Journal ArticleDOI
Application of commercial microwave ovens to organic synthesis.
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In this article, commercial microwave ovens have been safely used to dramatically reduce the reaction times (at comparable yield) of Diels-Alder, Claisen, and ene reactions.About:
This article is published in Tetrahedron Letters.The article was published on 1986-01-01. It has received 1028 citations till now. The article focuses on the topics: Microwave oven.read more
Citations
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Journal ArticleDOI
A novel and faster route for the synthesis of polyether-polycarbonate from carbon dioxide and epoxide through microwave irradiation
Manju Mamparambath Dharman,Ji-Yeon Ahn,Mi-Kyung Lee,Hye-Lim Shim,Kyung-Hoon Kim,Il Kim,Dae-Won Park +6 more
TL;DR: In this article, the authors investigated the utilization of CO2 in order to obtain polyether-polycarbonate by the co-polymerization of epoxide with CO2 using microwave irradiation.
Journal ArticleDOI
Highly efficient synthesis of extended triptycenes via Diels–Alder cycloaddition in water under microwave radiation
Bao Jian Pei,Albert W. M. Lee +1 more
TL;DR: In this article, the cycloadducts with high efficiencies were obtained by dehydration of 8a-g in a mixture of AcOH and Ac2O with good overall yields.
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A Green Approach for Organic Transformations Using Microwave Reactor
Subrata Das,Rupak Banik,Brajesh Kumar,Subhadip Roy,Noorussabah,Khursheed Amhad,Pradip K. Sukul +6 more
TL;DR: This study believes that the current study of the green microwave heating technique will be highly beneficial for the researchers from both academia and industry in their near future.
Dissertation
Eco-extraction par micro-ondes couplée à un champ centrifuge
TL;DR: In this article, le pilote experimental a l'echelle semi-industrielle combinant micro-ondes and centrifugation and son adaptation potentielle for le domaine de l’eco-extraction.
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Heterogeneous Phase Microwave-Assisted Reactions under CO2 or CO Pressure
Emanuela Calcio Gaudino,Laura Rinaldi,Laura Rotolo,Diego Carnaroglio,Camillo Pirola,Giancarlo Cravotto +5 more
TL;DR: A panoramic snapshot of MW-assisted organic reactions with gaseous reagents, in particular CO and CO2, and outline future applications of microwave heating to promote heterogeneous reactions under gas pressure is provided.
References
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Journal ArticleDOI
Acceleration of the diels-alder reaction by aluminum chloride
Peter Yates,Philip E. Eaton +1 more
Journal ArticleDOI
Some Reactions of Δ2-Cyclohexenone, Including the Synthesis of Bicyclo(2,2,2)-octanedione-2,6
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The reaction of anthracene with maleic and fumaric acid and their derivatives and with citraconic anhydride and mesaconic acid.
W. E. Bachmann,L. B. Scott +1 more
TL;DR: The initial precipitate of long dense needles had become contaminated by a small superficial layer of fluffy crystalline balls, apparently containing the saturated dioltrione (XXIV) and after two further recrystallizations from alcohol melted at 23!-238’.
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Chlorination of organoboranes: synthesis of (z)-vinyl chlorides
TL;DR: Chloration d'(alcene-1yl dihydroxy) boranes et obtention stereoselective de cis-chloro-1 alcenes as mentioned in this paper.