Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Solvent-free microwave-assisted Bingel reaction in carbon nanohorns
Solon P. Economopoulos,Georgia Pagona,Masako Yudasaka,Masako Yudasaka,Sumio Iijima,Sumio Iijima,Nikos Tagmatarchis +6 more
TL;DR: In this paper, the authors exploit the benefits of microwave assisted functionalization of carbon nanohorns (CNHs) using Bingel reaction conditions and successfully incorporate malonyl moieties in CNHs.
Journal ArticleDOI
Microwave‐assisted Chemical Reactions
Ah Keow Man,Radiman Shahidan +1 more
TL;DR: In this paper, the application of microwave assisted synthesis in the medicinal and pharmaceutical industries is discussed, and some of the reactions that have been accelerated with higher yields under MW irradiation are discussed.
Journal ArticleDOI
Rapid synthesis of ZnO nanostructures through microwave heating process
TL;DR: In this article, polycrystalline zinc oxide (ZnO) nanostructures have been prepared by a hydrothermal synthesis through rapid microwave heating (180 ǫs).
Journal ArticleDOI
Paramagnetism of cobalt-doped ZnO nanoparticles obtained by microwave solvothermal synthesis.
Jacek Wojnarowicz,Sylwia Kusnieruk,Tadeusz Chudoba,Stanislaw Gierlotka,Witold Lojkowski,W. Knoff,M.I. Lukasiewicz,Bartlomiej S. Witkowski,Anna Wolska,Marcin T. Klepka,Tomasz Story,Marek Godlewski +11 more
TL;DR: The results of the magentometry investigation indicated that all as-synthesized samples displayed paramagnetic properties with a contribution of anti-ferromagnetic coupling of Co–Co pairs, likely related to the precipitation of metallic Co in nanoparticles.
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Application of microwave energy to organic synthesis : improved technology
TL;DR: The application of microwave energy to the sulfonation of naphthalene and anthraquinone, to the amination of p -chloronitrobenzene, and to the hydrosilylation of 2-and 4- vinylpyridine has been studied as discussed by the authors.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.