Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Size Control and Photophysical Properties of Quantum Dots Prepared via a Novel Tunable Hydrothermal Route
TL;DR: In this paper, the authors used a synthetic microwave reactor for dielectric heating that provides both kinetic control, and in situ monitoring of temperature and pressure, and showed the ability to fabricate highly emissive CdSe/CdS/ZnS qdots under fine-tuned hydrothermal conditions.
Patent
Carbon Nanotube Mediated Membrane Extraction
Kamilah Hylton,Somenath Mitra +1 more
TL;DR: In this paper, an improved membrane or substrate having carbon nanotubes introduced and/or immobilized therein, and an improved method for introducing and or immobilizing carbon Nanotubes in membranes or substrates is presented.
Journal ArticleDOI
The use of a microwave oven in the chemical transformation of long chain fatty acid esters
TL;DR: The use of microwaves not only decreased the reaction time considerably but also allowed smaller volumes of solvent and lower quantities of reagents to be used as compared with the conventional methodologies reported.
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Microwave Irradiation Plus Solid-Liquid Phase Transfer Catalysis Without Solvent: Further Improvement in Anionic Activation
TL;DR: In this paper, conditions for alkylations of potassium acetate by n-octyl or n-cetyl halides are nearly quantitative within 2 minutes on appreciable quantities.
Journal ArticleDOI
Microwave synthesis, characterization, and electrochemical properties of α-Fe2O3 nanoparticles
TL;DR: In this paper, the authors synthesized α-Fe2O3 nanoparticles with an extremely narrow distribution by microwave heating and showed that most primary particles have ellipsoid shapes, and the average diameter of the primary particles was less than 10nm.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.