Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Discovery of Small Peptides and Peptidomimetics Targeting the Substance P 1-7 Binding Site : Focus on Design, Synthesis, Structure-Activity Relationships and Drug-Like Properties
TL;DR: Biologically active peptides are important for many physiological functions in the human body and therefore serve as interesting starting points in drug discovery processes.
Journal ArticleDOI
Combustion enhancement by microwave superposition on Methane-Air premixed flame
Journal ArticleDOI
A RAPID SYNTHESIS OF ALKYL α-CYANOACETYL GLYCOLATES UNDER MICROWAVE IRRADIATION IN DRY MEDIUM
Cunde Wang,Hui Zhang +1 more
TL;DR: Alkyl α-cyanoacetyl glycolates (3) were effectively synthesized in few minutes by reaction of alkyl chloroacetates with sodium cyanoacetate absorbed on silica gel in the presence of tetrabutylammonium bromide under microwave irradiation without solvent as mentioned in this paper.
Journal ArticleDOI
Bis(phenyl-β-diketonato)titanium(IV) ethoxide complexes: Ring-opening polymerization of l-lactide by solvent-free microwave irradiation
TL;DR: In this article, a range of functionalized bis(phenyl-β-diketonato)titanium(IV) ethoxide complexes of the type [Ti(L)2(OEt)2], containing two asymmetric or symmetric phenyl-α-dikketonate ligands (L), have been synthesized and fully characterized.
Book ChapterDOI
Microwave-induced synthesis of steroids and their chemical manipulations
Preetismita Borah,Bimal K. Banik +1 more
TL;DR: Microwave (MW)-assisted chemical reactions are currently gaining considerable importance in steroid synthesis to contribute to green technology and hybrid systems in recent times are drawing considerable attention in the area of drug development.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.