Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Journal ArticleDOI
Preparation and Magnetic Properties of La-Substituted Strontium Hexaferrite by Microwave-Assisted Sol-Gel Method
TL;DR: In this article, the thermal decomposition process, structural, and magnetic properties of the products were studied by thermal differential scanning calorimeter (DSC), thermogravimetry (TG), X-ray diffraction (XRD), and vibrating sample magnetometer (VSM).
Journal ArticleDOI
Lewis acid catalysed microwave-assisted synthesis of diaryl sulfones and comparison of associated carbon dioxide emissions
TL;DR: In this article, a variety of Lewis acid catalysts were used under microwave activation to synthesize diaryl sulfones, and the most effective catalyst in terms of yield was found to be iron(III) chloride with a yield of 89%. Supported iron-III-closest to the 4,4′ isomer was obtained using supported bismuth-III chloride.
Book ChapterDOI
From Field to Shelf: How Microwave-Assisted Extraction Techniques Foster an Integrated Green Approach
TL;DR: In this article, a comprehensive review of microwave-assisted extraction of organic compounds from vegetal matrixes is presented, where microwave heating is coupled with other techniques, like ultrasounds, and indicating new paths, where the recent advent of new microwave solid-state generators has led to better process control and higher yields and energy efficiency.
Book ChapterDOI
Recent Advancement of Catalytic Pauson-Khand-type Reactions
Journal ArticleDOI
Nanoporous Solid Acid Catalyst for the Diels-Alder Reaction of 1,3-Dienes with Acrylates.
TL;DR: Nanoporous aluminosilicate, Al-HMS with a high aluminum content, strong acidity, and nanoporosity was found to catalyze the Diels-Alder reaction of 1,3-dienes with methacrylate and acrylate, and turned out to be a green alternative to homogeneous acid catalysts as mentioned in this paper.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
Journal ArticleDOI
The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.