Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Preparation of 1,6‐anhydroglucose from (1→4)‐glucans using microwave technology
TL;DR: In this paper, the authors show that heating of starch or other (14)-glucans in a conventional microwave oven yields 1,6-anhydro-β-D-glucopyranose within a few minutes.
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Green synthetic strategy of BCNO nanostructure and phosphor-based light – Emitting diodes
TL;DR: In this paper, the authors obtained BCNO nano-particle phosphor by microwave treating from boric acid, urea, and glucose at low temperatures and in short reaction time.
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Synthesis, physico-chemical properties and complexing abilities of new amphiphilic ligands from D-galacturonic acid
TL;DR: A convenient and efficient synthesis of new complexing surfactants from d-galacturonic acid and n-octanol as renewable raw materials in a two-step sequence is described.
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A re-entrant cavity for microwave-enhanced chemistry.
TL;DR: It is concluded that a re-entrant cavity may supply high electric field component that is theoretically favorable efficient microwave absorption process in a small liquid or solid chemical sample.
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Practical and Scalable Organic Reactions with Flow Microwave Apparatus.
TL;DR: This paper demonstrates the scale-up of fundamental organic reactions using a novel flow microwave system developed by the academic-industrial alliance between the University of Shizuoka, Advanced Industrial Science and Technology, and SAIDA FDS using the SAIDA flow microwave apparatus.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.