Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
TLDR
In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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The preparation and application of mesoporous materials for energy storage
TL;DR: The mesoporous materials, with high surface area, narrow distribution of pore size, good corrosion resistance, high stability, and tunable pore structure and easy surface modification, are widely used as electrocatalyst support and electrode in EDLC as mentioned in this paper.
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Chemical Reactions with a Novel 5.8-GHz Microwave Apparatus. 1. Characterization of Properties of Common Solvents and Application in a Diels–Alder Organic Synthesis
TL;DR: In this article, the authors demonstrated the usefulness of 5.8 GHz microwave radiation for the synthesis of 3,6-diphenyl-4-n-butylpyridazine through a Diels-Alder process.
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The Application of Microwaves in Combinatorial and High‐Throughput Synthesis as New Synthetic Procedure in Drug Discovery
TL;DR: A review of microwave-assisted organic synthesis can be found in this paper, where the authors outline the basic principles behind microwave technology and summarize the areas in which microwave technology has made an impact, to date.
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A rapid and efficient protocol for the synthesis of novel nitrothiazolo[3,2-c]pyrimidines via microwave-mediated Mannich cyclisation
TL;DR: Several 6-substituted 8-nitrothiazolo[3,2-c]pyrimidine derivatives have been obtained very efficiently by a multicomponent cyclisation of 2-(nitromethylene)thiazolidine, formaldehyde and various aliphatic or aromatic amines in water, using both microwave irradiation and conventional heating.
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Effects of Ultrasound and Microwaves on Selective Reduction: Catalyst Preparation and Reactions
TL;DR: In this article, a review mainly focuses on the selective reduction of substrates with multiple functional groups with the goal of industrial demonstration of selective hydrogenations intensified by microwaves and ultrasound.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.