Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
Reads0
Chats0
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
More filters
Book ChapterDOI
Solvent-free Reactions
TL;DR: A comprehensive review of solvent-free methods for microwave activation can be found in this article with microwave activation as a beneficial alternative to conventional heating under safe and efficient conditions with large enhancements in yields and savings in time.
Journal ArticleDOI
A simple continuous flow microwave reactor
TL;DR: A new simple procedure for microwave-assisted organic synthesis under continuous flow processing has been developed for use in a monomodal microwave synthesizer with direct temperature control using the instrument's in-built IR sensor.
Journal ArticleDOI
Aqueous hydrotrope solution as a safer medium for microwave enhanced hantzsch dihydropyridine ester synthesis
TL;DR: In this article, the first Hautzsch esters were prepared by condensing alkyl β-aminoerotonate, aldehyde and alkyls acetoacetate in aqueous sodium butylmonoglycolsulphate (NaBMGS) as a safe reaction medium in an unmodified domestic microwave oven.
Journal ArticleDOI
Advances in biomass transformation to 5-hydroxymethylfurfural and mechanistic aspects
TL;DR: In this paper, a review of 5-hydroxymethylfurfural (HMF) production from cellulose and lignocelluloses and mechanistic aspects of HMF formation is presented to bridge the gap in understanding the factors responsible for selective conversion and selection of catalyst.
References
More filters
Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
Journal ArticleDOI
The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
Journal ArticleDOI
Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.