Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
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Microwave specific effect on catalytic atropo-enantioselective ring-opening reaction of biaryl lactones
TL;DR: In this article, the microwave specific effect on the catalytic atropo-enantioselective ring-opening reaction of biaryl lactones was investigated and it was shown that the reaction was accelerated by microwave irradiation without any loss of the enanti-lectivity.
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Synthesis of Medicinally Important Quinazolines and Their Derivatives: A Review
TL;DR: In this article, a review article has focused on the synthesis of medicinally important quinazolines and their derivatives, which produce reaction products in less time with high yields, including more attention with eco-friendly green synthesis approaches incorporating multicomponent reactions (MCR), ionic liquids and microwave irradiations.
Journal ArticleDOI
Racemization of (−)-Vincadifformine Using Microwave Oven
TL;DR: In this article, a microwave oven has been used to accelerate the cycloaddition of (−)-vincamine in DMF, which brought about total racemization via concurrent Diels-Alder cycloreversion and cycloadding.
Development of benign synthesis of some terminal α-hydroxy ketones and aldehydes
TL;DR: In this paper, the synthesis of α-hydroxy aldehydes and hydroxymethyl ketones as well as their interconversion to each other are discussed in this thesis.
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Gram-scale synthesis of the p38α MAPK-inhibitor VX-745 for preclinical studies into Werner syndrome
Mark C. Bagley,Terence Davis,Matthew C. Dix,Vincenzo Fusillo,Morgane Pigeaux,Michal Jaroslaw Rokicki,David Glyn Kipling +6 more
TL;DR: This method delivers the p38 inhibitor VX-745 in sufficient quantities for preclinical studies to rescue the aging phenotype in Werner syndrome.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.