Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Microwave-assisted synthesis of nitrogen-containing 1-hydroxymethylenebisphosphonate drugs
TL;DR: In this article, a simple one-pot synthesis of heterocyclic (risedronate, zoledronate) and aminoalkyl bisphosphonate drugs using microwave irradiation is presented.
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Hydrolysis of sucrose by conventional and microwave heating in stirred tank reactor
TL;DR: In this article, the reaction kinetics of the hydrolysis of sucrose to fructose and glucose under catalysis by the strongly acidic cation-exchange resin Amberlite 200C in R-H form was investigated in thermal and microwave fields using a standard laboratory stirred tank reactor.
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Microwave-enhanced metal- and acid-catalysed hydrogen isotope exchange reactions
Jean M Barthez,Anton V. Filikov,Lottie B. Frederiksen,Marie-Loire Huguet,John R. Jones,Shuiyu Lu +5 more
TL;DR: The benefits of using microwaves to accelerate the rates of hydrogen isotope exchange reactions are illustrated by reference to heterogeneous and homogeneous metal-catalysed reactions as well as to... as discussed by the authors.
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Accelerated Heck reaction using ortho-palladated complex in a nonaqueous ionic liquid with controlled microwave heating
TL;DR: The Heck-Mizoroki CC cross-coupling reaction under conventional heating and microwave irradiation conditions in molten salt tetrabutylammonium bromide as the solvent and promoter at 130 °C was investigated in this article.
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Experimental study on removals of SO2 and NO(x) using adsorption of activated carbon/microwave desorption.
TL;DR: The pollutants control of flue gas in the power plants by the method of microwave-induced decomposition using adsorption of activated carbon/microwave desorption can meet the requirements of environmental protection, which will be stricter in the future.
References
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Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
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Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.