Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Microwave‐Assisted Synthesis under Continuous‐Flow Conditions
Toma N. Glasnov,C. Oliver Kappe +1 more
TL;DR: The state of the art in microwave-assisted chemistry is summarized in this paper, where the authors present an overview of microwave assisted synthesis using continuous-flow and stop-flow processing in custom-built or commercially available microwave reactors.
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Solvent-free and catalysts-free chemistry: a benign pathway to sustainability.
TL;DR: An overview of benign reactions through solvent- and catalyst-free (SF-CF) chemistry and a critical perspective on emerging synergies between SF-CF organic reactions are discussed.
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Kontrolliertes Erhitzen mit Mikrowellen in der modernen organischen Synthese
TL;DR: In den vergangenen Jahren ist das Erhitzen and Beschleunigen chemischer Reaktionen durch Mikrowellenenergie popular geworden as discussed by the authors.
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Microwave hydrodiffusion and gravity, a new technique for extraction of essential oils.
TL;DR: The essential oils extracted by MHG were quantitatively and qualitatively similar to those obtained by conventional hydrodistillation for 90 min, and prevents pollution through potential 90% of energy saved which can lead to greenhouse gas emission benefits.
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Rapid and amenable suzuki coupling reaction in water using microwave and conventional heating.
TL;DR: It is possible to prepare biaryls in good yield very rapidy on small and larger scales from aryl halides and phenylboronic acid using water as a solvent and palladium acetate as catalyst.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.