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Journal ArticleDOI

Electron tomography and holography in materials science

TLDR
An overview of the techniques of electron tomography and electron holography is presented and their capabilities with the aid of case studies that span materials science and the interface between the physical sciences and the life sciences are demonstrated.
Abstract
The rapid development of electron tomography, in particular the introduction of novel tomographic imaging modes, has led to the visualization and analysis of three-dimensional structural and chemical information from materials at the nanometre level. In addition, the phase information revealed in electron holograms allows electrostatic and magnetic potentials to be mapped quantitatively with high spatial resolution and, when combined with tomography, in three dimensions. Here we present an overview of the techniques of electron tomography and electron holography and demonstrate their capabilities with the aid of case studies that span materials science and the interface between the physical sciences and the life sciences.

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Citations
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Journal ArticleDOI

Synthesis of MoS2 and MoSe2 Films with Vertically Aligned Layers

TL;DR: This communication presents a synthesis process to grow MoS2 and MoSe2 thin films with vertically aligned layers, thereby maximally exposing the edges on the film surface, and confirmed their catalytic activity in a hydrogen evolution reaction (HER), in which the exchange current density correlates directly with the density of the exposed edge sites.
Journal ArticleDOI

Three-dimensional optical holography using a plasmonic metasurface

TL;DR: Huang et al. as mentioned in this paper developed ultrathin plasmonic metasurfaces to provide 3D optical holographic image reconstruction in the visible and near-infrared regions for circularly polarized light.
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Towards stable catalysts by controlling collective properties of supported metal nanoparticles

TL;DR: This work presents an alternative strategy based on control over collective properties, revealing the pronounced impact of the three-dimensional nanospatial distribution of metal particles on catalyst stability and paves the way towards the rational design of practically relevant catalysts and other nanomaterials with enhanced stability and functionality.
Journal ArticleDOI

Coherent X-ray diffraction imaging of strain at the nanoscale.

TL;DR: New X-ray diffraction techniques, which take advantage of the latest synchrotron radiation sources, can be used to obtain quantitative three-dimensional images of strain, leading to new knowledge of how nanomaterials behave within active devices and on unprecedented timescales.
Journal ArticleDOI

Three-dimensional atomic imaging of crystalline nanoparticles

TL;DR: 3D reconstruction of a complex crystalline nanoparticle at atomic resolution is reported, which helps close the gap between the atomic resolution achievable in two-dimensional electron micrographs and the coarser resolution that has hitherto been obtained by conventional electron tomography.
References
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Journal ArticleDOI

Microscopy by reconstructed wave-fronts

TL;DR: In this paper, it is shown that a coherent monochromatic wave can be used to reconstruct the original image of an object from its mirror image with respect to the coherent background.
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The Reconstruction of a Three-Dimensional Structure from Projections and its Application to Electron Microscopy

TL;DR: In this paper, the Fourier transform is used to combine data from a number of different views of a transmission electron micrograph to reconstruct a 3D image of a given particle to a given degree of resolution.
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3D electron microscopy in the physical sciences: the development of Z-contrast and EFTEM tomography

TL;DR: Examples of how STEM dark-field imaging and energy-filtered TEM can be used successfully to examine nearly all types of specimens likely to be encountered by the physical scientist are presented.
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Soft X-ray microscopy at a spatial resolution better than 15 nm

TL;DR: The achievement of sub-15-nm spatial resolution with a soft X-ray microscope—and a clear path to below 10 nm—using an overlay technique for zone plate fabrication is reported.
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Evidence for Aharonov-Bohm effect with magnetic field completely shielded from electron wave.

TL;DR: Evidence for the Aharonov-Bohm effect was obtained with magnetic fields shielded from the electron wave, and direct evidence for flux quantization also was given.
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