of steel fibres generally contributed towards the energy absorbing mechanism (bridging action) whereas, the non-metallic fibres resulted in delaying the formation of micro-cracks. Compared to other hybrid fibre reinforced concretes, the flexural toughness of steel–polypropylene hybrid fibre concretes was comparable to steel fibre concrete. Increased fibre availability in the hybrid fibre systems (due to the lower densities of non-metallic fibres), in addition to the ability of non-metallic fibres to bridge smaller micro cracks, are suggested as the reasons for the enhancement in mechanical properties.

Fabrication and Mechanical Properties of Completely Biodegradable Hemp Fiber Reinforced Polylactic Acid Composites

Abstract: Biodegradable composite materials can be produced by the combination of biodegradable polymers and natural fibers. In this study, a new biodegradable composite of hemp fiber reinforced polylactic acid (PLA) was fabricated using the hot press method. Mechanical properties of composites with different fiber volume fractions were tested. The optimum fiber content was determined according to the test results. Effects of alkali treatment on the fiber surface morphology and the mechanical properties of the composites were investigated. Test results show that the composite with 40% volume fraction of alkali treated fiber has the best mechanical properties. The tensile strength, elastic modulus, and flexural strength of the composite with 40% treated fiber are 54.6 MPa, 8.5 Gpa, and 112.7 MPa respectively, which are much higher than those of PLA alone. The composites have lower densities, which were measured to be from 1.19 g/cm3 to 1.25 g/cm3. Specific strengths were also calculated. Surface morphologies of fibe...

Mode I interlaminar fracture behavior and mechanical properties of CFRPs with nanoclay-filled epoxy matrix

Abstract: The mechanical properties and fracture behavior of nanocomposites and carbon fiber composites (CFRPs) containing organoclay in the epoxy matrix have been investigated. Morphological studies using TEM and XRD revealed that the clay particles within the epoxy resin were intercalated or orderly exfoliated. The organoclay brought about a significant improvement in flexural modulus, especially in the first few wt% of loading, and the improvement of flexural modulus was at the expense of a reduction in flexural strength. The quasi-static fracture toughness increased, whereas the impact fracture toughness dropped sharply with increasing the clay content. Flexural properties of CFRPs containing organoclay modified epoxy matrix generally followed the trend similar to the epoxy nanocomposite although the variation was much smaller for the CFRPs. Both the initiation and propagation values of mode I interlaminar fracture toughness of CFRP composites increased with increasing clay concentration. In particular, the propagation fracture toughness almost doubled with 7 wt% clay loading. A strong correlation was established between the fracture toughness of organoclay-modified epoxy matrix and the CFRP composite interlaminar fracture toughness.

Strength properties of thermally modified softwoods and its relation to polymeric structural wood constituents

Abstract: Thermal modification at relatively high temperatures (ranging from 150 to 260 °C) is an effective method to improve the dimensional stability and resistance against fungal attack. This study was performed to investigate the impact of heat treatment on the mechanical properties of wood. An industrially-used two-stage heat treatment method under relative mild conditions (< 200 °C) was used to treat the boards. Heat treatment revealed a clear effect on the mechanical properties of softwood species. The tensile strength parallel to the grain showed a rather large decrease, whereas the compressive strength parallel to the fibre increased after heat treatment. The bending strength, which is a combination of the tensile stress, compressive stress and shear stress, was lower after heat treatment. This decrease was less than the decrease of only the tensile strength. The impact strength showed a rather large decrease after heat treatment. An increase of the modulus of elasticity during the bending test has been noticed after heat treatment. Changes and/or modifications of the main wood components appear to be involved in the effects of heat treatment on the mechanical properties. The possible effect of degradation and modification of hemicelluloses, degradation and/or crystallization of amorphous cellulose, and polycondensation reactions of lignin on the mechanical properties of heat treated wood have been discussed. The effect of natural defects, such as knots, resin pockets, abnormal slope of grain and reaction wood, on the strength properties of wood appeared to be affected by heat treatment. Nevertheless, heat treated timber shows potential for use in constructions, but it is important to carefully consider the stresses that occur in a construction and some practical consequences when heat treated timber is used.

A concise interface constitutive law for analysis of delamination and splitting in composite materials and its application to scaled notched tensile specimens

Abstract: A concise constitutive law for cohesive interfaces is proposed in this paper. A new state variable is introduced to track the extent of damage accumulated at the interface. The constitutive equations not only account for mixed-mode delamination propagation in composite materials, but also satisfactorily deal with mode ratio change during the debonding process. The interface model is implemented in the LS-DYNA explicit finite element code. The model has been applied to scaled open hole tension tests on laminated composite material. Comparison between numerical results and experiments shows good correlation for failure modes and strengths for a range of different specimen sizes. Copyright © 2006 John Wiley & Sons, Ltd.

Efficacy of CFRP-based techniques for the flexural and shear strengthening of concrete beams

Abstract: Near surface mounted (NSM) and externally bonded reinforcement (EBR) strengthening techniques are based on the use of carbon fiber reinforced polymer (CFRP) materials and have been used for the structural rehabilitation of concrete structures. In the present work, the efficacies of the NSM and EBR techniques for the flexural and shear strengthening of reinforced concrete beams are compared carrying out two experimental groups of tests. For the flexural strengthening, the efficacy of applying CFRP laminates according to NSM is compared to those resulting from applying CFRP laminates and wet lay-up CFRP sheets according to EBR technique. The influences of the equivalent reinforcement ratio (steel and laminates) and spacing of the laminates on the efficiency of the NSM technique for the flexural strengthening is also investigated. A numerical strategy is implemented to analyze the applicability of the FRP effective strain concept, proposed by ACI and fib in the design of FRP systems for the flexural strengthening. To assess the efficacy of the NSM technique for the shear strengthening of concrete beams, four beam series of distinct depth and longitudinal tensile steel reinforcement ratio are tested. Each series is composed of one beam without any shear reinforcement and one beam using the following shear reinforcing systems: conventional steel stirrups; strips of wet lay-up CFRP sheet of U configuration applied according to EBR technique; and laminates of CFRP embedded into vertical or inclined (45°) pre-cut slits on the concrete cover of the beam lateral faces, according to the NSM technique. Using the obtained experimental results, the performance of the analytical formulations proposed by ACI, fib and Italian guidelines is appraised.

Experimental study on the thermal and mechanical properties of multi-walled carbon nanotube-reinforced epoxy

Abstract: In this study, multi-walled carbon nanotubes (CNTs) were infused into Epon 862 epoxy through a high intensity ultrasonic liquid processor and then mixed with EpiCure curing agent W using a high-speed mechanical agitator. The trapped air and reaction volatiles were removed from the mixture using a high vacuum. Dynamic mechanical analysis (DMA), thermogravimetric analysis (TGA), and flexural tests were performed on unfilled, 0.1, 0.2, 0.3, and 0.4 wt% CNT-filled epoxy to identify the loading effect on the thermal and mechanical properties of composites. DMA studies revealed that filling the carbon nanotube into epoxy can produce a 90% enhancement in storage modulus and a 22 °C increase in Tg. However, due to the lower crosslink density of the nanophased systems, a 6 °C decrease in decomposition temperature was observed in the 0.4 wt% CNT/epoxy in the TGA test. The flexural results showed that modulus increased with higher CNT loading percentages and the 0.3 wt% CNT-infusion system showed the maximum strength enhancement. Based on the experiment's results, a nonlinear constitutive equation was established for neat and nanophased epoxy.

Effect of hot pressing time and temperature on the microstructure and mechanical properties of ZrB2-SiC

Abstract: Structure–property relations were examined for ZrB2 containing 30 volume percent SiC particulates. Two grades of ZrB2 with initial particle sizes of 2 and 6 μm were used. Billets of ZrB2–SiC were produced by hot pressing at 1850, 1950 or 2050 °C for 45 min. In addition, the material prepared from ZrB2 with an initial particle size of 2 μm was hot pressed at 2050 °C for 90 and 180 min. Microstructures and mechanical properties were characterized to determine the effects of the initial particle size, hot pressing time, and hot pressing temperature on the final grain size and morphology. The average grain size of the ZrB2 phase ranged from 2.2 to 4.7 μm. Similarly, the average grain size of the SiC phase ranged from 1.2 to 2.7 μm. Hardness and modulus of elasticity were not affected by the processing conditions with average values of 22 and 505 GPa, respectively. However, flexural strength decreased as grain size increased from a maximum of ∼1050 MPa for the finest grain sizes to ∼700 MPa for the largest grain sizes. Analysis suggested that the strength of ZrB2–SiC was limited by the size of the SiC inclusions in the ZrB2 matrix.

Flexural strength and fracture toughness of dental core ceramics.

Abstract: Statement of problem Many different strengthened all-ceramic core materials are available. In vitro study of their mechanical properties, such as flexural strength and fracture toughness, is necessary before they are used clinically. Purpose The purpose of this study was to evaluate and compare the mechanical properties of 6 commonly used all-ceramic core materials using biaxial flexural strength and indentation fracture toughness tests. Material and methods Specimens of 6 ceramic core materials (Finesse, Cergo, IPS Empress, In-Ceram Alumina, In-Ceram Zirconia, and Cercon Zirconia) were fabricated (n=25) with a diameter of 15 mm and width of 1.2 ± 0.2 mm. For each group, the specimens were tested to compare their biaxial flexural strength (piston on 3 balls) (n=15), Weibull modulus, and indentation fracture toughness (n=10) (IF method). The data were analyzed with 1-way ANOVA test (a=.05). The Tamhane multiple comparison test was used for post hoc analysis. Results Mean (SD) of biaxial flexural strength values (MPa) and Weibull modulus ( m ) results were: Finesse (F): 88.04 (31.61), m =3.17; Cergo (C): 94.97 (13.62), m =7.94; IPS Empress (E): 101.18 (13.49), m =10.13; In-Ceram Alumina (ICA): 341.80 (61.13), m =6.96; In-Ceram Zirconia (ICZ): 541.80 (61.10), m =10.17; and Cercon Zirconia (CZ): 1140.89 (121.33), m =13.26. The indentation fracture toughness results showed that there were significant differences between the tested ceramics. The highest fracture toughness values (MPa × m 0.5 ) were obtained with the zirconia-based ceramic core materials. Conclusions Significant differences were found in strength and toughness values of the materials evaluated. Cercon Zirconia core material showed high values of biaxial flexural strength and indentation fracture toughness when compared to the other ceramics studied.

The effect of silane treated-and untreated-talc on the mechanical and physico-mechanical properties of poly(lactic acid)/newspaper fibers/talc hybrid composites

Abstract: This paper evaluates the effect of the addition of silane treated- and untreated- talc as the fillers on the mechanical and physico-mechanical properties of poly(lactic acid) (PLA)/recycled newspaper cellulose fibers (RNCF)/talc hybrid composites. For this purpose, 10 wt% of a talc with and without silane treatment were incorporated into PLA/RNCF (60 wt%/30 wt%) composites that were processed by a micro-compounding and molding system. PLA is utilized is a bio-based polymer that made from dextrose, a derivative of corn. Talc is also a natural product. The RNCF and talc hybrid reinforcements of PLA polymer matrix were targeted to design and engineer bio-based composites of balanced properties with added advantages of cost benefits besides the eco-friendliness of all the components in the composites. In this work, the flexural and impact properties of PLA/RNCF composites improved significantly with the addition of 10 wt% talc. The flexural and impact strength of these hybrid composites were found to be significantly higher than that made from either PLA/RNCF. The hybrid composites showed improved properties such as flexural strength of 132 MPa and flexural modulus of 15.3 GPa, while the unhybridized PLA/RNCF based composites exhibited flexural strength and modulus values of 77 MPa and 6.7 GPa, respectively. The DMA storage modulus and the loss modulus of the PLA/RNCF hybrid composites were found to increase, whereas the mechanical loss factor (tan delta) was found to decrease. The storage modulus increased with the addition of talc, because the talc generated a stiffer interface in the polymer matrix. Differential scanning calorimetry (DSC) thermograms of neat PLA and of the hybrid composites showed nearly the similar glass transition temperatures and melting temperatures. Scanning electron microscopy (SEM) micrographs of the fracture surface of Notched Izod impact specimen of 10 wt% talc filled PLA/RNCF composite showed well filler particle dispersion in the matrix and no large aggregates are present. The comparison data of mechanical properties among samples filled with silane-treated- and untreated- talc fillers showed that the hybrid composites filled with silane treated talc displayed the better mechanical prosperities relative to the other hybrid composites. Talc-filled RNCF-reinforced polypropylene (PP) hybrid composites were also made in the same way that of PLA hybrid composites for a comparison. The PLA hybrid bio-based composites showed much improvement in mechanical properties as compared to PP-based hybrid counterparts. This suggests that these PLA hybrid bio-based composites have a potential to replace glass fibers in many applications that do not require very high load bearing capabilities and these recycled newspaper cellulose fibers could be a good candidate reinforcement fiber of high performance hybrid biocomposites.

Resistance to Thermal Shock and to Oxidation of Metal Diborides–SiC Ceramics for Aerospace Application

Abstract: Two SiC-containing metal diborides materials, classified in the ultra-high-temperature ceramics (UHTCs) group, were fabricated by hot-pressing. SiC, sinterability apart, promoted resistance to oxidation of the diboride matrices. Both the compositions, oxidized in air at 1450°C for 1200 min, had mass gains lower than 5 mg/cm2. Slight deviations from parabolic oxidation kinetics were seen. The resistance to thermal shock (TSR) was studied through the method of the retained flexure strength after water quenching (20°C of bath temperature). Experimental data showed that the (ZrB2+HfB2)–SiC and the ZrB2–SiC materials retained more than 70% of their initial mean flexure strength for thermal quenchs not exceeding 475° and 385°C, respectively. Certain key TSR properties (i.e., fracture strength and toughness, elastic modulus, and thermal expansion coefficient) are very similar for the two compositions. The observed superior critical thermal shock of the (ZrB2+HfB2)–SiC composite was explained in terms of more favorable heat transfer parameters conditions that induce less severe thermal gradients across the specimens of small dimensions (i.e., bars 25 mm × 2.5 mm × 2 mm) during the quench down in water. The experimental TSRs are expected to approach the calculated R values (196° and 218°C for ZrB2+HfB2–SiC and ZrB2–SiC, respectively) as the specimen size increases.