Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Microwave Field Applicator Design in Small-Scale Chemical Processing
TL;DR: In this paper, the authors explore the possibilities to apply a microwave field in micro-structured reactor systems, and demonstrate the feasibility of long residence time continuous flow processing under microwave activation in a novel reactor type that the rectangular waveguide uniquely supports.
Journal ArticleDOI
Conductive carbon tape as a sample platform for microwave-based MALDI MS detection of proteins and phosphoproteins
TL;DR: A novel microwave-assisted protein preparation and digestion method for matrix-assisted laser desorption/ionization (MALDI) time-of-flight mass spectrometry analysis and identification of proteins that involves using conductive carbon tape as a sample platform for sample prepared and digestion under microwave heating and as a plate for MALDI analysis.
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Recent Progress in Microwave-assisted Modification of Vegetable Oils or Their Derivatives
Zhang Jinshuai,Hu Yun,Zhang Fei,Lu Jianyu,Huang Jia,Liu Chengguo,Jia Puyou,Hu Lihong,An Rongrong,Zhou Yonghong +9 more
TL;DR: In this article, the authors summarized recent advances on microwave-assisted modification of vegetable oils or their derivatives, such as esterification of free fatty acids, transesterification of triglycerides, epoxidation, and polymerization.
Journal ArticleDOI
Design of a capacity-enhanced single-mode reactor for microwave chemistry researches
TL;DR: In this paper , a capacity-enhanced single-mode microwave this paper was proposed for microwave chemistry research at the frequency of 5.8 GHz, where the higher-order propagating electromagnetic modes of the microwave were restrained and only left the first-order TE10 mode.
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Mechanism for microwave heating of 1-(4'-cyanophenyl)-4-propylcyclohexane characterized by in situ microwave irradiation NMR spectroscopy.
Yugo Tasei,Takuya Yamakami,Izuru Kawamura,Teruaki Fujito,Kiminori Ushida,Motoyasu Sato,Akira Naito +6 more
TL;DR: It is demonstrated that microwave heating generates very high temperature within a short time using an in situ microwave irradiation NMR spectrometer.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.